蝶豆花净油挥发性香气成分分析及卷烟加香应用
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摘要
[目的]开发新的烟用天然植物香料产品。[方法]采用超临界CO_2萃取法制备蝶豆花净油,运用GC/MS法分析蝶豆花净油中的挥发性成分,并进行卷烟加香试验和感官评价。[结果]蝶豆花净油中主要挥发性成分有57种,包括棕榈酸乙酯、棕榈酸甲酯、植酮、亚油酸乙酯、亚油酸甲酯、硬脂酸乙酯、新植二烯等。[结论]蝶豆花净油可用于卷烟加香,可以提质增香,修饰烟气,降低刺激性,改善余味,提升卷烟抽吸品质。
[Objective] The research aimed to develop new natural plant fragrance products for tobacco.[Method]The absolute oil from Clitoria ternatea flower was obtained by CO_2 supercritical extraction method,the volatile components in Clitoria ternatea flower absolute oil were analyzed by GC/MS method,and the cigarette flavoring test and sensory evaluation were carried out.[Result]There were 57 main volatile components in the absolute oil,including ethyl palmitate,methyl palmitate,phytonone,ethyl linoleate,methyl linoleate,ethyl stearate,and Neophytadiene,etc.[Conclusion]Clitoria ternatea flower absolute oil can be used for cigarette flavoring,which can enhance the aroma,modify the smooth of smoke,reduce the irritation,improve the aftertaste and improve the sensory quality of the cigarette.
[Objective] The research aimed to develop new natural plant fragrance products for tobacco.[Method]The absolute oil from Clitoria ternatea flower was obtained by CO_2 supercritical extraction method,the volatile components in Clitoria ternatea flower absolute oil were analyzed by GC/MS method,and the cigarette flavoring test and sensory evaluation were carried out.[Result]There were 57 main volatile components in the absolute oil,including ethyl palmitate,methyl palmitate,phytonone,ethyl linoleate,methyl linoleate,ethyl stearate,and Neophytadiene,etc.[Conclusion]Clitoria ternatea flower absolute oil can be used for cigarette flavoring,which can enhance the aroma,modify the smooth of smoke,reduce the irritation,improve the aftertaste and improve the sensory quality of the cigarette.
引文
[1] 中国科学院《中国植物志》编辑委员会.中国植物志:第41卷[M].北京:科学出版社,1995:262.
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[3] 中国科学院植物研究所编委会.中国高等植物图鉴:第2册[M].北京:科学出版社,1972:488.
[4] 林茂,唐遒冥,王华新,等.藤蔓花卉蝶豆的栽培技术[J].北方园艺,2013(18):80-81.
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[6] MUKHERJEE P K,KUMAR V,KUMAR N S,et al.The Ayurvedic medicine Clitoria ternatea:From traditional use to scientific assessment[J].Journal of ethnopharmacology,2008,120 (3):291-301.
[7] ZINGARE M L,ZINGARE P L,DUBEY A K,et al.Clitoria ternatea (aparajita):A review of the antioxidant,antidiabetic and hepatoprotective potentials[J].International journal of pharmacy and biological sciences,2013,3(1):203-213.
[8] NAIR V,BANG W Y,SCHRECKINGER E,et al.Protective role of ternatin anthocyanins and quercetin glycosides from butterfly pea (Clitoria ternatea leguminosae) blue flower petals against lipopolysaccharide (LPS)-induced inflammation in macrophage cells[J].Journal of agricultural & food chemistry,2015,63(28):6355-6365.
[9] TERAHARA N,ODA M,MATSUI T,et al.Five new anthocyanins,ternatins A3,B4,B3,B2 and D2 from Clitoria ternatea flowers[J].Journal of natural products,1996,59(2):139-144.
[10] KAZUMA K,NODA N,SUZUKI M.Malonylated flavonol glycosides from the petals of Clitoria ternatea[J].Phytochemistry,2003,62(2):229-237.
[11] REPETTO M G,LLESUY S F.Antioxidant properties of natural compounds used in popular medicine for gastric ulcers[J].Brazilian journal of medical & biological research,2002,35(5):523-534.
[12] 伍锦鸣,卓浩廉,普元柱,等.蓝莓花青素超声提取工艺优化及在卷烟中的应用研究[J].食品工业,2012,33(4):30-33.
[13] 毕薇,杨清,杨蕾,等.臭灵丹提取物在卷烟中增香降害应用研究[J].食品工业,2013,34(6):159-162.
[14] 瞿万云,余爱农,叶锐.超临界CO2萃取月季花挥发油的工艺研究[J].中药材,2006,29(5):488-490.
[15] 王恩鹏.人参花挥发油的质谱研究[D].长春:长春中医药大学,2010.
[16] 李东亮,胡军,许自成,等.单料烟感官质量的层次模糊综合评价[J].郑州轻工业学院学报(自然科学版),2007,22(1):27-30.
[17] 赵铭钦.卷烟调香学[M].北京:科学出版社,2008.
[18] 李丹丹,陈宣钦,赵得瑞,等.铁皮石斛改善卷烟评吸品质的物质基础研究[J].昆明理工大学学报(自然科学版),2016,41(5):100-105.
[19] 史宏志,刘国顺.烟草香味学[M].北京:中国农业出版社,1998.
[20] 佘世科,葛少林,徐迎波,等.超临界CO2流体萃取糊毛烟净油成分分析及其对卷烟感官质量的影响研究[J].香料香精化妆品 ,2015(3):17-21.
[21] 叶楠,肖作兵,刘强,等.气质联用-选择离子扫描测定卷烟主流烟气中糠醛的含量[J].食品工业科技,2012,33(9):366-368.
[22] 谢剑平.烟草香原料[M].北京:化学工业出版社,2009.
[23] 张悠金,金闻博.烟用香料香精[M].合肥:中国科学技术大学出版社,1996.
[2] 陈焕镛.海南植物志:第2卷[M].北京:科学出版社,1965:298-299.
[3] 中国科学院植物研究所编委会.中国高等植物图鉴:第2册[M].北京:科学出版社,1972:488.
[4] 林茂,唐遒冥,王华新,等.藤蔓花卉蝶豆的栽培技术[J].北方园艺,2013(18):80-81.
[5] BHUVAD S,NISHTESWAR K,SUMANASINGHE B G S M.Ethnomedicinal claims and pharmacological studies of Clitoria ternatea Linn:A review[J].Punarnav FEB,2015,2(6):1-10.
[6] MUKHERJEE P K,KUMAR V,KUMAR N S,et al.The Ayurvedic medicine Clitoria ternatea:From traditional use to scientific assessment[J].Journal of ethnopharmacology,2008,120 (3):291-301.
[7] ZINGARE M L,ZINGARE P L,DUBEY A K,et al.Clitoria ternatea (aparajita):A review of the antioxidant,antidiabetic and hepatoprotective potentials[J].International journal of pharmacy and biological sciences,2013,3(1):203-213.
[8] NAIR V,BANG W Y,SCHRECKINGER E,et al.Protective role of ternatin anthocyanins and quercetin glycosides from butterfly pea (Clitoria ternatea leguminosae) blue flower petals against lipopolysaccharide (LPS)-induced inflammation in macrophage cells[J].Journal of agricultural & food chemistry,2015,63(28):6355-6365.
[9] TERAHARA N,ODA M,MATSUI T,et al.Five new anthocyanins,ternatins A3,B4,B3,B2 and D2 from Clitoria ternatea flowers[J].Journal of natural products,1996,59(2):139-144.
[10] KAZUMA K,NODA N,SUZUKI M.Malonylated flavonol glycosides from the petals of Clitoria ternatea[J].Phytochemistry,2003,62(2):229-237.
[11] REPETTO M G,LLESUY S F.Antioxidant properties of natural compounds used in popular medicine for gastric ulcers[J].Brazilian journal of medical & biological research,2002,35(5):523-534.
[12] 伍锦鸣,卓浩廉,普元柱,等.蓝莓花青素超声提取工艺优化及在卷烟中的应用研究[J].食品工业,2012,33(4):30-33.
[13] 毕薇,杨清,杨蕾,等.臭灵丹提取物在卷烟中增香降害应用研究[J].食品工业,2013,34(6):159-162.
[14] 瞿万云,余爱农,叶锐.超临界CO2萃取月季花挥发油的工艺研究[J].中药材,2006,29(5):488-490.
[15] 王恩鹏.人参花挥发油的质谱研究[D].长春:长春中医药大学,2010.
[16] 李东亮,胡军,许自成,等.单料烟感官质量的层次模糊综合评价[J].郑州轻工业学院学报(自然科学版),2007,22(1):27-30.
[17] 赵铭钦.卷烟调香学[M].北京:科学出版社,2008.
[18] 李丹丹,陈宣钦,赵得瑞,等.铁皮石斛改善卷烟评吸品质的物质基础研究[J].昆明理工大学学报(自然科学版),2016,41(5):100-105.
[19] 史宏志,刘国顺.烟草香味学[M].北京:中国农业出版社,1998.
[20] 佘世科,葛少林,徐迎波,等.超临界CO2流体萃取糊毛烟净油成分分析及其对卷烟感官质量的影响研究[J].香料香精化妆品 ,2015(3):17-21.
[21] 叶楠,肖作兵,刘强,等.气质联用-选择离子扫描测定卷烟主流烟气中糠醛的含量[J].食品工业科技,2012,33(9):366-368.
[22] 谢剑平.烟草香原料[M].北京:化学工业出版社,2009.
[23] 张悠金,金闻博.烟用香料香精[M].合肥:中国科学技术大学出版社,1996.