辛夷药材及嫁接品种挥发油的GC-MS鉴别研究
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摘要
目的:建立辛夷药材挥发油GC-MS分析法,区别辛夷药材的不同来源。方法:采用GC-MS法,对比找出不同品种辛夷药材及嫁接品种的特有成分。结果:不同品种的辛夷药材及嫁接品种间的化学成分差异较大,对比分析,可指认出3个望春花的特有成分、13个武当玉兰的特有成分、2个玉兰的特有成分及5个河南嫁接品种的特有成分。结论:通过分析可找出不同品种辛夷的化学特征性成分,表明该方法可用于市场上辛夷药材的不同品种及挥发油提取物的来源鉴别。
Objective: To develop a GC-MS method for volatile oil of Magnoliae Flos, and to distinguish different sources of Magnoliae Flos. Methods: GC-MS method was used to find out the unique components of different varieties of Magnoliae Flos and grafted varieties. Results: The chemical constituents of Magnoliae Flos of different varieties and grafted varieties were different. The comparative analysis showed that three characteristic components were in Magnolia biondii Pamp., thirteen characteristic components were in Magnolia sprengeri Pamp., and two characteristic component was in Magnolia denudata Desr.. Meanwhile, five characteristic components were in grafted varieties of Henan. Conclusion: The characteristic components of different varieties can be found by analysis. This method can be used to identify the different varieties of Magnoliae Flos and different sources of volatile oil extracts in the market.
Objective: To develop a GC-MS method for volatile oil of Magnoliae Flos, and to distinguish different sources of Magnoliae Flos. Methods: GC-MS method was used to find out the unique components of different varieties of Magnoliae Flos and grafted varieties. Results: The chemical constituents of Magnoliae Flos of different varieties and grafted varieties were different. The comparative analysis showed that three characteristic components were in Magnolia biondii Pamp., thirteen characteristic components were in Magnolia sprengeri Pamp., and two characteristic component was in Magnolia denudata Desr.. Meanwhile, five characteristic components were in grafted varieties of Henan. Conclusion: The characteristic components of different varieties can be found by analysis. This method can be used to identify the different varieties of Magnoliae Flos and different sources of volatile oil extracts in the market.
引文
[1]国家药典委员会.中华人民共和国药典.一部.北京:中国医药科技出版社,2015:182
[2]尹献忠,李晓,李胜华,等.水蒸气蒸馏法提取辛夷精油及在卷烟加香中的应用研究.郑州轻工业学学院学报,2003,18(4):65-67
[3]魏鹏程.辛夷致香物质提取分离及在卷烟中的加香应用.郑州:河南农业大学,2013
[4]刘星,单杨.辛夷的提取、应用及其品质评价研究进展.食品工业科技,2011(11):506-510
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[6]马羚.川产辛夷及其嫁接品种的品质研究.成都:成都中医药大学,2007
[7]张婷婷,郭夏丽,黄学勇,等.辛夷挥发油GC-MS分析及其抗氧化、抗菌活性.食品科学,2016,37(10):144-150
[8]杨健,徐植灵,潘炯光,等.辛夷挥发油的成分分析.中国中药杂志,1998,23(5):295-298
[9]蔡桂香,刘应煊,胡卫兵.广玉兰花香精油的化学成分及其抗氧化活性研究.化学与生物工程,2012,29(9):91-94
[2]尹献忠,李晓,李胜华,等.水蒸气蒸馏法提取辛夷精油及在卷烟加香中的应用研究.郑州轻工业学学院学报,2003,18(4):65-67
[3]魏鹏程.辛夷致香物质提取分离及在卷烟中的加香应用.郑州:河南农业大学,2013
[4]刘星,单杨.辛夷的提取、应用及其品质评价研究进展.食品工业科技,2011(11):506-510
[5]国家药典委员会.中华人民共和国药典.四部.北京:中国医药科技出版社,2015:203
[6]马羚.川产辛夷及其嫁接品种的品质研究.成都:成都中医药大学,2007
[7]张婷婷,郭夏丽,黄学勇,等.辛夷挥发油GC-MS分析及其抗氧化、抗菌活性.食品科学,2016,37(10):144-150
[8]杨健,徐植灵,潘炯光,等.辛夷挥发油的成分分析.中国中药杂志,1998,23(5):295-298
[9]蔡桂香,刘应煊,胡卫兵.广玉兰花香精油的化学成分及其抗氧化活性研究.化学与生物工程,2012,29(9):91-94