Adsorptive removal of resorcinol on a novel ordered mesoporous carbon(OMC) employing COK-19 silica scaffold:Kinetics and equilibrium study
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摘要
Phenolic compounds and their derivatives have been found in industrial wastewater, which pose threats to the natural environment. Ordered mesoporous carbon(OMC) has been identified as an ideal adsorbent possessing high specific surface area and large pore volume to alleviate these pollutants. A novel ordered mesoporous carbon was prepared using COK-19 template with the cubic Fm3 m structure for the first time. Ordered mesoporous silica COK-19 was synthesized and reported in 2015. Sucrose as the carbon precursor was impregnated into the mesopores of silica and converted to carbon through carbonization process using sulfuric acid as a catalyst. Ordered mesoporous carbon was obtained after the removal of silica framework using hydrofluoric acid. Boric acid was employed for the preparation of OMCs with tunable pore sizes in the range of 6.9–16.6 nm. Several characterization techniques such as nitrogen adsorption–desorption isotherms, transmission electron microscope(TEM), Fourier transform infrared spectroscopy, Boehm titration and elemental analysis were employed to characterize the OMCs. The pore size analysis and TEM images confirmed that OMC has replicated the mesostructure of the COK-19. Results obtained from adsorption kinetics and isotherms suggest that the Pseudo-second-order model and Langmuir isotherm well described the experimental data.
Phenolic compounds and their derivatives have been found in industrial wastewater, which pose threats to the natural environment. Ordered mesoporous carbon(OMC) has been identified as an ideal adsorbent possessing high specific surface area and large pore volume to alleviate these pollutants. A novel ordered mesoporous carbon was prepared using COK-19 template with the cubic Fm3 m structure for the first time. Ordered mesoporous silica COK-19 was synthesized and reported in 2015. Sucrose as the carbon precursor was impregnated into the mesopores of silica and converted to carbon through carbonization process using sulfuric acid as a catalyst. Ordered mesoporous carbon was obtained after the removal of silica framework using hydrofluoric acid. Boric acid was employed for the preparation of OMCs with tunable pore sizes in the range of 6.9–16.6 nm. Several characterization techniques such as nitrogen adsorption–desorption isotherms, transmission electron microscope(TEM), Fourier transform infrared spectroscopy, Boehm titration and elemental analysis were employed to characterize the OMCs. The pore size analysis and TEM images confirmed that OMC has replicated the mesostructure of the COK-19. Results obtained from adsorption kinetics and isotherms suggest that the Pseudo-second-order model and Langmuir isotherm well described the experimental data.
Phenolic compounds and their derivatives have been found in industrial wastewater, which pose threats to the natural environment. Ordered mesoporous carbon(OMC) has been identified as an ideal adsorbent possessing high specific surface area and large pore volume to alleviate these pollutants. A novel ordered mesoporous carbon was prepared using COK-19 template with the cubic Fm3 m structure for the first time. Ordered mesoporous silica COK-19 was synthesized and reported in 2015. Sucrose as the carbon precursor was impregnated into the mesopores of silica and converted to carbon through carbonization process using sulfuric acid as a catalyst. Ordered mesoporous carbon was obtained after the removal of silica framework using hydrofluoric acid. Boric acid was employed for the preparation of OMCs with tunable pore sizes in the range of 6.9–16.6 nm. Several characterization techniques such as nitrogen adsorption–desorption isotherms, transmission electron microscope(TEM), Fourier transform infrared spectroscopy, Boehm titration and elemental analysis were employed to characterize the OMCs. The pore size analysis and TEM images confirmed that OMC has replicated the mesostructure of the COK-19. Results obtained from adsorption kinetics and isotherms suggest that the Pseudo-second-order model and Langmuir isotherm well described the experimental data.
引文
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Goscianska,J.,Marciniak,M.,Pietrzak,R.,2014.Mesoporous carbons modified with lanthanum(III)chloride for methyl orange adsorption.Chem.Eng.J.247,258-264.
Goscianska,J.,Marciniak,M.,Pietrzak,R.,2015.Ordered mesoporous carbons modified with cerium as effective adsorbents for azo dyes removal.Sep.Purif.Technol.154,236-245.
Goscianska,J.,Fathy,N.A.,Aboelenin,R.M.M.,2017.Adsorption of solophenyl red 3BL polyazo dye onto amine-functionalized mesoporous carbons.J.Colloid Interface Sci.505,593-604.
Goscianska,J.,Pietrzak,R.,Matos,J.,2018.Catalytic performance of ordered mesoporous carbons modified with lanthanides in dry methane reforming.Catal.Today 301,204-216.
Guo,R.,Guo,J.,Yu,F.,Gang,D.D.,2013.Synthesis and surface functional group modifications of ordered mesoporous carbons for resorcinol removal.Microporous Mesoporous Mater.175,141-146.
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Konggidinata,M.I.,Chao,B.,Lian,Q.,Subramaniam,R.,Zappi,M.Gang,D.D.,2017.Equilibrium,kinetic and thermodynamic studies for adsorption of BTEX onto Ordered Mesoporous Carbon(OMC).J.Hazard.Mater.336,249-259.
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Arafat,A.A.,Franz,M.,Pinto,N.G.,1999.Effect of salt on the mechanism of adsorption of aromatics on activated carbon.Langmuir 15(18),5997-6003.
Arana,J.,Melian,E.P.,López,V.R.,Alonso,A.P.,Rodríguez,J.D.,Díaz,O.G.,et al.,2007.Photocatalytic degradation of phenol and phenolic compounds:Part I.Adsorption and FTIR study.J.Hazard.Mater.146,520-528.
Bashkova,S.,Bagreev,A.,Bandosz,T.J.,2003.Adsorption/oxidation of CH3SH on activated carbons containing nitrogen.Langmuir 19(15),6115-6121.
Bayram,E.,Hoda,N.,Ayranci,E.,2009.Adsorption/electrosorption of catechol and resorcinol onto high area activated carbon cloth.J.Hazard.Mater.168,1459-1466.
Belhamdi,B.,Merzougui,Z.,Trari,M.,Addoun,A.,2016.A kinetic equilibrium and thermodynamic study of l-phenylalanine adsorption using activated carbon based on agricultural waste(date stones).J.Appl.Res.Technol.14,354-366.
Boehm,H.P.,1994.Some aspects of the surface chemistry of carbon blacks and other carbons.Carbon 32,759-769.
Cansado,I.P.,Mour?o,P.A.,Falc?o,A.I.,Carrott,M.R.,Carrott,P.J.,2012.The influence of the activated carbon post-treatment on the phenolic compounds removal.Fuel Process.Technol.103,64-70.
Chai,G.S.,Yoon,S.B.,Yu,J.S.,Choi,J.H.,Sung,Y.E.,2004.Ordered porous carbons with tunable pore sizes as catalyst supports in direct methanol fuel cell.J.Phys.Chem.B 108,7074-7079.
Chao,B.,Konggidinata,M.I.,Lin,L.,Zappi,M.,Gang,D.D.,2017.Effect of carbon precursors and pore expanding reagent on ordered mesoporous carbon for resorcinol removal.J.Water Process Eng.17,256-263.
Chen,T.,Wang,T.,Wang,D.J.,Xue,H.R.,Zhao,J.Q.,Ding,X.C.,et al.,2011.Synthesis of ordered large-pore mesoporous carbon for Cr(VI)adsorption.Mater.Res.Bull.46,1424-1430.
Chutia,P.,Kato,S.,Kojima,T.,Satokawa,S.,2009.Adsorption of As(V)on surfactant-modified natural zeolites.J.Hazard.Mater.162,204-211.
Din,A.T.M.,Hameed,B.H.,Ahmad,A.L.,2009.Batch adsorption of phenol onto physiochemical-activated coconut shell.J.Hazard.Mater.161,1522-1529.
Dai,W.,Zheng,M.,Zhao,Y.,Liao,S.,Ji,G.,Cao,J.,2009.Template synthesis of three-dimensional cubic ordered mesoporous carbon with tunable pore sizes.Nanoscale Res.Lett.5,103-107.
Darmstadt,H.,Roy,C.,Kaliaguine,S.,Choi,S.J.,Ryoo,R.,2002.Surface chemistry of ordered mesoporous carbons.Carbon 40,2673-2683.
Duan,F.,Yang,Y.,Li,Y.,Cao,H.,Wang,Y.,Zhang,Y.,2014.Heterogeneous Fenton-like degradation of 4-chlorophenol using iron/ordered mesoporous carbon catalyst.J.Environ.Sci.26,1171-1179.
Dursun,A.Y.,Kalayci,C.S.,2005.Equilibrium,kinetic and thermodynamic studies on the adsorption of phenol onto chitin.J.Hazard.Mater.123,151-157.
El-Naas,M.H.,Al-Zuhair,S.,Alhaija,M.A.,2010.Removal of phenol from petroleum refinery wastewater through adsorption on date-pit activated carbon.Chem.Eng.J.162(3),997-1005.
Fang,B.,Zhou,H.,Honma,I.,2006.Ordered porous carbon with tailored pore size for electrochemical hydrogen storage application.J.Phys.Chem.B 110,4875-4880.
Freundlich,H.,1907.über die adsorption in l?sungen.Z.Phys.Chem.57,385-470.
Fuertes,A.B.,Sonia,A.,2004.Graphitic mesoporous carbons synthesised through mesostructured silica templates.Carbon42,3049-3055.
Fytianos,K.,Voudrias,E.,Kokkalis,E.,2000.Sorption-desorption behaviour of 2,4-dichlorophenol by marine sediments.Chemosphere 40,3-6.
Gattrell,M.,Kirk,D.W.,1990.The electrochemical oxidation of aqueous phenol at a glassy carbon electrode.Can.J.Chem.Eng.68,997-1003.
Goscianska,J.,Olejnik,A.,2018.Dispersion stability of the aminosilane-grafted mesoporous carbons in different solvents.Microporous Mesoporous Mater.265,149-161.
Goscianska,J.,Marciniak,M.,Pietrzak,R.,2014.Mesoporous carbons modified with lanthanum(III)chloride for methyl orange adsorption.Chem.Eng.J.247,258-264.
Goscianska,J.,Marciniak,M.,Pietrzak,R.,2015.Ordered mesoporous carbons modified with cerium as effective adsorbents for azo dyes removal.Sep.Purif.Technol.154,236-245.
Goscianska,J.,Fathy,N.A.,Aboelenin,R.M.M.,2017.Adsorption of solophenyl red 3BL polyazo dye onto amine-functionalized mesoporous carbons.J.Colloid Interface Sci.505,593-604.
Goscianska,J.,Pietrzak,R.,Matos,J.,2018.Catalytic performance of ordered mesoporous carbons modified with lanthanides in dry methane reforming.Catal.Today 301,204-216.
Guo,R.,Guo,J.,Yu,F.,Gang,D.D.,2013.Synthesis and surface functional group modifications of ordered mesoporous carbons for resorcinol removal.Microporous Mesoporous Mater.175,141-146.
Huang,J.,Huang,K.,Yan,C.,2009.Application of an easily water-compatible hypercrosslinked polymeric adsorbent for efficient removal of catechol and resorcinol in aqueous solution.J.Hazard.Mater.167,69-74.
Joo,S.H.,Jun,S.,Ryoo,R.,2001.Synthesis of ordered mesoporous carbon molecular sieves CMK-1.Microporous Mesoporous Mater.44,153-158.
Joo,J.B.,Kim,P.,Kim,W.,Kim,J.,Yi,J.,2006.Preparation of mesoporous carbon templated by silica particles for use as a catalyst support in polymer electrolyte membrane fuel cells.Catal.Today 111,171-175.
Katsoulidis,A.P.,Kanatzidis,M.G.,2011.Phloroglucinol based microporous polymeric organic frameworks with-OHfunctional groups and high CO2 capture capacity.Chem.Mater.23,1818-1824.
Kerkhofs,S.,Willhammar,T.,Van Den Noortgate,H.,Kirschhock C.E.,Breynaert,E.,Van Tendeloo,G.,et al.,2015.Self assembly of Pluronic F127-silica spherical coreshell nanoparticles in cubic close-packed structures.Chem.Mater.27,5161-5169.
Kim,S.S.,Karkamkar,A.,Pinnavaia,T.J.,Kruk,M.,Jaroniec,M.,2001.Synthesis and characterization of ordered,very large pore MSU-H silicas assembled from water-soluble silicates.J.Phys.Chem.B 105,7663-7670.
Kim,C.H.,Lee,D.K.,Pinnavaia,T.J.,2004.Graphitic mesostructured carbon prepared from aromatic precursors.Langmuir 20,5157-5159.
Kim,D.J.,Lee,H.I.,Yie,J.E.,Kim,S.J.,Kim,J.M.,2005.Ordered mesoporous carbons:implication of surface chemistry,pore structure and adsorption of methyl mercaptan.Carbon 43,1868-1873.
Konggidinata,M.I.,Chao,B.,Lian,Q.,Subramaniam,R.,Zappi,M.Gang,D.D.,2017.Equilibrium,kinetic and thermodynamic studies for adsorption of BTEX onto Ordered Mesoporous Carbon(OMC).J.Hazard.Mater.336,249-259.
Kresge,C.T.,Leonowicz,M.E.,Roth,W.J.,Vartuli,J.C.,Beck,J.S.,1992.Ordered mesoporous molecular sieves synthesized by a liquid-crystal template mechanism.Nature 359,710-712.
Kumar,A.,Kumar,S.,Kumar,S.,2003.Adsorption of resorcinol and catechol on granular activated carbon:equilibrium and kinetics.Carbon 41,3015-3025.
Kumar,S.,Zafar,M.,Prajapati,J.K.,Kumar,S.,Kannepalli,S.,2011Modeling studies on simultaneous adsorption of phenol and resorcinol onto granular activated carbon from simulated aqueous solution.J.Hazard.Mater.185,287-294.
Lin,S.H.,Juang,R.S.,2009.Adsorption of phenol and its derivatives from water using synthetic resins and low-cost natural adsorbents:a review.J.Environ.Manag.90,1336-1349.
Lagergren,S.,1898.Zur theorie der sogenannten adsorption geloster stoffe.Kungliga svenska vetenskapsakademiens.Handlingar 24,1-39.
Lee,W.H.,Reucroft,P.J.,1999.Vapor adsorption on coal-and wood-based chemically activated carbons:(I)surface oxidation states and adsorption of H2O.Carbon 37(1),7-14.
Lee,J.S.,Joo,S.H.,Ryoo,R.,2002.Synthesis of mesoporous silicas of controlled pore wall thickness and their replication to ordered nanoporous carbons with various pore diameters.J.Am.Chem.Soc.124,1156-1157.
Lee,H.I.,Kim,J.H.,You,D.J.,Lee,J.E.,Kim,J.M.,Ahn,W.S.,et al.,2008.Rational synthesis pathway for ordered mesoporous carbon with controllable 30-to 100-Angstrom pores.Adv.Mater.20,757-762.
Lettow,J.S.,Han,Y.J.,Schmidt-Winkel,P.,Yang,P.,Zhao,D.,Stucky,G.D.,et al.,2000.Hexagonal to mesocellular foam phase transition in polymer-templated mesoporous silicas.Langmuir 16,8291-8295.
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