高分辨连续光源原子吸收光谱仪的改造及功能拓展
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摘要
以高分辨连续光源原子吸收光谱仪为基础,通过对仪器硬件系统的改造、相关附件的安装以及软件的升级更新,实现砷、汞等重金属元素,铝、钛、锡等高温元素以及高盐样品的准确测定,从而实现了仪器的升级改造及功能拓展,应用范围得到提升,为研究工作提供更全面的无机元素分析.
Based on the high resolution continuous light source atomic absorption spectrometer,the accurate determination of heavy metals such as arsenic,mercury,high temperature elements such as aluminium,titanium,tin and high salt samples can be realized through the modification of the hardware system,the installation of relevant accessories and the upgrading of software. Thus,the expansion of the functions of the instrument and the promotion of its application scope can be realized,and a more comprehensive analysis of inorganic elements can be provided for the relevant research work.
Based on the high resolution continuous light source atomic absorption spectrometer,the accurate determination of heavy metals such as arsenic,mercury,high temperature elements such as aluminium,titanium,tin and high salt samples can be realized through the modification of the hardware system,the installation of relevant accessories and the upgrading of software. Thus,the expansion of the functions of the instrument and the promotion of its application scope can be realized,and a more comprehensive analysis of inorganic elements can be provided for the relevant research work.
引文
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[9]胡玥,丁玉竹,高旭东,等.微波消解-高分辨连续光源原子吸收光谱法测定锁阳和韭菜籽中的重金属元素含量[J].分析技术测试与仪器,2016,22(2):90-95.[HU Yue,DING Yu-zhu,GAO Xu-dong,et al.Determination of heavy metals in Cynomorium songaricum and Chinese chive seeds by microwave digestion-high resolution continuous light source atomic absorption spectrometry[J].Analytical Techniques and Instruments,2016,22(2):90-95.]
[10]杨惟慎,林励吾.负载型铂锡催化剂的研究进展[J].石油化工,1993,22(5):347-351.[YANG Wei-shen,LIN Li-wu.Progress in supported platinum-tin catalysts[J].Petrochemical,1993,22(5):347-351.]
[11]辛仁轩,王建强.镍电解液中主要成分和微量成分的ICP-AES测定[J].光谱实验室,1996,13(6):4-6.[XIN Ren-xuan,WANG Jian-qiang.ICP-AESdetermination of major and trace components in nickel electrolyte[J].Spectrum Laboratory,1996,13(6):4-6.]
[2]孙博思,任婷,赵丽娇,等.浊点萃取-高分辨连续光源石墨炉原子吸收光谱法测定环境水样中的痕量铅[J].光谱学与光谱分析,2012,32(10):2847-2852.[SUN Bo-si,REN Ting,ZHAO Li-jiao,et al.Cloud point extraction-high resolution continuous light source graphite furnace atomic absorption spectrometry for the determination of trace lead in environmental water samples[J].Spectroscopy and Spectral Analysis,2012,32(10):2847-2852.]
[3]任婷,赵丽娇,钟儒刚.高分辨连续光源石墨炉原子吸收光谱法测定面制食品中的铝[J].光谱学与光谱分析,2011,31(12):3388-3391.[REN Ting,ZHAO Li-jiao,ZHONG Ru-gang.Determination of aluminum in noodle food by high resolution continuous light source graphite furnace atomic absorption spectrometry[J].Spectroscopy and Spectral Analysis,2011,31(12):3388-3391.]
[4]邓勃.应用原子吸收与原子荧光光谱分析(第二版)[M].北京:化学工业出版社,2007.[DENG Bo.Applied atomic absorption spectrometry and atomic fluorescence spectrometry(second ddition)[M].Beijing:Chemical Industry Press,2007.]
[5]李华昌,高介平,符斌.ATC006原子吸收光谱分析技术[M].北京:中国质检出版社,2011.[LI Huachang,GAO Ji-eping,FU Bin.ATC006 atomic absorption spectrometry[M].Beijing:China Quality Detection Edition,2011.]
[6]马旻,柴昌信,祝建国.氢化物发生-原子荧光光谱法的干扰及其消除[J].分析测试技术与仪器,2011,17(3):179-182.[MA Min,CHAI Changxin,ZHU Jian-guo.Hydride generation-atomic fluorescence spectrometry interference and its elimination[J].Analytical Testing Techniques and Instruments,2011,17(3):179-182.]
[7]张丽.氢化物原子吸收法与氢化物原子荧光法测定饮用水中砷的方法比较[J].广东微量元素科学,2013,20(8):10-13.[ZHANG Li.Comparison of hydride atomic absorption spectrometry and hydride atomic fluorescence spectrometry for the determination of arsenic in drinking water[J].Guangdong Trace Elements Science,2013,20(8):10-13.]
[8]郭石,许启泰,陈东升.15种中成药中有害重金属铅、镉、铜含量的测定[J].广东微量元素科学,2011,18(5):59-62.[GUO Shi,XU Qi-tai,CHENDong-sheng.Determination of harmful heavy metals such as lead,cadmium and copper in 15 kinds of Chinese patent medicines[J].Guangdong Trace Elements Science,2011,18(5):59-62.]
[9]胡玥,丁玉竹,高旭东,等.微波消解-高分辨连续光源原子吸收光谱法测定锁阳和韭菜籽中的重金属元素含量[J].分析技术测试与仪器,2016,22(2):90-95.[HU Yue,DING Yu-zhu,GAO Xu-dong,et al.Determination of heavy metals in Cynomorium songaricum and Chinese chive seeds by microwave digestion-high resolution continuous light source atomic absorption spectrometry[J].Analytical Techniques and Instruments,2016,22(2):90-95.]
[10]杨惟慎,林励吾.负载型铂锡催化剂的研究进展[J].石油化工,1993,22(5):347-351.[YANG Wei-shen,LIN Li-wu.Progress in supported platinum-tin catalysts[J].Petrochemical,1993,22(5):347-351.]
[11]辛仁轩,王建强.镍电解液中主要成分和微量成分的ICP-AES测定[J].光谱实验室,1996,13(6):4-6.[XIN Ren-xuan,WANG Jian-qiang.ICP-AESdetermination of major and trace components in nickel electrolyte[J].Spectrum Laboratory,1996,13(6):4-6.]