废弃红砖微粉填料制备环保乳胶漆及其性能研究
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摘要
研究了利用废弃红砖生产环保乳胶漆的制备方法,通过正交试验分析了乳液种类、乳液含量、醇酯十二含量、丙二醇含量和增稠剂含量对环保乳胶漆性能的影响.结果表明,废弃红砖微粉与苯丙乳液有较好的相容性,当乳液含量为25%～30%,醇酯十二0.4%～1.2%,丙二醇3.00%～3.75%,增稠剂1‰～1.5‰时,砖质环保乳胶漆产品低温稳定性良好,可成完全悬浮状态,表干时间小于30min,摆杆阻尼次数可达103次,附着力等级大于5,这为建筑废物资源化提供新的途径.
In this paper, the preparation of environmentally friendly latex paint with red brick waste was investigated. Effects ofemulsion type, and the dosages of emulsion, coalescent, propylene glycol and thickener were studied in detail. It was indicated thatred brick waste powder had a good compatibility with styrene acrylic emulsion. The environmentally friendly latex paint wascompletely suspended and had an excellent low temperature stability under the optimum condition, which was the dosages of emulsion, coalescent, propylene glycol and thickener were 25%～30%, 0.4%～1.2%, 3.00%～3.75% and 1.0‰～1.5‰, respectively. Inaddition, under the optimum condition, the drying time, damped pendulum rod time and adhesion level were less than 30 min, 103 andmore than 5, respectively. All of the promising results manifested that the environmentally friendly latex paint was a potentialresource and provided a new platform for reusing construction waste.
In this paper, the preparation of environmentally friendly latex paint with red brick waste was investigated. Effects ofemulsion type, and the dosages of emulsion, coalescent, propylene glycol and thickener were studied in detail. It was indicated thatred brick waste powder had a good compatibility with styrene acrylic emulsion. The environmentally friendly latex paint wascompletely suspended and had an excellent low temperature stability under the optimum condition, which was the dosages of emulsion, coalescent, propylene glycol and thickener were 25%～30%, 0.4%～1.2%, 3.00%～3.75% and 1.0‰～1.5‰, respectively. Inaddition, under the optimum condition, the drying time, damped pendulum rod time and adhesion level were less than 30 min, 103 andmore than 5, respectively. All of the promising results manifested that the environmentally friendly latex paint was a potentialresource and provided a new platform for reusing construction waste.
引文
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[6]王竞妍.再生骨料缺陷对再生混凝土耐久性的影响[D].北京:北京交通大学,2013.Wang Jinyan.Influence of Recycled Aggregate Defects on the Durability of Recycled Aggregate Concrete[D].Beijing:Beijing Jiaotong University,2013.
[7]李婷.再生骨料缺陷对再生混凝土力学性能影响的研究[D].北京:北京交通大学,2013.Li Ting.Influence of Recycled Aggregate Defects on the Mechanical Properties of Recycled Aggregate Concrete[D].Beijing:Beijing Jiaotong University,2013.
[8]Pérez I,Pasandín A R,Medina L.Hot mix asphalt using C&D waste as coarse aggregates[J].Materials&Design,2012,(36):840-846.
[9]Pasandín A R,Pérez I.Laboratory evaluation of hot-mix asphalt containing construction and demolition waste[J].Construction&Building Materials,2014,52(2):284-293.
[10]Fallah Fatemeh,Khorasani Manouchehr,Ebrahimi Morteza.Improving the mechanical properties of waterborne nitrocellulose coating using nano-silica particles[J].Process in Organic Coatings,2017,(109):110-116.
[11]王杰,闫小星,王粲,等.碳酸钙和硅烷偶联剂协同改性对水性涂料性能的影响[J].科技创新与应用,2017,(24):27-28.Wang Jie,Yan Xiaoxing,Wang Can,ct al.Effect of Co-modification of Calcium Carbonate and Silane Coupling Agent on Performance of Waterborne Coatings[J].Scientific Technological Innovation and Application,2017,(24):27-28.
[12]黄志雄,马波,石敏先,等.滑石粉/苯丙乳液水性阻尼涂料的制备与研究[J].武汉理工大学学报,2016,38(8):7-12.Huang Zhixiong,Ma Bo,Shi Minxian,ct al.Talcum/Styrene-acrylate Emulsion Prepared Aqueous Damping Coatings and Its Study[J].Journal of Wuhan University of Technology,2016,38(8):7-12.
[13]熊绍泊.经济型耐洗刷乳胶漆及除醛耐洗刷乳胶漆的开发和性能研究[D].广州:华南理工大学,2016.Xiong Shaobo.Study on the Development and Performance of the Economical Scrub Resistant Latex Paint and Formaldehyde-removing Scrub Resistant Latex Paint[D].Guangzhou:South China University of Technology,2016.
[14]胡钊,类成林,杨涛.填料对水性阻尼涂料性能的影响[J].涂料工业,2012,42(6):52-54+59.Hu Zhao,Lei Chenglin,Yang Tao.Influence of Fillers on Aqueous Damping Coating[J].Paint&Coatings Industry,2012,42(6):52-54+59.
[15]雷敏娟.玻璃体复合水性锌铝涂层的制备及组织和耐蚀性能的研究[D].广州:广东工业大学,2012.Lei Minjuan.Study on preparation and Organization structure and corrosion resistance performance of glass composite water-based zinc-aluminum coating[D].Guangzhou:Guangdong Unibersity of Technology,2012.
[16]Zedan Sayieda R,Mohamed Maha R,Ahmed Doaa A,ct al.Effect of demolition/construction wastes on the properties of alkali activated slag cement[J].HBRC Journal,2015,13(3):331-336.
[17]陈建,马鸿文,蒋周青,等.高铝粉煤灰提铝硅钙渣制备硅灰石微晶玻璃研究[J].硅酸盐通报,2016,35(9):2898-2903.Chen Jian,Ma Hongwen,Jiang Zhouqing,ct al.Preparation of Wollastonite Glass-ceramics by Using Silicate-calcium Slag Generated in Process of Extracting Alumina from High-alumina Fly Ash[J].Bulletin of The Chinese Ceramic Society,2016,35(9):2898-2903.
[18]高章韵.工业副产石膏资源化处理及用于干粉涂料制备的研究[D].长沙:湖南大学,2010.Gao Zhangyun.Utilization of Industrial by-product Gypsumand and its application in architecture powder coating[D].Changsha:Hunan University,2010.
[19]Zheng Keren,Chen Lou,Gbozee Mulbah.Thermal stability of geopolymers used as supporting materials for Ti O2 film coating through sol-gel process:Feasibility and improvement[J].Construction and Building Materials,2016,(125):1114-1126.
[20]Song Huiping,Liu Jianqiang,Xue Fangbin,ct al.The application of ultra-fine fly ash in the seal coating for the wall of underground coal mine[J].Advanced Powder Technology,2016,27(4):1645-1650.
[21]Yew M C,Ramli Sulong N H,Yew M K,ct al.Eggshells:A novel bio-filler for intumescent flame-retardant coatings[J].Progress in Organic Coatings,2015,(81):116-124.
[22]Yew M C,Ramli Sulong N H,Yew M K,ct al.The formulation and study of the thermal stability and mechanical properties of an acrylic coating using chicken eggshell as a novel bio-filler[J].Progress in Organic Coatings,2013,(76):1549-1555.
[23]Dong Jin Kang,Kaushik Pal,Se Jeong Park,ct al.Effect of eggshell and silk fibroin on styrene-ethylene/butylene-styrene as bio-filler[J].Materials and Design,2009,31(4):2216-2219.
[24]张雯文.废黏土砖在铝硅系不定形耐火材料中的利用[C]//河北省冶金学会.2013钢铁用耐火材料生产、研发和应用技术交流会论文集.2013:3.Zhang Wenwen.Utilization of Waste Clay Bricks in Amorphous Refractories of Aluminum-Silicon System[C]//Proceedings of 2013Symposium on Technology Exchange of Production,Research and Development and Application of Refractories for Iron and Steel.
[25]王立旺.水泥窑用硅莫砖回收料制备喷涂料的研究与应用[C]//2015耐火材料综合学术年会(第十三届全国不定形耐火材料学术会议和2015耐火原料学术交流会)论文集(3)Wang Liwang.Research and Application of Spraying Coatings Prepared from Silicon Mould Brick Recycling Material Used in Cement Kiln[C]//Proceedings of 2015 Annual Conference on Refractories.
[26]GB/T 1727-1992漆膜一般制备法[S].GB/T 1727-1992 General preparation of paint film[S].
[27]GB/T 1723-1993涂料粘度测定法[S].GB/T 1723-1993Determination of viscosity of coatings[S].
[28]GB/T 9268-2008乳胶漆耐冻融性的测定[S].GB/T 9268-2008 Determination of freeze-thaw resistance of latex and emulsion paints[S].
[29]GB/T 1728-1979漆膜、腻子膜干燥时间测定法[S].GB/T 1728-1979 Methods of test for drying time of coatings of paints and putties[S].
[30]GB/T 1720-1979漆膜附着力测定法[S].GB/T 1720-1979 Method of test for adhesion of paint films[S].
[31]GB/T 1730-2007色漆和清漆摆杆阻尼试验[S].GB/T 1730-2007 Paints and varnishes-Pendulum damping test[S].
[2]战立伟,张玉玲.分析建筑固体废物污染的资源化处理[J].资源节约与环保,2016,(1):93.Zhan Liwei,Zhang Yuling.Analysis of Resource-based Treatment of Construction Solid Waste Pollution[J].Resources Economization&Environment Protection,2016,(1):93.
[3]谢田,高小峰,黄晟,等.重金属建筑废物中污染物随酸雨的迁移研究[J].山东化工,2015,44(6):157-160+164.Xie Tian,Gao Xiaofeng,Huang Sheng,ct al.Pollution Transformation of Heavy Metal Polluted CDW in Acid Rain[J].Shandong Chemical Industry,2015,44(6):157-160+164.
[4]冷发光,何更新,张仁瑜,等.国内外建筑垃圾资源化现状及发展趋势[J].环境卫生工程,2009,17(1):33-35.Leng Faguang,He Gengxin,Zhang Renyu,et al.Status and Development Trend of Construction Waste Resource at Home and Abroad[J].Environmental Sanitation Engineering,2009,17(1):33-35.
[5]孙丽蕊.再生微粉材性及其对再生制品影响的研究[D].北京:北京建筑工程学院,2012.Sun Lirui.Research on properties of recycled fine powder and its effects to recycled products[D].Beijing:Beijing Institute of Civil Engineering and Architecture,2012.
[6]王竞妍.再生骨料缺陷对再生混凝土耐久性的影响[D].北京:北京交通大学,2013.Wang Jinyan.Influence of Recycled Aggregate Defects on the Durability of Recycled Aggregate Concrete[D].Beijing:Beijing Jiaotong University,2013.
[7]李婷.再生骨料缺陷对再生混凝土力学性能影响的研究[D].北京:北京交通大学,2013.Li Ting.Influence of Recycled Aggregate Defects on the Mechanical Properties of Recycled Aggregate Concrete[D].Beijing:Beijing Jiaotong University,2013.
[8]Pérez I,Pasandín A R,Medina L.Hot mix asphalt using C&D waste as coarse aggregates[J].Materials&Design,2012,(36):840-846.
[9]Pasandín A R,Pérez I.Laboratory evaluation of hot-mix asphalt containing construction and demolition waste[J].Construction&Building Materials,2014,52(2):284-293.
[10]Fallah Fatemeh,Khorasani Manouchehr,Ebrahimi Morteza.Improving the mechanical properties of waterborne nitrocellulose coating using nano-silica particles[J].Process in Organic Coatings,2017,(109):110-116.
[11]王杰,闫小星,王粲,等.碳酸钙和硅烷偶联剂协同改性对水性涂料性能的影响[J].科技创新与应用,2017,(24):27-28.Wang Jie,Yan Xiaoxing,Wang Can,ct al.Effect of Co-modification of Calcium Carbonate and Silane Coupling Agent on Performance of Waterborne Coatings[J].Scientific Technological Innovation and Application,2017,(24):27-28.
[12]黄志雄,马波,石敏先,等.滑石粉/苯丙乳液水性阻尼涂料的制备与研究[J].武汉理工大学学报,2016,38(8):7-12.Huang Zhixiong,Ma Bo,Shi Minxian,ct al.Talcum/Styrene-acrylate Emulsion Prepared Aqueous Damping Coatings and Its Study[J].Journal of Wuhan University of Technology,2016,38(8):7-12.
[13]熊绍泊.经济型耐洗刷乳胶漆及除醛耐洗刷乳胶漆的开发和性能研究[D].广州:华南理工大学,2016.Xiong Shaobo.Study on the Development and Performance of the Economical Scrub Resistant Latex Paint and Formaldehyde-removing Scrub Resistant Latex Paint[D].Guangzhou:South China University of Technology,2016.
[14]胡钊,类成林,杨涛.填料对水性阻尼涂料性能的影响[J].涂料工业,2012,42(6):52-54+59.Hu Zhao,Lei Chenglin,Yang Tao.Influence of Fillers on Aqueous Damping Coating[J].Paint&Coatings Industry,2012,42(6):52-54+59.
[15]雷敏娟.玻璃体复合水性锌铝涂层的制备及组织和耐蚀性能的研究[D].广州:广东工业大学,2012.Lei Minjuan.Study on preparation and Organization structure and corrosion resistance performance of glass composite water-based zinc-aluminum coating[D].Guangzhou:Guangdong Unibersity of Technology,2012.
[16]Zedan Sayieda R,Mohamed Maha R,Ahmed Doaa A,ct al.Effect of demolition/construction wastes on the properties of alkali activated slag cement[J].HBRC Journal,2015,13(3):331-336.
[17]陈建,马鸿文,蒋周青,等.高铝粉煤灰提铝硅钙渣制备硅灰石微晶玻璃研究[J].硅酸盐通报,2016,35(9):2898-2903.Chen Jian,Ma Hongwen,Jiang Zhouqing,ct al.Preparation of Wollastonite Glass-ceramics by Using Silicate-calcium Slag Generated in Process of Extracting Alumina from High-alumina Fly Ash[J].Bulletin of The Chinese Ceramic Society,2016,35(9):2898-2903.
[18]高章韵.工业副产石膏资源化处理及用于干粉涂料制备的研究[D].长沙:湖南大学,2010.Gao Zhangyun.Utilization of Industrial by-product Gypsumand and its application in architecture powder coating[D].Changsha:Hunan University,2010.
[19]Zheng Keren,Chen Lou,Gbozee Mulbah.Thermal stability of geopolymers used as supporting materials for Ti O2 film coating through sol-gel process:Feasibility and improvement[J].Construction and Building Materials,2016,(125):1114-1126.
[20]Song Huiping,Liu Jianqiang,Xue Fangbin,ct al.The application of ultra-fine fly ash in the seal coating for the wall of underground coal mine[J].Advanced Powder Technology,2016,27(4):1645-1650.
[21]Yew M C,Ramli Sulong N H,Yew M K,ct al.Eggshells:A novel bio-filler for intumescent flame-retardant coatings[J].Progress in Organic Coatings,2015,(81):116-124.
[22]Yew M C,Ramli Sulong N H,Yew M K,ct al.The formulation and study of the thermal stability and mechanical properties of an acrylic coating using chicken eggshell as a novel bio-filler[J].Progress in Organic Coatings,2013,(76):1549-1555.
[23]Dong Jin Kang,Kaushik Pal,Se Jeong Park,ct al.Effect of eggshell and silk fibroin on styrene-ethylene/butylene-styrene as bio-filler[J].Materials and Design,2009,31(4):2216-2219.
[24]张雯文.废黏土砖在铝硅系不定形耐火材料中的利用[C]//河北省冶金学会.2013钢铁用耐火材料生产、研发和应用技术交流会论文集.2013:3.Zhang Wenwen.Utilization of Waste Clay Bricks in Amorphous Refractories of Aluminum-Silicon System[C]//Proceedings of 2013Symposium on Technology Exchange of Production,Research and Development and Application of Refractories for Iron and Steel.
[25]王立旺.水泥窑用硅莫砖回收料制备喷涂料的研究与应用[C]//2015耐火材料综合学术年会(第十三届全国不定形耐火材料学术会议和2015耐火原料学术交流会)论文集(3)Wang Liwang.Research and Application of Spraying Coatings Prepared from Silicon Mould Brick Recycling Material Used in Cement Kiln[C]//Proceedings of 2015 Annual Conference on Refractories.
[26]GB/T 1727-1992漆膜一般制备法[S].GB/T 1727-1992 General preparation of paint film[S].
[27]GB/T 1723-1993涂料粘度测定法[S].GB/T 1723-1993Determination of viscosity of coatings[S].
[28]GB/T 9268-2008乳胶漆耐冻融性的测定[S].GB/T 9268-2008 Determination of freeze-thaw resistance of latex and emulsion paints[S].
[29]GB/T 1728-1979漆膜、腻子膜干燥时间测定法[S].GB/T 1728-1979 Methods of test for drying time of coatings of paints and putties[S].
[30]GB/T 1720-1979漆膜附着力测定法[S].GB/T 1720-1979 Method of test for adhesion of paint films[S].
[31]GB/T 1730-2007色漆和清漆摆杆阻尼试验[S].GB/T 1730-2007 Paints and varnishes-Pendulum damping test[S].
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