Further understanding on the three domains of isotactic polypropylene by investigating the crystalline morphologies evolution after treatment at different domains

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• 作者：Ding-ding Hu ; Shi-bing Ye ; Fei Yu ; Jia-chun Feng 冯嘉斿/a>
• 关键词：Polypropylene ; Self ; nucleating ; Annealing ; Crystallization morphology
• 刊名：Chinese Journal of Polymer Science
• 出版年：2016
• 出版时间：March 2016
• 年：2016
• 卷：34
• 期：3
• 页码：344-358
• 全文大小：2,999 KB
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• 作者单位：Ding-ding Hu (1)
  Shi-bing Ye (1)
  Fei Yu (1)
  Jia-chun Feng 冯嘉春 (1)
  
  1. State Key Laboratory of Molecular Engineering of Polymers, Collaborative Innovation Center of Polymers and Polymer Composite Materials, Department of Macromolecular Science, Fudan University, Shanghai, 200433, China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Condensed Matter Physics
  Industrial Chemistry and Chemical Engineering
  Polymer Sciences
  Characterization and Evaluation of Materials
  
• 出版者：Chinese Chemical Society and Institute of Chemistry, CAS, co-published with Springer
• ISSN：1439-6203

文摘

The introduction of concept of the three domains of isotactic polypropylene (iPP) by Wittmann and Lotz et al. is an important advance in understanding the influence of the melt structures on the crystallization behaviors and consequent properties. To further understand the physical nature of the melt structures, the crystalline structures of iPP after thermal treatment in the three domains are systematically investigated. It is found that after treated at different domains the crystal morphologies, including the sizes and birefringence of spherulitic, the proportion of radial and tangential lamellae, etc., have distinctly different features. Our study reveals that the “nuclei” at domain II compose of locally ordered chains and the induced memory effect could not be erased under annealing treatment, while the “nuclei” at domain III compose of crystal fragments, which will aggregate under annealing process. Based on our results, highly schematic diagrams are proposed to illustrate the probable physical characteristics of the melt structures at the three different domains.