提升出水瓷器脱盐效率的方法研究
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摘要
研究了几种在传统浸泡法的基础上提高出水瓷器脱盐效率的方法,电导率测试结果、XRF检测结果以及硝酸银定性分析结果表明,这几种方法均可以在一定程度上提高瓷器脱盐效率,压缩传统浸泡脱盐法所需的时间。
Several modifications were studied to improve the efficiency of traditional soaking methods for desalination of porcelains found in undersea environments. Conductivity testing, X-ray fluorescence(XRF) testing and qualitative analysis using silver nitrate were performed to see the effects. The results show that these modifications can improve the porcelain desalination efficiency to a certain extent, primarily by taking less time needed.
Several modifications were studied to improve the efficiency of traditional soaking methods for desalination of porcelains found in undersea environments. Conductivity testing, X-ray fluorescence(XRF) testing and qualitative analysis using silver nitrate were performed to see the effects. The results show that these modifications can improve the porcelain desalination efficiency to a certain extent, primarily by taking less time needed.
引文
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[2] 中国国家博物馆水下考古研究中心,海南省文物保护管理办公室编著.西沙水下考古1998—1999[M].北京:科学出版社,2006.The Underwater Archaeological Research Center of the National Museum of China,the office of Hainan Province Heritage Conservation and Management.Underwater archaeology in Xisha 1998—1999[M].Beijing:Science Press,2006.
[3] 王艳蓉,朱铁权,冯泽阳,等.“南海Ⅰ号”出水古陶瓷器科技分析研究[J].岩矿测试,2014,33(3):332-339.WANG Yanrong,ZHU Tiequan,FENG Zeyang,et al.The technological analysis of the ancient ceramics discovered from “Nanhai No.1 Shipwreck” [J].Rock and Mineral Analysis,2014,33(3):332-339.
[4] 包春磊.海洋出水陶瓷器的科技保护[J].文物鉴定与鉴赏,2013(7):52-57.BAO Chunlei.Scientific and technological protection of ocean outflow water ceramics[J].Identification and Appreciation to Cultural Relics,2013(7):52-57.
[5] 王惠贞,宋迪生,程玉冰,等.汉阳陵出土陶质文物保护研究[J].文博,2009(6):244-250.WANG Huizhen,SONG Disheng,CHENG Yubing,et al.Research of Yangling excaveted ceramic relics[J].Relics and Museology,2009(6):244-250.
[6] 樊再轩,陈港泉,苏伯民,等.莫高窟第98窟酥碱壁画保护修复实验研究[J].敦煌研究,2009(6):4-7.FAN Zaixuan,CHEN Gangquan,SU Bomin,et al.The testing study for repairing the disruption wall paintings in Cave 98 at Mogao Grottoes[J].Dunhuang Research,2009(6):4-7.
[7] 张步宁,刘永,崔英德,等.基于可再生天然原料的绿色高吸水树脂的研究进展[J].材料导报,2009,23(17):63-66.ZHANG Buning,LIU Yong,CUI Yingde,et al.Research progress in renewable natural materials-based green superabsorbent polymers[J].Materials Reports,2009,23(17):63-66.
[8] SELWITZ C,DOEHNE E.The evaluation of crystallization modifiers for controlling salt damage to limestone[J].Journal of Cultural Heritage,2002,3(3):205-216.
[9] 卢燕玲.文物保护修复理论与实践[M].北京:文物出版社,2016:35-36.LU Yanling.Theory and practice of cultural relics conservation and restoration[M].Beijing:Cultural Relics Press,2016:35-36.
[10] 马燕如.我国水下考古发掘陶瓷器的脱盐保护初探[J].博物馆研究,2007(1):85-88.MA Yanru.Preliminary study of desalination protection of ceramics from underwater archaeological excavations in China[J].Museum Research,2007(1):85-88.
[11] 席细平,马重芳,王伟.超声波技术应用现状[J].山西化工,2007,27(1):25-29.XI Xiping,MA Chongfang,WANG Wei.Application situation of ultrasonic technology[J].Shanxi Chemical Industry,2007,27(1):25-29.
[12] 刘国洪,匡同春,胡松青,等.超声波电镀的研究进展[J].电镀与涂饰,2006,25(3):47-50.LIU Guohong,KUANG Tongchun,HU Songqing,et al.Development of electroplating in ultrasonic field[J].Electroplating and Finishing,2006,25(3):47-50.
[13] 赵国玺,朱步瑶.表面活性剂作用原理[J].日用化学工业信息,2003(17):16.ZHAO Guoxi,ZHU Buyao.Principle of surfactant action[J].China Surfactant Detergent & Cosmetics,2003(17):16.
[14] 成小林,陈淑英,韩英,等.氯离子选择性电极测定铁器碱性脱盐溶液中氯离子的含量[J].文物保护与考古科学,2010,22(3):10-14.CHENG Xiaolin,CHEN Shuying,HAN Ying,et al.Measuring chloride ion concentration in alkaline solutions by chloride specific ion electrode during trentment of corroded iron objects[J].Sciences of Conservation and Archaeology,2010,22(3):10-14.
[15] 冯伟,徐金霞,蒋林华,等.有机添加剂对电化学除盐效率的影响研究[J].混凝土,2016(10):100-103.FENG Wei,XU Jinxia,JIANG Linhua,et al.Influence of organic addictive on electrochemical chloride extraction efficiency[J].Concrete,2016(10):100-103.
[16] 戴忠旭,甘复兴,汪的华,等.铜缓蚀剂成膜过程的PECQCM研究[C]//第四届中国青年腐蚀与防护学术研讨会暨第六届全国青年腐蚀与防护科技论文讲评会,1999:133-136.DAI Zhongxu,GAN Fuxing,WANG Dehua,et al.PECQCM study on filming process of copper corrosion inhibitor[C]//The Fourth China Youth Corrosion and Protection Symposium and the Sixth National Youth Corrosion and Protection Scientific and Technological Papers Appraisement Meeting,1999:133-136.