Methods and Protocols for Electrochemical Energy Storage Materials Research

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• 作者：Elahe Talaie ; Patrick Bonnick ; Xiaoqi Sun ; Quan Pang ; Xiao Liang ; Linda F. Nazar
• 刊名：Chemistry of Materials
• 出版年：2017
• 出版时间：January 10, 2017
• 年：2017
• 卷：29
• 期：1
• 页码：90-105
• 全文大小：991K
• ISSN：1520-5002

文摘

We present an overview of the procedures and methods to prepare and evaluate materials for electrochemical cells in battery research in our laboratory, including cell fabrication, two- and three-electrode cell studies, and methodology for evaluating diffusion coefficients and impedance measurements. Informative characterization techniques employed to assess new materials for batteries are also described, including operando XRD, pair-distribution function analysis, X-ray photoelectron spectroscopy, and operando X-ray absorption spectroscopy. Examples of insightful information that each technique has provided in the research areas of Li-S, Na-ion, and Mg batteries are presented along with excellent references for detailed descriptions of the theory, experimental procedures, and various designs, as well as methods for data processing and analysis.