水中苯氧羧酸类除草剂残留检测的研究进展
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摘要
随着苯氧羧酸类除草剂使用量和使用范围的日益增大,该类除草剂已成为影响水质安全和人类身体健康的重要因素。实现水中苯氧羧酸类除草剂的有效吸附富集和快速测定对保证水质安全和人类身体健康具有重要意义。对水中苯氧羧酸类除草剂残留检测的前处理方法,水滑石在吸附水中苯氧羧酸类除草剂的应用及水中苯氧羧酸类除草剂残留的检测方法进行了分析与探讨,旨在为实现水中苯氧羧酸类除草剂的有效吸附富集和快速测定提供依据。
Along with increasing enlargement of the range and quantity of phenoxyacid herbicides used, it had became the important factor that affected water quality security and human health. Realization of effective adsorption and rapid determination of phenoxyacid herbicides in water had great significance for ensuring water quality security and human health. In order to provide basis for achieving effective adsorption and rapid determination of phenoxyacid herbicides in water, the study presented analysis and discussion on pretreatment methods of detection of phenoxyacid herbicides residues in water, application of hydrotalcite used in adsorption of phenoxyacid herbicides in water and detection methods of phenoxyacid herbicides residues in water.
Along with increasing enlargement of the range and quantity of phenoxyacid herbicides used, it had became the important factor that affected water quality security and human health. Realization of effective adsorption and rapid determination of phenoxyacid herbicides in water had great significance for ensuring water quality security and human health. In order to provide basis for achieving effective adsorption and rapid determination of phenoxyacid herbicides in water, the study presented analysis and discussion on pretreatment methods of detection of phenoxyacid herbicides residues in water, application of hydrotalcite used in adsorption of phenoxyacid herbicides in water and detection methods of phenoxyacid herbicides residues in water.
引文
[1]董凤伟,范丽娜,邢丽梅,等.苯氧羧酸类除草剂的分析方法综述[C]//公共安全中的化学问题研究进展(第二卷)[A].中国化学会,2011:5.
[2]张静,张文君,周欣欣,等.我国除草剂产品登记现状及分析[J].农药科学与管理,2013,34(04):20-23.
[3]PURCELL M,NEAULT J F,MALONGA H,et al.Interactions of atrazine and 2,4-D with human serum albumin studied by gel and capillary electrophoresis and FTIR spectroscopy[J].Biochimica Biophysica Acta,2001,1548(1):129-138.
[4]于艳伟.层状氢氧化镁铝的改性成型及其对卤素阴离子的吸附性能[D].青岛:中国海洋大学,2010.
[5]XU S,YU J Y,SUN Y B,et al.Synthesis and characterization of organic intercalated layered double hydroxides and their application in bitumen modification[J].Materials Chemistry and Physics,2015(152):54-61.
[6]BOUBERKA Z,BENABBOU K A,KHENIFI A,et al.Degradation by irradiation of an acid orange 7 on colloidal Ti O2/(LDHs)[J].Journal of Photochemistry and Photobiology A:Chemistry,2014(275):21-29.
[7]张泾凯,鄢姝恺,顾俊,等.液-液萃取/高效液相色谱法测定水中灭草松和2,4-滴[J].中国给水排水,2013,29(06):100-101,105.
[8]张莉,桂建业,张永涛,等.预衍生化-气相色谱-质谱法测定水中酸性除草剂[J].理化检验(化学分册),2011,47(01):8-11.
[9]MALOSCHIK E,M?RTL M,SZéKáCS A.Novel derivatisation technique for the determination of chlorophenoxy acid type herbicides by gas chromatography-mass spectrometry[J].Analytical and Bioanalytical Chemistry,2010,397(2):537-548.
[10]郑磊,胡小键,张海婧,等.饮用水中痕量灭草松和2,4-滴的固相萃取-高效液相色谱串联质谱测定法[J].环境与健康杂志,2015,32(03):246-248.
[11]王家斌,吴芳玲,赵琦.整体柱在线固相微萃取-高效液相色谱同步富集检测水中的苯氧羧酸类除草剂[J].色谱,2015,33(08):849-855.
[12]SCHEYER A,BRIAND O,MORVILLE S,et al.Analysis of trace levels of pesticides in rainwater by SPME and GCtandem mass spectrome-try after derivatisation with PFFBr[J].Analytical and Bioanalytical Chemistry,2007,387(1):359-368.
[13]杨素萍,郭振福,刘敏,等.功能化离子液体/离子液体分散液-液微萃取测定水中苯氧羧酸类除草剂[J].分析化学,2015,43(06):904-908.
[14]BEHBAHANI M,NAJAFI F,BAGHERI S,et al.Coupling of solvent-based de-emulsification dispersive liquid-liquid microextraction with high performance liquid chromatography for simultaneous simple and rapid trace monitoring of 2,4-dichlorophenoxyacetic acid and 2-methyl-4-chlorophenoxyacetic acid[J].Environmental Monitoring and Assessment,2014,186(4):2609-2618.
[15]POPOV S A,CHUMICHKINA Y A,SHAPOVALOVA E N,et al.Preconcentration of 2,4-dichlorophenoxyacetic acid on molecularly imprinted polymers and its subsequent determination by high performance liquid chromatography[J].Journal of Analytical Chemistry,2011,66(1):6-10.
[16]CHAPARADZA A,HOSSENLOPP J M.Removal of 2,4-dichlorophenoxyacetic acid by calcined Zn-Al-Zr layered double hydroxide[J].Journal of Colloid and Interface Science,2011,363(1):92-97.
[17]CARDOSO L P,VALIM J B.Study of acids herbicides removal by calcined Mg-Al-CO3-LDH[J].Journal of Physics and Chemistry of Solids,2006,67(5):987-993.
[18]PAVLOVIC I,GONZáLEZ M A,RODRíGUEZRIVAS F,et al.Caprylate intercalated layered double hydroxide as adsorbent of the linuron,2,4-DB and metamitron pesticides from aqueous solution[J].Journal of Applied Clay Science,2013,80-81(4):76-84.
[19]NEJATI K,DAVARY S,SAATI M.Study of 2,4-dichlorophenoxyacetic acid(2,4-D)removal by Cu-Fe-layered double hydroxide from aqueous solution[J].Journal of Applied Surface Science,2013,280(9):67-73.
[20]张念华,王军淋,应英,等.全自动固相萃取-气相色谱法检测水中的2,4-滴[J].中国卫生检验杂志,2016(01):26-27.
[21]谭海彬,曾锦明.柱前衍生-气相色谱法同时测定饮用水中2,4-滴和灭草松[J].广东化工,2012,39(1):99-100.
[22]李慧,戴晓莹,许欢.固相萃取-硅烷化衍生-气相色谱-质谱法测定水中2,4-滴[J].理化检验(化学分册),2013,49(8):997-998.
[23]张永涛,张莉,左海英,等.重氮甲烷衍生气相色谱-质谱法检测地下水中17种酸性除草剂[J].岩矿测试,2010,29(4):345-349.
[24]FARHADI K,MATIN A A,HASHEMI P.LC determination of trace amounts of phenoxyacetic acid herbicides in water after dispersive liquid-liquid microextraction[J].Chromatographia,2009,69(1):45-49.
[25]彭晓俊,庞晋山,邓爱华.中空纤维三相液相微萃取-高效液相色谱法测定环境水样中的7种苯氧羧酸类除草剂[J].色谱,2011,29(12):1199-1204.
[26]周弛,王斐,郭晋君,等.浅析高效液相色谱-质谱/质谱法测定饮用水中的灭草松和2,4-D[J].地下水,2015,37(2):183-183.
[27]CAPPIELLO A,PIERINI E,PALMA P.An SPE method for the concurrent extraction of organochlorine and phenoxy acidic pesticides in river water[J].Chromatographia,2011,73(7):691-699.
[28]朱惠扬,甘平胜,李晓晶.离子色谱法测定水中2,4-滴[J].中国卫生检验杂志,2013,23(4):845-846.
[29]丘露,邓钧.离子色谱法同时检测饮用水中草甘膦、2,4-D和灭草松[J].广东农业科学,2013,40(2):93-94.
[2]张静,张文君,周欣欣,等.我国除草剂产品登记现状及分析[J].农药科学与管理,2013,34(04):20-23.
[3]PURCELL M,NEAULT J F,MALONGA H,et al.Interactions of atrazine and 2,4-D with human serum albumin studied by gel and capillary electrophoresis and FTIR spectroscopy[J].Biochimica Biophysica Acta,2001,1548(1):129-138.
[4]于艳伟.层状氢氧化镁铝的改性成型及其对卤素阴离子的吸附性能[D].青岛:中国海洋大学,2010.
[5]XU S,YU J Y,SUN Y B,et al.Synthesis and characterization of organic intercalated layered double hydroxides and their application in bitumen modification[J].Materials Chemistry and Physics,2015(152):54-61.
[6]BOUBERKA Z,BENABBOU K A,KHENIFI A,et al.Degradation by irradiation of an acid orange 7 on colloidal Ti O2/(LDHs)[J].Journal of Photochemistry and Photobiology A:Chemistry,2014(275):21-29.
[7]张泾凯,鄢姝恺,顾俊,等.液-液萃取/高效液相色谱法测定水中灭草松和2,4-滴[J].中国给水排水,2013,29(06):100-101,105.
[8]张莉,桂建业,张永涛,等.预衍生化-气相色谱-质谱法测定水中酸性除草剂[J].理化检验(化学分册),2011,47(01):8-11.
[9]MALOSCHIK E,M?RTL M,SZéKáCS A.Novel derivatisation technique for the determination of chlorophenoxy acid type herbicides by gas chromatography-mass spectrometry[J].Analytical and Bioanalytical Chemistry,2010,397(2):537-548.
[10]郑磊,胡小键,张海婧,等.饮用水中痕量灭草松和2,4-滴的固相萃取-高效液相色谱串联质谱测定法[J].环境与健康杂志,2015,32(03):246-248.
[11]王家斌,吴芳玲,赵琦.整体柱在线固相微萃取-高效液相色谱同步富集检测水中的苯氧羧酸类除草剂[J].色谱,2015,33(08):849-855.
[12]SCHEYER A,BRIAND O,MORVILLE S,et al.Analysis of trace levels of pesticides in rainwater by SPME and GCtandem mass spectrome-try after derivatisation with PFFBr[J].Analytical and Bioanalytical Chemistry,2007,387(1):359-368.
[13]杨素萍,郭振福,刘敏,等.功能化离子液体/离子液体分散液-液微萃取测定水中苯氧羧酸类除草剂[J].分析化学,2015,43(06):904-908.
[14]BEHBAHANI M,NAJAFI F,BAGHERI S,et al.Coupling of solvent-based de-emulsification dispersive liquid-liquid microextraction with high performance liquid chromatography for simultaneous simple and rapid trace monitoring of 2,4-dichlorophenoxyacetic acid and 2-methyl-4-chlorophenoxyacetic acid[J].Environmental Monitoring and Assessment,2014,186(4):2609-2618.
[15]POPOV S A,CHUMICHKINA Y A,SHAPOVALOVA E N,et al.Preconcentration of 2,4-dichlorophenoxyacetic acid on molecularly imprinted polymers and its subsequent determination by high performance liquid chromatography[J].Journal of Analytical Chemistry,2011,66(1):6-10.
[16]CHAPARADZA A,HOSSENLOPP J M.Removal of 2,4-dichlorophenoxyacetic acid by calcined Zn-Al-Zr layered double hydroxide[J].Journal of Colloid and Interface Science,2011,363(1):92-97.
[17]CARDOSO L P,VALIM J B.Study of acids herbicides removal by calcined Mg-Al-CO3-LDH[J].Journal of Physics and Chemistry of Solids,2006,67(5):987-993.
[18]PAVLOVIC I,GONZáLEZ M A,RODRíGUEZRIVAS F,et al.Caprylate intercalated layered double hydroxide as adsorbent of the linuron,2,4-DB and metamitron pesticides from aqueous solution[J].Journal of Applied Clay Science,2013,80-81(4):76-84.
[19]NEJATI K,DAVARY S,SAATI M.Study of 2,4-dichlorophenoxyacetic acid(2,4-D)removal by Cu-Fe-layered double hydroxide from aqueous solution[J].Journal of Applied Surface Science,2013,280(9):67-73.
[20]张念华,王军淋,应英,等.全自动固相萃取-气相色谱法检测水中的2,4-滴[J].中国卫生检验杂志,2016(01):26-27.
[21]谭海彬,曾锦明.柱前衍生-气相色谱法同时测定饮用水中2,4-滴和灭草松[J].广东化工,2012,39(1):99-100.
[22]李慧,戴晓莹,许欢.固相萃取-硅烷化衍生-气相色谱-质谱法测定水中2,4-滴[J].理化检验(化学分册),2013,49(8):997-998.
[23]张永涛,张莉,左海英,等.重氮甲烷衍生气相色谱-质谱法检测地下水中17种酸性除草剂[J].岩矿测试,2010,29(4):345-349.
[24]FARHADI K,MATIN A A,HASHEMI P.LC determination of trace amounts of phenoxyacetic acid herbicides in water after dispersive liquid-liquid microextraction[J].Chromatographia,2009,69(1):45-49.
[25]彭晓俊,庞晋山,邓爱华.中空纤维三相液相微萃取-高效液相色谱法测定环境水样中的7种苯氧羧酸类除草剂[J].色谱,2011,29(12):1199-1204.
[26]周弛,王斐,郭晋君,等.浅析高效液相色谱-质谱/质谱法测定饮用水中的灭草松和2,4-D[J].地下水,2015,37(2):183-183.
[27]CAPPIELLO A,PIERINI E,PALMA P.An SPE method for the concurrent extraction of organochlorine and phenoxy acidic pesticides in river water[J].Chromatographia,2011,73(7):691-699.
[28]朱惠扬,甘平胜,李晓晶.离子色谱法测定水中2,4-滴[J].中国卫生检验杂志,2013,23(4):845-846.
[29]丘露,邓钧.离子色谱法同时检测饮用水中草甘膦、2,4-D和灭草松[J].广东农业科学,2013,40(2):93-94.