4-松油醇型白千层枝叶连续提取茶树油及黄酮的技术
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摘要
采用水蒸气蒸馏法从白千层(Melaleuca)枝叶中提取茶树油,直接从生产的废水废渣中用水连续提取水溶性黄酮,浓缩干燥制备白千层黄酮。结果表明,提取的茶树油质量达到ISO 4730:2017标准,产品黄酮含量为18.1%。
Tea tree oil was extracted by steam distillation from the branches and leaves of terpinen-4-ol type Melaleuca and water-soluble flavonoids were continuously extracted by water directly from the waste water and residue, then concentrated and dried to prepare the flavonoids. Results showed that the quality of tea tree oil reached ISO 4730:2017 standard and the flavonoid content was 18.1%.
Tea tree oil was extracted by steam distillation from the branches and leaves of terpinen-4-ol type Melaleuca and water-soluble flavonoids were continuously extracted by water directly from the waste water and residue, then concentrated and dried to prepare the flavonoids. Results showed that the quality of tea tree oil reached ISO 4730:2017 standard and the flavonoid content was 18.1%.
引文
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[10]范超君,鲍长余,陈湛娟,等.白千层枝和叶总黄酮含量的测定[J].海南师范大学学报:自然科学版,2012,25(1):63-65.
[11]张燕君,陈利芳.蒸馏时间与互叶白千层精油主要化学成分及出油率关系的研究[J].林产化学与工业,2002,22(3):33-36.
[12]陈祖洪,周丽珠,梁忠云,等.不同蒸馏方式对茶树油主要成分含量及得油率的影响[J].林产化工通讯,2003,(37)5:21-22.
[13]刘布鸣,林霄,邱宏聪,等.互叶白千层总黄酮的制备及其检测方法:201510247241.0[P].2015-05-19.
[2]柯家厚.一种采用澳洲茶树渣制备的营养均衡的平菇培养基以及制备方法:201510389450.9[P].2015-07-06.
[3]VIEIRA T R,BERBASA L C A,MALTHA C R A,et al.Chemical constituents from Melaleuca alternifolia(Mytraceae)[J].Quimica Nova,2009,27(4):536-539.
[4]刘布鸣,董晓敏,黄艳,等.互叶白千层的化学成分研究[J].中草药,2011,42(7):1282-1284.
[5]林霄,董晓敏,陈明生,等.高效液相色谱法同时测定互叶白千层中的槲皮素和山奈酚[J].林产化学与工业,2012,32(4):113-116.
[6]李燕婧,钟正贤,林霄,等.互叶白千层水提物药理作用研究[J].中医药导报,2013,19(5):86-88.
[7]李燕婧,钟正贤,林霄,等.互叶白千层醇提物的药理作用研究[J].广西中医药,2013,36(3):77-79.
[8]刘祥义,凌清华,周光平.一种同时提取澳洲茶树黄酮和β-谷甾醇的方法:CN 103159724 A[P].2013-06-19.
[9]刘祥义,凌清华,周光平.同时提取澳洲茶树精油及黄酮甙的方法:CN 103146473 A[P].2013-06-12.
[10]范超君,鲍长余,陈湛娟,等.白千层枝和叶总黄酮含量的测定[J].海南师范大学学报:自然科学版,2012,25(1):63-65.
[11]张燕君,陈利芳.蒸馏时间与互叶白千层精油主要化学成分及出油率关系的研究[J].林产化学与工业,2002,22(3):33-36.
[12]陈祖洪,周丽珠,梁忠云,等.不同蒸馏方式对茶树油主要成分含量及得油率的影响[J].林产化工通讯,2003,(37)5:21-22.
[13]刘布鸣,林霄,邱宏聪,等.互叶白千层总黄酮的制备及其检测方法:201510247241.0[P].2015-05-19.