直接进样技术在测定谷物中重金属中的应用
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摘要
对直接进样技术进行概括总结,着重对悬浮液直接进样技术、浸出液直接进样技术及固体直接进样技术的研究进展,技术难点以及在谷物中重金属检测中的实际应用情况等展开了具体的介绍与讨论,同时对其应用前景进行展望。
The mainly direct sampling techniques were summarized,including the suspension direct injection,the extracted solution direct injection and the solid direct injection.The research progress,technical difficulties,and the actual application of the direct injection techniques in detection of heavy metals in grain were specifically discussed.Meanwhile,the application of direct injection techniques was prospected.
The mainly direct sampling techniques were summarized,including the suspension direct injection,the extracted solution direct injection and the solid direct injection.The research progress,technical difficulties,and the actual application of the direct injection techniques in detection of heavy metals in grain were specifically discussed.Meanwhile,the application of direct injection techniques was prospected.
引文
[1]周明慧,伍燕湘,王松雪.国内外粮谷中元素含量检测标准现状与进展[J].中国农业科技导报,2013,15(4):25-30.
[2]吴少尉,吴青菊.电感耦合等离子体光/质谱中的进样技术[J].湖北民族学院学报(自然科学版),2009,27(4):427-433.
[3]YI Y Z,JIANG S J,SAHAYAM A C.Palladium nanoparticles as the modifier for the determination of Zn,As,Cd,Sb,Hg and Pb in biological samples by ultrasonic slurry sampling electrothermal vaporization inductively coupled plasma mass spectrometry[J].Journal of Analytical Atomic Spectrometry,2012,27(3):426-431.
[4]ARAUJO R G,OLESZCZUK N,RAMPAZZOA RT,et al.Comparison of direct solid sampling and slurry sampling for the determination of cadmium in wheat flour by electrothermal atomic absorption spectrometry[J].Talanta,2008,77(1):400-406.
[5]SAVIO M,CERUTTI S,MARTINEZ L D,SMI-CHOWSKI P,et al.Study of matrix effects and spectral interferences in the determination of lead in sediments,sludges and soils by SR-ETAAS using slurry sampling[J].Talanta,2010,82(2):523-527.
[6]KATAOKA H,OKAMOTO Y,TSUKAHARA S,et al.Separate vaporisation of boric acid and inorganic boron from tungsten sample cuvette-tungsten boat furnace followed by the detection of boron species by inductively coupled plasma mass spectrometry and atomic emission spectrometry(ICP-MS and ICP-AES)[J].Analytica Chimica Acta,2008,610(2):179-185.
[7]周明慧,王松雪,伍燕湘.稀酸温和提取直接进样石墨炉原子吸收法快速测定谷物中铅的含量研究[J].分析化学,2014,42(3):459-460.
[8]毛雪飞,刘霁欣,王敏,等.固体进样元素分析技术在农产品质量安全中的应用[J].中国农业科学,2013,46(16):3432-3443.
[9]TSENG Y J,LIU C C,JIANG S J.Slurry sampling electrothermal vaporization inductively coupled plasma mass spectrometry for the determination of As and Se in soil and sludge[J].Analytica Chimica Acta,2007,588(2):173-178.
[10]BELARRA M A,MARTINEZ-GARBAYO M P,ANZANO J M,et al.Graphite-furnace atomic absorption spectrometric method for direct determination of iron and zinc in solid rice samples[J].Analytical Sciences,1996,12(3):483-487.
[11]HUANG R J,ZHUANG Z X,TAI Y,et al.Direct analysis of mercury in traditional chinese medicines using thermolysis coupled with on-line atomic absorption spectrometry[J].Talanta,2006,68(3):728-734.
[12]BEZERRA M A,CASTRO J T,MACEDO R C,et al.Use of constrained mixture design for optimization of method for determination of zinc and manganese in tea leaves employing slurry sampling[J].Analytica Chimica Acta,2010,670(1/2):33-38.
[13]金晓艳,黄正杰.原子吸收法悬浮液直接进样测定鱼样中的铅[J].中国卫生检验杂志,2007,17(8):1442-1444.
[14]张洪波,徐佳,陈庆阳,等.悬浮进样-火焰原子吸收光谱法直接测定[J].光谱实验室,2011,28(4):2684-2686.
[15]WANG L,HU B,JIANG Z C,et al.Speciation of Cr(Ⅲ)and Cr(Ⅵ)in aqueous samples by coprecipitation/slurry sampling fluorination assisted graphite furnace atomic absorption spectrometry[J].International Journal of Environmental Analytical Chemistry,2002,82(6):387-393.
[16]邵坤,易建春,雷勇,等.悬浮液进样-基体改进石墨炉原子吸收法直接测定松香中微量砷[J].分析科学学报,2013,29(4):569-572.
[17]渠荣遴,何绯,王惠.对石墨管内锆图层作用的初探[J].理化检验-化学分册,1995,31(3):171-172.
[18]杨兴华,马仁乐.悬浮液进样-石墨炉原子吸收光谱法测定大米中铅的含量[J].怀化学院学报,2014,33(11):62-65.
[19]孙汉文,刘晓莉.悬浮进样-氢化物发生原子吸收法直接测定面粉中的微量砷[J].食品科学,2009,30(6):160-163.
[20]吴云钊,孟鹏,曹民,等.不完全消解-石墨炉原子吸收光谱法测定粮食中的铅和镉[J].中国卫生检疫杂志,2014,24(17):2464-2466.
[21]PENG Y,GUO W,ZHANG P,et al.Heated slurry sampling for determination of Cadmium in Food by electrothermal atomic absorption spectrometry[J].Analytical Letters,2015,48(18):2894-2907.
[22]ARISTIDIS N A,CONSTANTINA M,PASCHA-LIA B,et al.On-line micro-volume introduction system developed for lower density than water extraction solvent and dispersive liquid-liquid microextraction coupled with flame atomic absorption spectrometry[J].Analytica Chimica Acta,2012,733(13):34-37.
[23]赵桂生.酸提取技术在重金属迅速检测中应用分析[J].轻工科技,2012,5:135-136.
[24]赵尔敏,方勇,王明洋,等.ICP-MS直接进样对大米酶解液中痕量硒的测定[J].食品科学,2017,38(10):168-172.
[25]方勇,陈悦,鞠兴荣,等.微量直接进样-二元泵联用ICP-MS分析大米蛋白中痕量铅[J].分析实验室,2015,34(2):151-154.
[26]李芝薇.用于碳水化合物类农产品重金属ELISA检测的样品前处理研究[D].广州:暨南大学,2011.
[27]吴玉萍,王东丹,李琼珍,等.盐酸浸提-电感耦合等离子体发射光谱法测定烟草中的多元素[J].分析化学,2002,30(3):315-317.
[28]岳兵,刘丽萍,谢科,等.不同方法对大米中无机砷含量测定结果的影响[J].中国食品卫生杂志,2013,25(3):238-240.
[29]周明慧,王松雪,伍燕湘.稀酸温和提取直接进样快速测定大米中镉含量[J].中国粮油学报,2015,30(2):97-102.
[30]王松雪,周明慧,伍燕湘,等.一种从谷物中快速温和提取重金属的方法:ZL.2013 10595297.6[P].2016-04-20.
[31]汪素萍.直接固体进样石墨炉原子吸收分析技术在农产品检测中的应用[J].现代科学仪器,2006,16(1):39-41.
[32]ISAAC R A,KERBER J D.Atomic absorption and flame photometry:Techniques and uses in soil,plant,and water analysis[J].Instrumental Methods for Analysis of Soils and Plant Tissue,1971,34(34):17-37.
[33]GUO X Q,HE M,CHEN B B,et al.Phase transfer hollow fiber liquid phase microextraction combined with electrothermal vaporization inductively coupled plasma mass spectrometry for the determination of trace heavy metals in environmental and biological samples[J].Talanta,2012,101:516-523.
[34]SERVIN A D,CASTILLO-MICHEL H,HER-NANDEZ-VIEZCAS J A,et al.Synchrotron microXRF and micro-XANES confirmation of the uptake and translocation of TiO2 nanoparticles in cucumber(Cucumis sativus)plants[J].Environmental Science and Technology,2012,46(14):7637-7643.
[35]KUAR J,KUMAR A.Elemental analysis of different varieties of rice samples using XRF technique[C].AIP Conference Proceedings,2016,1728:020350.
[36]YADA S,KAWASAKI A,MATSUDA K,et al.Rapid and simple determination of cadmium concentrations in rice grain samples by using a new-energy dispersive X-ray fluorescence spectrometer(XRF)[J].Science of Soil&Manure Japan,2006,77:165-170.
[37]张辉,余正东,吴敏,等.ED-XRF法快速测定大米中镉元素的实用性分析[J].食品工业,2015,36(12):259-263.
[38]黄秋鑫,孙秀敏.粉末标准曲线XRF法检测土壤中的重金属[J].环境科学与技术,2014,37(9):92-98.
[39]张晓红,冯礼,路东,等.固体进样原子荧光用于测量农产品中的镉[J].现代科学仪器,2012(6):157-161.
[40]ARAUJO R G,OLESZCZUK N,RAMPAZZOA RT,et al.Comparison of direct solid sampling and slurry sampling for the determination of cadmium in wheat flour by electrothermal atomic absorption spectrometry[J].Talanta,2008,77(1):400-406.
[41]杨娟,陈建忠,杨清华,等.全自动测汞仪直接测定食品中总汞[J].中国卫生检验杂志,2016,26(6):782-788.
[42]GB 5009.12-2017食品安全国家标准食品中铅的测定[S].
[43]GB 5009.15-2014食品安全国家标准食品中镉的测定[S].
[44]GB 5009.11-2014食品安全国家标准食品中总砷及无机砷的测定[S].
[45]GB 5009.17-2014食品安全国家标准食品中总汞及有机汞的测定[S].
[46]GB 5009.123-2014食品安全国家标准食品中铬的测定[S].
[47]AOAC Official Method 972.25 Lead in food A-tomic absorption spectrophotometric method[S].
[48]AOAC Official Method 973.34 Cadmium in food Atomic absorption spectrophotometric method[S].
[49]EN ISO 15774-2012 Animal and vegetable fats and oils.Determination of cadmium content by direct graphite furnace atomic absorption spectrometry[S].
[50]ISO 8294-1999 Animal and vegatable fats and oils-Determination of copper,iron and nickel contents-Graphite furnace atomic absorption method[S].
[51]ISO 27085-2009 Animal feeding stuffs-Determination of calcium,sodium,phosphorus,magnesium,potassium,iron,zinc,copper,manganese,cobalt,molybdenum,arsenic,lead and cadmium by ICP-AES[S].
[52]AOAC Official Method 999.10 Lead,cadmium,zinc,copper,and iron in foods Atomic absorption sepctrophotometry after microwave digestion[S].
[2]吴少尉,吴青菊.电感耦合等离子体光/质谱中的进样技术[J].湖北民族学院学报(自然科学版),2009,27(4):427-433.
[3]YI Y Z,JIANG S J,SAHAYAM A C.Palladium nanoparticles as the modifier for the determination of Zn,As,Cd,Sb,Hg and Pb in biological samples by ultrasonic slurry sampling electrothermal vaporization inductively coupled plasma mass spectrometry[J].Journal of Analytical Atomic Spectrometry,2012,27(3):426-431.
[4]ARAUJO R G,OLESZCZUK N,RAMPAZZOA RT,et al.Comparison of direct solid sampling and slurry sampling for the determination of cadmium in wheat flour by electrothermal atomic absorption spectrometry[J].Talanta,2008,77(1):400-406.
[5]SAVIO M,CERUTTI S,MARTINEZ L D,SMI-CHOWSKI P,et al.Study of matrix effects and spectral interferences in the determination of lead in sediments,sludges and soils by SR-ETAAS using slurry sampling[J].Talanta,2010,82(2):523-527.
[6]KATAOKA H,OKAMOTO Y,TSUKAHARA S,et al.Separate vaporisation of boric acid and inorganic boron from tungsten sample cuvette-tungsten boat furnace followed by the detection of boron species by inductively coupled plasma mass spectrometry and atomic emission spectrometry(ICP-MS and ICP-AES)[J].Analytica Chimica Acta,2008,610(2):179-185.
[7]周明慧,王松雪,伍燕湘.稀酸温和提取直接进样石墨炉原子吸收法快速测定谷物中铅的含量研究[J].分析化学,2014,42(3):459-460.
[8]毛雪飞,刘霁欣,王敏,等.固体进样元素分析技术在农产品质量安全中的应用[J].中国农业科学,2013,46(16):3432-3443.
[9]TSENG Y J,LIU C C,JIANG S J.Slurry sampling electrothermal vaporization inductively coupled plasma mass spectrometry for the determination of As and Se in soil and sludge[J].Analytica Chimica Acta,2007,588(2):173-178.
[10]BELARRA M A,MARTINEZ-GARBAYO M P,ANZANO J M,et al.Graphite-furnace atomic absorption spectrometric method for direct determination of iron and zinc in solid rice samples[J].Analytical Sciences,1996,12(3):483-487.
[11]HUANG R J,ZHUANG Z X,TAI Y,et al.Direct analysis of mercury in traditional chinese medicines using thermolysis coupled with on-line atomic absorption spectrometry[J].Talanta,2006,68(3):728-734.
[12]BEZERRA M A,CASTRO J T,MACEDO R C,et al.Use of constrained mixture design for optimization of method for determination of zinc and manganese in tea leaves employing slurry sampling[J].Analytica Chimica Acta,2010,670(1/2):33-38.
[13]金晓艳,黄正杰.原子吸收法悬浮液直接进样测定鱼样中的铅[J].中国卫生检验杂志,2007,17(8):1442-1444.
[14]张洪波,徐佳,陈庆阳,等.悬浮进样-火焰原子吸收光谱法直接测定[J].光谱实验室,2011,28(4):2684-2686.
[15]WANG L,HU B,JIANG Z C,et al.Speciation of Cr(Ⅲ)and Cr(Ⅵ)in aqueous samples by coprecipitation/slurry sampling fluorination assisted graphite furnace atomic absorption spectrometry[J].International Journal of Environmental Analytical Chemistry,2002,82(6):387-393.
[16]邵坤,易建春,雷勇,等.悬浮液进样-基体改进石墨炉原子吸收法直接测定松香中微量砷[J].分析科学学报,2013,29(4):569-572.
[17]渠荣遴,何绯,王惠.对石墨管内锆图层作用的初探[J].理化检验-化学分册,1995,31(3):171-172.
[18]杨兴华,马仁乐.悬浮液进样-石墨炉原子吸收光谱法测定大米中铅的含量[J].怀化学院学报,2014,33(11):62-65.
[19]孙汉文,刘晓莉.悬浮进样-氢化物发生原子吸收法直接测定面粉中的微量砷[J].食品科学,2009,30(6):160-163.
[20]吴云钊,孟鹏,曹民,等.不完全消解-石墨炉原子吸收光谱法测定粮食中的铅和镉[J].中国卫生检疫杂志,2014,24(17):2464-2466.
[21]PENG Y,GUO W,ZHANG P,et al.Heated slurry sampling for determination of Cadmium in Food by electrothermal atomic absorption spectrometry[J].Analytical Letters,2015,48(18):2894-2907.
[22]ARISTIDIS N A,CONSTANTINA M,PASCHA-LIA B,et al.On-line micro-volume introduction system developed for lower density than water extraction solvent and dispersive liquid-liquid microextraction coupled with flame atomic absorption spectrometry[J].Analytica Chimica Acta,2012,733(13):34-37.
[23]赵桂生.酸提取技术在重金属迅速检测中应用分析[J].轻工科技,2012,5:135-136.
[24]赵尔敏,方勇,王明洋,等.ICP-MS直接进样对大米酶解液中痕量硒的测定[J].食品科学,2017,38(10):168-172.
[25]方勇,陈悦,鞠兴荣,等.微量直接进样-二元泵联用ICP-MS分析大米蛋白中痕量铅[J].分析实验室,2015,34(2):151-154.
[26]李芝薇.用于碳水化合物类农产品重金属ELISA检测的样品前处理研究[D].广州:暨南大学,2011.
[27]吴玉萍,王东丹,李琼珍,等.盐酸浸提-电感耦合等离子体发射光谱法测定烟草中的多元素[J].分析化学,2002,30(3):315-317.
[28]岳兵,刘丽萍,谢科,等.不同方法对大米中无机砷含量测定结果的影响[J].中国食品卫生杂志,2013,25(3):238-240.
[29]周明慧,王松雪,伍燕湘.稀酸温和提取直接进样快速测定大米中镉含量[J].中国粮油学报,2015,30(2):97-102.
[30]王松雪,周明慧,伍燕湘,等.一种从谷物中快速温和提取重金属的方法:ZL.2013 10595297.6[P].2016-04-20.
[31]汪素萍.直接固体进样石墨炉原子吸收分析技术在农产品检测中的应用[J].现代科学仪器,2006,16(1):39-41.
[32]ISAAC R A,KERBER J D.Atomic absorption and flame photometry:Techniques and uses in soil,plant,and water analysis[J].Instrumental Methods for Analysis of Soils and Plant Tissue,1971,34(34):17-37.
[33]GUO X Q,HE M,CHEN B B,et al.Phase transfer hollow fiber liquid phase microextraction combined with electrothermal vaporization inductively coupled plasma mass spectrometry for the determination of trace heavy metals in environmental and biological samples[J].Talanta,2012,101:516-523.
[34]SERVIN A D,CASTILLO-MICHEL H,HER-NANDEZ-VIEZCAS J A,et al.Synchrotron microXRF and micro-XANES confirmation of the uptake and translocation of TiO2 nanoparticles in cucumber(Cucumis sativus)plants[J].Environmental Science and Technology,2012,46(14):7637-7643.
[35]KUAR J,KUMAR A.Elemental analysis of different varieties of rice samples using XRF technique[C].AIP Conference Proceedings,2016,1728:020350.
[36]YADA S,KAWASAKI A,MATSUDA K,et al.Rapid and simple determination of cadmium concentrations in rice grain samples by using a new-energy dispersive X-ray fluorescence spectrometer(XRF)[J].Science of Soil&Manure Japan,2006,77:165-170.
[37]张辉,余正东,吴敏,等.ED-XRF法快速测定大米中镉元素的实用性分析[J].食品工业,2015,36(12):259-263.
[38]黄秋鑫,孙秀敏.粉末标准曲线XRF法检测土壤中的重金属[J].环境科学与技术,2014,37(9):92-98.
[39]张晓红,冯礼,路东,等.固体进样原子荧光用于测量农产品中的镉[J].现代科学仪器,2012(6):157-161.
[40]ARAUJO R G,OLESZCZUK N,RAMPAZZOA RT,et al.Comparison of direct solid sampling and slurry sampling for the determination of cadmium in wheat flour by electrothermal atomic absorption spectrometry[J].Talanta,2008,77(1):400-406.
[41]杨娟,陈建忠,杨清华,等.全自动测汞仪直接测定食品中总汞[J].中国卫生检验杂志,2016,26(6):782-788.
[42]GB 5009.12-2017食品安全国家标准食品中铅的测定[S].
[43]GB 5009.15-2014食品安全国家标准食品中镉的测定[S].
[44]GB 5009.11-2014食品安全国家标准食品中总砷及无机砷的测定[S].
[45]GB 5009.17-2014食品安全国家标准食品中总汞及有机汞的测定[S].
[46]GB 5009.123-2014食品安全国家标准食品中铬的测定[S].
[47]AOAC Official Method 972.25 Lead in food A-tomic absorption spectrophotometric method[S].
[48]AOAC Official Method 973.34 Cadmium in food Atomic absorption spectrophotometric method[S].
[49]EN ISO 15774-2012 Animal and vegetable fats and oils.Determination of cadmium content by direct graphite furnace atomic absorption spectrometry[S].
[50]ISO 8294-1999 Animal and vegatable fats and oils-Determination of copper,iron and nickel contents-Graphite furnace atomic absorption method[S].
[51]ISO 27085-2009 Animal feeding stuffs-Determination of calcium,sodium,phosphorus,magnesium,potassium,iron,zinc,copper,manganese,cobalt,molybdenum,arsenic,lead and cadmium by ICP-AES[S].
[52]AOAC Official Method 999.10 Lead,cadmium,zinc,copper,and iron in foods Atomic absorption sepctrophotometry after microwave digestion[S].
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