二硫化钼制备工艺研究进展
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摘要
介绍了二硫化钼的基本性质及应用状况,综述了几种制备二硫化钼工艺的原理、优缺点、研究现状及未来的发展方向,指出多种工艺结合可以制备性能更优异的二硫化钼。
The basic properties and applications of molybdenum disulfide are briefly introduced.The principles,advantages and disadvantages,research status and future development direction of preparation processes for molybdenum disulfide are reviewed.It is pointed out that more excellent molybdenum disulfide can be prepared by combining a variety of processes.
The basic properties and applications of molybdenum disulfide are briefly introduced.The principles,advantages and disadvantages,research status and future development direction of preparation processes for molybdenum disulfide are reviewed.It is pointed out that more excellent molybdenum disulfide can be prepared by combining a variety of processes.
引文
[1]向铁根.钼冶金[M].长沙:中南大学出版社,2002.
[2]沃恒洲,胡坤宏,胡立明,等.纳米二硫化钼制备现状与发展[J].广东化工,2010,37(1):73-75.
[3]胡平,陈震宇,王快社,等.二维层状二硫化钼复合材料的研究进展及发展趋势[J].化工学报,2017,68(4):1286-1298.
[4]何江山,崔雅茹,李凯茂.纳米MoS2的制备与研究进展[J].湿法冶金,2012,31(5):274-277.
[5] Splendiani Andrea,SUN Liang,ZHANG Yuanbo,et al.Emerging photoluminescence in monolayer MoS2[J].Nano Letters,2010,10(4):1271-1275.
[6] MAK K F,HE Keliang,SHAN Jie,et al.Control of valley polarization in monolayer MoS2by optical helicity[J].Nature Nanotechnology,2012,7(8):494-498.
[7] YU Yifei,HUANG Shengyang,LI Yanpeng,et al.Layerdependent electrocatalysis of MoS2for hydrogen evolution[J].Nano Letters,2014,14(2):553-558.
[8] DING Shujiang,ZHANG Dongyang,CHEN Junsong,et al.Facile synthesis of hierarchical MoS2 microspheres composed of few-layered nanosheets and their lithium storage properties[J].Nanoscale,2012,4(1):95-98.
[9] LOO A H,BONANNI A,AMBROSI A,et al.Molybdenum disulfide(MoS2)nanoflakes as inherently electroactive labels for DNA hybridization detection[J].Nanoscale,2014,6(20):11971-11975.
[10] LIN T,ZHONG L,GUO L,et al.Seeing diabetes:visual detection of glucose based on the intrinsic peroxidase-like activity of MoS2nanosheets[J].Nanoscale,2014,6(20):11856-11862.
[11] LIU T,SHI S,LIANG C,et al.Iron oxide decorated MoS2nanosheets with double PEGylation for chelator-free radiolabeling and multimodal imaging guided photothermal therapy[J].ACS Nano,2015,9(1):950-60.
[12] CHANG Kun,CHEN Weixiang.Single-layer MoS/graphene dispersed in amorphous carbon:towards high electrochemical performances in rechargeable lithium ion batteries[J].Journal of Materials Chemistry,2011,21(43):17175-17184.
[13] XU X,FAN Z,DING S,et al.Fabrication of MoS2nanosheet@TiO2 nanotube hybrid nanostructures for lithium storage[J].Nanoscale,2014,6(10):5245-5250.
[14] DENG Z,HU Y,REN D,et al.Reciprocal hybridization of MoO2nanoparticles and few-layer MoS2for stable lithiumion batteries[J].Chemical Communications,2015,51(72):13838-13841.
[15] CAI Yu,YANG Xi,LIANG Tao,et al.Easy incorporation of single-walled carbon nanotubes into two-dimensional MoS2for high-performance hydrogen evolution[J].Nanotechnology,2014,25(46):465401-465406.
[16] MANNEBACH E M,DUERLOO K A N,PELLOUCHOUD L A,et al.Ultrafast electronic and structural response of monolayer MoS2under intense photoexcitation conditions[J].ACS Nano,2014,8(10):10734-10742.
[17] SHI Jianping,MA Donglin,HAN Gaofeng,et al.Controllable growth and transfer of monolayer MoS2on Au foils and its potential application in hydrogen evolution reaction[J].ACS Nano,2014,8(10):10196-10204.
[18]曾一,赵鹏,王跃峰,等.气相反应条件对合成高纯度富勒烯结构二硫化钼的影响[J].中国钨业,2008,23(1):42-44.
[19]吴晨,杨帆,张熠,等.银掺杂对MoS2薄膜特性的影响[J].微纳电子技术,2014,51(8):498-502.
[20] ZHAN Yongjie,LIU Zheng,NAJMAEI S,et al.Large-area vapor-phase growth and characterization of MoS2atomic layers on a SiO2substrate[J].Small,2012,8(7):966-971.
[21] ZAK A,FELDMAN Y,ALPEROVICH V,et al.Growth mechanism of MoS2fullerene-like nanoparticles by gasphase synthesis[J].Journal of The American Chemical Society,2000,122(45):11108-11116.
[22]张亨.纳米二硫化钼的制备及性质研究进展[J].中国钼业,2015,39(3):5-9.
[23]田野,何俣,朱永法,等.MoS2的水热合成及其润滑性能[J].物理化学学报,2003,19(11):1044-1048.
[24] LAVAYEN V,MIRABAL N,O’DWYER C,et al.The formation of nanotubes and nanocoils of molybdenum disulphide[J].Applied Surface Science,2007,253(12):5185-5190.
[25]李汗,李飞,蒋波,等.球中球结构二硫化钼的制备及其光催化性能研究[J].淮北师范大学学报(自然科学版),2016,37(4):52-55.
[26]邢相栋,兰新哲,周军,等.纳米二硫化钼制备过程中硫源及分散剂的研究[J].中国钼业,2008,32(3):40-42.
[27]何晓云,钟淮真,李国强,等.纳米MoS2的制备及其与聚吡咯物复合膜光学性能的研究[J].化学世界,2006,47(2):69-70.
[28]武继芬,傅洵,周晓东,等.萃取溶剂热法制备球形和棒状MOS2颗粒[J].稀有金属材料与工程,2007,36(2):91-94.
[29] AFANASIEV P,GEANTET C,THOMAZEAU C,et al.ChemInform abstract:molybdenum polysulfide hollow microtubules grown at room temperature from solution[J].Cheminform,2000,31(35):1001-1002.
[30]沃恒洲,胡献国,胡淑丽,等.均匀沉淀法制备纳米二硫化钼粉末的研究[J].合肥工业大学学报(自然科学版),2003,26(4):486-489.
[31]邹同征,涂江平,夏正志,等.聚乙二醇为分散剂的沉淀法制备IF-MoS2[J].无机化学学报,2005,21(8):1170-1174.
[32]胡献国,沃恒洲,胡坤宏,等.用硫化钠制备二硫化钼纳米颗粒[J].机械工程材料,2004,28(1):32-34.
[33] WANG J,LAUWERENS W,WIEERS E,et al.Structure and tribological properties of MoSxcoatings prepared by bipolar DC magnetron sputtering[J].Surface&Coatings Technology,2001,139(2):143-152.
[34]杨久流.高纯二硫化钼的制备工艺[J].有色金属(选矿部分),2000(5):19-23.
[35] EDA G,YAMAGUCHI H,VOIRY D,et al.Photoluminescence from chemically exfoliated MoS2[J].Nano Letters,2011,11(12):5111-5116.
[36]周克清.典型聚合物基二硫化钼纳米复合材料的制备及其热稳定性与燃烧性能研究[D].合肥:中国科学技术大学,2015.
[37]周丽春,吴伟端,赵煌.纳米二硫化钼的制备与表征[J].电子显微学报,2004,23(6):618-621.
[38] LIU Na,KIM P,KIM J H,et al.Large-area atomically thin MoS2nanosheets prepared using electrochemical exfoliation[J].ACS Nano,2014,8(7):6902-6910.
[39]花文文.纳米二硫化钼的制备修饰及其在复合材料中的应用[D].南京:南京大学,2015.
[40] ZHU Yingjie,WANG Weiwei,QI Ruijuan,et al.Microwave-assisted synthesis of single-crystalline tellurium nanorods and nanowires in ionic liquids[J].Angewandte Chemie,2004,43(11):1410-1414.
[41]赵潇璇,刘艳茹,董斌,等.纳米二硫化钼的化学法合成研究进展[J].材料导报,2013,27(23):60-65.
[2]沃恒洲,胡坤宏,胡立明,等.纳米二硫化钼制备现状与发展[J].广东化工,2010,37(1):73-75.
[3]胡平,陈震宇,王快社,等.二维层状二硫化钼复合材料的研究进展及发展趋势[J].化工学报,2017,68(4):1286-1298.
[4]何江山,崔雅茹,李凯茂.纳米MoS2的制备与研究进展[J].湿法冶金,2012,31(5):274-277.
[5] Splendiani Andrea,SUN Liang,ZHANG Yuanbo,et al.Emerging photoluminescence in monolayer MoS2[J].Nano Letters,2010,10(4):1271-1275.
[6] MAK K F,HE Keliang,SHAN Jie,et al.Control of valley polarization in monolayer MoS2by optical helicity[J].Nature Nanotechnology,2012,7(8):494-498.
[7] YU Yifei,HUANG Shengyang,LI Yanpeng,et al.Layerdependent electrocatalysis of MoS2for hydrogen evolution[J].Nano Letters,2014,14(2):553-558.
[8] DING Shujiang,ZHANG Dongyang,CHEN Junsong,et al.Facile synthesis of hierarchical MoS2 microspheres composed of few-layered nanosheets and their lithium storage properties[J].Nanoscale,2012,4(1):95-98.
[9] LOO A H,BONANNI A,AMBROSI A,et al.Molybdenum disulfide(MoS2)nanoflakes as inherently electroactive labels for DNA hybridization detection[J].Nanoscale,2014,6(20):11971-11975.
[10] LIN T,ZHONG L,GUO L,et al.Seeing diabetes:visual detection of glucose based on the intrinsic peroxidase-like activity of MoS2nanosheets[J].Nanoscale,2014,6(20):11856-11862.
[11] LIU T,SHI S,LIANG C,et al.Iron oxide decorated MoS2nanosheets with double PEGylation for chelator-free radiolabeling and multimodal imaging guided photothermal therapy[J].ACS Nano,2015,9(1):950-60.
[12] CHANG Kun,CHEN Weixiang.Single-layer MoS/graphene dispersed in amorphous carbon:towards high electrochemical performances in rechargeable lithium ion batteries[J].Journal of Materials Chemistry,2011,21(43):17175-17184.
[13] XU X,FAN Z,DING S,et al.Fabrication of MoS2nanosheet@TiO2 nanotube hybrid nanostructures for lithium storage[J].Nanoscale,2014,6(10):5245-5250.
[14] DENG Z,HU Y,REN D,et al.Reciprocal hybridization of MoO2nanoparticles and few-layer MoS2for stable lithiumion batteries[J].Chemical Communications,2015,51(72):13838-13841.
[15] CAI Yu,YANG Xi,LIANG Tao,et al.Easy incorporation of single-walled carbon nanotubes into two-dimensional MoS2for high-performance hydrogen evolution[J].Nanotechnology,2014,25(46):465401-465406.
[16] MANNEBACH E M,DUERLOO K A N,PELLOUCHOUD L A,et al.Ultrafast electronic and structural response of monolayer MoS2under intense photoexcitation conditions[J].ACS Nano,2014,8(10):10734-10742.
[17] SHI Jianping,MA Donglin,HAN Gaofeng,et al.Controllable growth and transfer of monolayer MoS2on Au foils and its potential application in hydrogen evolution reaction[J].ACS Nano,2014,8(10):10196-10204.
[18]曾一,赵鹏,王跃峰,等.气相反应条件对合成高纯度富勒烯结构二硫化钼的影响[J].中国钨业,2008,23(1):42-44.
[19]吴晨,杨帆,张熠,等.银掺杂对MoS2薄膜特性的影响[J].微纳电子技术,2014,51(8):498-502.
[20] ZHAN Yongjie,LIU Zheng,NAJMAEI S,et al.Large-area vapor-phase growth and characterization of MoS2atomic layers on a SiO2substrate[J].Small,2012,8(7):966-971.
[21] ZAK A,FELDMAN Y,ALPEROVICH V,et al.Growth mechanism of MoS2fullerene-like nanoparticles by gasphase synthesis[J].Journal of The American Chemical Society,2000,122(45):11108-11116.
[22]张亨.纳米二硫化钼的制备及性质研究进展[J].中国钼业,2015,39(3):5-9.
[23]田野,何俣,朱永法,等.MoS2的水热合成及其润滑性能[J].物理化学学报,2003,19(11):1044-1048.
[24] LAVAYEN V,MIRABAL N,O’DWYER C,et al.The formation of nanotubes and nanocoils of molybdenum disulphide[J].Applied Surface Science,2007,253(12):5185-5190.
[25]李汗,李飞,蒋波,等.球中球结构二硫化钼的制备及其光催化性能研究[J].淮北师范大学学报(自然科学版),2016,37(4):52-55.
[26]邢相栋,兰新哲,周军,等.纳米二硫化钼制备过程中硫源及分散剂的研究[J].中国钼业,2008,32(3):40-42.
[27]何晓云,钟淮真,李国强,等.纳米MoS2的制备及其与聚吡咯物复合膜光学性能的研究[J].化学世界,2006,47(2):69-70.
[28]武继芬,傅洵,周晓东,等.萃取溶剂热法制备球形和棒状MOS2颗粒[J].稀有金属材料与工程,2007,36(2):91-94.
[29] AFANASIEV P,GEANTET C,THOMAZEAU C,et al.ChemInform abstract:molybdenum polysulfide hollow microtubules grown at room temperature from solution[J].Cheminform,2000,31(35):1001-1002.
[30]沃恒洲,胡献国,胡淑丽,等.均匀沉淀法制备纳米二硫化钼粉末的研究[J].合肥工业大学学报(自然科学版),2003,26(4):486-489.
[31]邹同征,涂江平,夏正志,等.聚乙二醇为分散剂的沉淀法制备IF-MoS2[J].无机化学学报,2005,21(8):1170-1174.
[32]胡献国,沃恒洲,胡坤宏,等.用硫化钠制备二硫化钼纳米颗粒[J].机械工程材料,2004,28(1):32-34.
[33] WANG J,LAUWERENS W,WIEERS E,et al.Structure and tribological properties of MoSxcoatings prepared by bipolar DC magnetron sputtering[J].Surface&Coatings Technology,2001,139(2):143-152.
[34]杨久流.高纯二硫化钼的制备工艺[J].有色金属(选矿部分),2000(5):19-23.
[35] EDA G,YAMAGUCHI H,VOIRY D,et al.Photoluminescence from chemically exfoliated MoS2[J].Nano Letters,2011,11(12):5111-5116.
[36]周克清.典型聚合物基二硫化钼纳米复合材料的制备及其热稳定性与燃烧性能研究[D].合肥:中国科学技术大学,2015.
[37]周丽春,吴伟端,赵煌.纳米二硫化钼的制备与表征[J].电子显微学报,2004,23(6):618-621.
[38] LIU Na,KIM P,KIM J H,et al.Large-area atomically thin MoS2nanosheets prepared using electrochemical exfoliation[J].ACS Nano,2014,8(7):6902-6910.
[39]花文文.纳米二硫化钼的制备修饰及其在复合材料中的应用[D].南京:南京大学,2015.
[40] ZHU Yingjie,WANG Weiwei,QI Ruijuan,et al.Microwave-assisted synthesis of single-crystalline tellurium nanorods and nanowires in ionic liquids[J].Angewandte Chemie,2004,43(11):1410-1414.
[41]赵潇璇,刘艳茹,董斌,等.纳米二硫化钼的化学法合成研究进展[J].材料导报,2013,27(23):60-65.