电感耦合等离子体原子发射光谱法在金属材料分析应用技术方面的进展
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摘要
对近5年国内电感耦合等离子体原子发射光谱法(ICP-AES)在金属材料分析方面中样品溶解、样品富集分离和干扰等问题的应用进展进行了综述。发现ICP-AES在分析速度、准确度和应用范围等方面都得到大幅度的提升;样品前处理技术的改进,降低了ICP-AES对金属材料样品中痕量元素分析的测定下限,满足金属材料中个别元素质量分数在0.000 1%以下的测定要求;在实际应用中ICP-AES法可用于镀层材料、金属材料夹杂物及重金属溶出量的分析。
The progress in application of inductively coupled plasma atomic emission spectrometry(ICPAES)in analysis of metal materials in recent five years in China was reviewed.The sample dissolution,sample enrichment and separation as well as interference problems were discussed.It was found that the analysis speed,accuracy and application range of ICP-AES had been greatly improved.The improvement of sample pretreatment technology reduced the low limit of determination of trace elements in metal materials by ICP-AES.The determination requirements of low mass fraction(w<0.000 1%)of several elements could be satisfied.In actual application,ICP-AES could be used for the analysis of dissolving-out amount of coating materials,inclusions in metal material and heavy metals.
The progress in application of inductively coupled plasma atomic emission spectrometry(ICPAES)in analysis of metal materials in recent five years in China was reviewed.The sample dissolution,sample enrichment and separation as well as interference problems were discussed.It was found that the analysis speed,accuracy and application range of ICP-AES had been greatly improved.The improvement of sample pretreatment technology reduced the low limit of determination of trace elements in metal materials by ICP-AES.The determination requirements of low mass fraction(w<0.000 1%)of several elements could be satisfied.In actual application,ICP-AES could be used for the analysis of dissolving-out amount of coating materials,inclusions in metal material and heavy metals.
引文
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