Synthesis, crystal structures and spectral characterization of imidazo[1,2-a]pyrimidin-2-yl-acetic acid and related analog with imidazo[2,1-b]thiazole ring
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- 作者：Agnieszka Dylonga ; Waldemar Goldemana ; Michał Sowaa ; Katarzyna Ślepokurab ; Piotr Drożdżewskia ; Ewa Matczak-Jona ; ewa.matczak-jon@pwr.edu.pl" class="auth_mail" title="E-mail the corresponding author
- 关键词：Imidazo[1 ; 2-a]pyrimidine ; Imidazo[2 ; 1-b]thiazole ; Single-crystal X-ray diffraction ; Hirshfeld surface analysis ; DFT calculations ; Vibrational spectroscopy
- 刊名：Journal of Molecular Structure
- 出版年：2016
- 出版时间：5 August 2016
- 年：2016
- 卷：1117
- 期：Complete
- 页码：153-163
- 全文大小：2628 K
文摘
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Acetate appended imidazo[1,2-a]pyrimidine and imidazo[2,1-b]thiazole.
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Structures of both compounds determined by single crystal X-ray diffraction.
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Hirshfeld surface analysis used for description of intermolecular interactions.
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IR and Raman spectra interpreted based on deuteration effects and DFT calculations.
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1H NMR experiments in solution confirm conclusions drawn from vibrational analysis.