高温热台在材料研究领域中的应用
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摘要
综述了高温热台在材料研究领域中的应用,包括实时观察晶体熔融与生长、材料烧结、相变、纳米粉体熔化和低共熔。对比常规实验方法,指出了高温热台在研究材料结构、性能方面的优势,总结了高温热台在材料研究领域中所取得的一些创新性成果。最后指出了高温热台在研究材料组成、结构、性能以及原位观察等方面存在的不足,并展望了其未来的发展方向。
The application of hot-stage device in material scientific research is summarized,including in situ observation of crystal melting/growth behavior,material sintering process,phase transition,nano-particle melting and eutectic process.Compared with normal analytical method,heating-stage have a great many advantage in investigating the structure and property of materials,a series of innovative achievements making by hot-stage device are listed.Finally,it is pointed out that the defect and improvement of in situ hot-stage research method in material research area under micro-scale and mesoscopic-scale.
The application of hot-stage device in material scientific research is summarized,including in situ observation of crystal melting/growth behavior,material sintering process,phase transition,nano-particle melting and eutectic process.Compared with normal analytical method,heating-stage have a great many advantage in investigating the structure and property of materials,a series of innovative achievements making by hot-stage device are listed.Finally,it is pointed out that the defect and improvement of in situ hot-stage research method in material research area under micro-scale and mesoscopic-scale.
引文
1蒋国昌,尤静林.用于硅酸盐熔体微结构研究的高温Ra-mam光谱技术[J].硅酸盐学报,2003,31(10):998
2 Tsukamoto K,Abe T,Sunagawa I.In situ observation ofcrystals growing in high temperature melts or solutions[J].J Cryst Growth,1983,63(1):215
3 Kozo Fujiwara,Kensaku Maeda,et al.In situobservation ofSi faceted dendrite growth from low-degree-of-undercoolingmelts[J].Acta Mater,2008,56(11):2633
4 Pan Xiuhong,Jin Weiqing,Hong Yong,et al.In situ ob-servation of skeletal shape transition during BaB2O4crystalgrowth in high-temperature solution[J].Chin Phys Lett,2006,23(8):2269
5洪勇,潘秀红,张学华,等.β-BaB2O4枝蔓晶的形成机理[J].中国科学E期:技术科学,2007,37(11):1430
6潘秀红,金蔚青,刘岩.BaB2O4单晶快速生长时的界面形态与表面台阶形貌[J].中国科学G辑:物理学力学天文学,2007,37(3):403
7梁歆桉,金蔚青.Bi12SiO20熔体表面张力对流研究[J].无机材料学报,2001,16(1):32
8潘秀红,金蔚青,艾飞,等.表面张力对BaB2O4晶体生长界面边界层的作用[J].无机材料学报,2007,22(6):1239
9蔡丽霞,金蔚青,等.对流效应和溶质浓度对KNbO3晶体界面形貌稳定性的影响[J].无机材料学报,2001,16(4):609
10 Massera J,Remond J.Nucleation and growth behavior ofglasses in the TeO2-Bi2O3-ZnO glass system[J].J Non-Crystalline Solids,2010,356(52-54):2947
11艾飞,金蔚青,洪勇,等.磁场对氧化物熔体中振荡态热毛细对流的抑制作用研究[J].中国科学G期:物理学力学天文学,2007,37(3):385
12 Kozo Fujiwara,Yoshikazu Obinata,Toru Ujihara,et al.In-situ observations of melt growth behavior of polycrystallinesilicon[J].J Cryst Growth,2004,262(1-4):124
13 Toshiro Minami,Susumu Maeda,Mitsuo Higasa.In-situ ob-servation of bubble formation at silicon melt-silica glass in-terface[J].J Cryst Growth,2011,318(1):196
14 Wu Yongkuan,Liu Kun,Li Dawei.In situ AFM and Ra-man spectroscopy study of the crystallization behavior ofGe2Sb2Te5films at different temperature[J].Appl Surf Sci,2011,258(4):1619
15 Malinov S,Sha W,Voon C S.In situ high temperature mi-croscopy study of the surface oxidation and phase transfor-mations in titanium alloys[J].J Microscopy,2002,207(3):163
16 Huang Ling,Li Qingjie,Shan Zhiwei.A new regime formechanical annealing and strong sample-size strengthening inbody centred cubic molybdenum[J].Nat Commun,2011,547(2):1
17 Wu J,Howe J M,Zhang W Z.An in situ transmission elec-tron microscopy study of interface growth during martensitictransformation in an Fe-Ni-Mn alloy[J].Acta Mater,2011,59(8):3297
18 Orlando Rios,Sonalika Goye,Michael S Kesler.An evalua-tion of high-temperature phase stability in the Ti-Al-Nb sys-tem[J].Scr Mater,2009,60(3):156
19Shintani H,Tanaka H.Frustration on the way to crystalli-zation in glass[J].Nat Phys,2006,2(3):200
20 Grant S Henderson,Daniel R Neuville.The structure ofGeO2-SiO2glasses and melts:A Raman spectroscopy study[J].J Non-Crystalline Solids,2009,355(8):468
21Shigeaki Ono,Yasuo Ohishi.In situ X-ray observation ofphase transformation in Fe2O3at high pressures and hightemperatures[J].J Phys Chem Solids,2005,66(10):1714
22仇怀利,王爱华,尤静林.BSO晶体的高温拉曼光谱与高温结构特征[J].光谱学与光谱分析,2005,25(2):222
23 Dittmera S,Olofssona N.In situ Raman studies of single-walled carbon nanotubes grown by local catalyst heating[J].Chem Phys Lett,2008,457(1-3):206
24张芳,张澜庭,单爱党,等.NbSi2在1023K氧化动力学和氧化行为的高温原位观察[J].中国科学E辑:技术科学,2006,36(3):235
25 Adella V,Cheesemana C R,et al.Characterising the sinte-ring behaviour of pulverised fuel ash using heating stage mi-croscopy[J].Mater Charact,2007,58(10):980
26 Aldo R Boccaccinia,Reinhard Conradt.Isotropic shrinkageof plateletcontainingglass powder compacts during isother-mal sintering[J].Int J Inorg Mater,2001,3(2):101
27 Dweck J,Morais L C,Fonseca M V A,et al.Calcinedsludge sintering evalution by heating microscopy thermalanalysis[J].J Therm Anal Calorim,2009,95(3):985
28Boccaccini A R,et al.Use of heating microscopy to assesssintering anisotropy in layered glass metal powder compacts[J].Adv Appl Ceram,2006,105(5):232
29 Tarek K Khalil,Aldo R Boccaccini.Heating microscopystudy of the sintering behaviour of glass powder compacts inthe binary system SiO2-TiO2[J].Mater Lett,2002,56(3):317
30 Markus Eberstein,Stefan Reinsch,Joachim Deubener.Sin-tering of glass matrix composites with small rigid inclusions[J].J Eur Ceram Soc,2009,29(12):2469
31Smilja Markovic',Dragan Uskokovic'.The master sinteringfor BaTi0.975Sn0.025O3/BaTi0.85Sn0.15O3functionally gradedmaterials[J].J Eur Ceram Soc,2009,29(11):2309
32Emamy M,Mahta M,Rasizadeh J.Formation of TiB2parti-cles during dissolution of TiAl3 in Al-TiB2 metal matrixcomposite using an in situ technique[J].Compos Sci Techn,2006,66(7-8):1063
33Zafeiropoulos N E,Baillie C A,Matthews F L.A study oftranscrystallinity and its effect on the interface in flax fibrereinforced compositematerials[J].Compos Part A,2001,32(3-4):525
34Rankin J,Sheldon B W.In situ TEM sintering of nano-sizedZrO2particles[J].Mater Sci Eng A,1995,204(1-2):48
35Olson E A,Efremov Yu M,et al.Size-dependent melting ofBi nanoparticles[J].J Appl Phys,2005,97(3):030041
36 Mitome M.In-situ observation of melting of fine lead parti-cles by high-resolution electron microscopy[J].Surf SciLett,1999,442(1):953
2 Tsukamoto K,Abe T,Sunagawa I.In situ observation ofcrystals growing in high temperature melts or solutions[J].J Cryst Growth,1983,63(1):215
3 Kozo Fujiwara,Kensaku Maeda,et al.In situobservation ofSi faceted dendrite growth from low-degree-of-undercoolingmelts[J].Acta Mater,2008,56(11):2633
4 Pan Xiuhong,Jin Weiqing,Hong Yong,et al.In situ ob-servation of skeletal shape transition during BaB2O4crystalgrowth in high-temperature solution[J].Chin Phys Lett,2006,23(8):2269
5洪勇,潘秀红,张学华,等.β-BaB2O4枝蔓晶的形成机理[J].中国科学E期:技术科学,2007,37(11):1430
6潘秀红,金蔚青,刘岩.BaB2O4单晶快速生长时的界面形态与表面台阶形貌[J].中国科学G辑:物理学力学天文学,2007,37(3):403
7梁歆桉,金蔚青.Bi12SiO20熔体表面张力对流研究[J].无机材料学报,2001,16(1):32
8潘秀红,金蔚青,艾飞,等.表面张力对BaB2O4晶体生长界面边界层的作用[J].无机材料学报,2007,22(6):1239
9蔡丽霞,金蔚青,等.对流效应和溶质浓度对KNbO3晶体界面形貌稳定性的影响[J].无机材料学报,2001,16(4):609
10 Massera J,Remond J.Nucleation and growth behavior ofglasses in the TeO2-Bi2O3-ZnO glass system[J].J Non-Crystalline Solids,2010,356(52-54):2947
11艾飞,金蔚青,洪勇,等.磁场对氧化物熔体中振荡态热毛细对流的抑制作用研究[J].中国科学G期:物理学力学天文学,2007,37(3):385
12 Kozo Fujiwara,Yoshikazu Obinata,Toru Ujihara,et al.In-situ observations of melt growth behavior of polycrystallinesilicon[J].J Cryst Growth,2004,262(1-4):124
13 Toshiro Minami,Susumu Maeda,Mitsuo Higasa.In-situ ob-servation of bubble formation at silicon melt-silica glass in-terface[J].J Cryst Growth,2011,318(1):196
14 Wu Yongkuan,Liu Kun,Li Dawei.In situ AFM and Ra-man spectroscopy study of the crystallization behavior ofGe2Sb2Te5films at different temperature[J].Appl Surf Sci,2011,258(4):1619
15 Malinov S,Sha W,Voon C S.In situ high temperature mi-croscopy study of the surface oxidation and phase transfor-mations in titanium alloys[J].J Microscopy,2002,207(3):163
16 Huang Ling,Li Qingjie,Shan Zhiwei.A new regime formechanical annealing and strong sample-size strengthening inbody centred cubic molybdenum[J].Nat Commun,2011,547(2):1
17 Wu J,Howe J M,Zhang W Z.An in situ transmission elec-tron microscopy study of interface growth during martensitictransformation in an Fe-Ni-Mn alloy[J].Acta Mater,2011,59(8):3297
18 Orlando Rios,Sonalika Goye,Michael S Kesler.An evalua-tion of high-temperature phase stability in the Ti-Al-Nb sys-tem[J].Scr Mater,2009,60(3):156
19Shintani H,Tanaka H.Frustration on the way to crystalli-zation in glass[J].Nat Phys,2006,2(3):200
20 Grant S Henderson,Daniel R Neuville.The structure ofGeO2-SiO2glasses and melts:A Raman spectroscopy study[J].J Non-Crystalline Solids,2009,355(8):468
21Shigeaki Ono,Yasuo Ohishi.In situ X-ray observation ofphase transformation in Fe2O3at high pressures and hightemperatures[J].J Phys Chem Solids,2005,66(10):1714
22仇怀利,王爱华,尤静林.BSO晶体的高温拉曼光谱与高温结构特征[J].光谱学与光谱分析,2005,25(2):222
23 Dittmera S,Olofssona N.In situ Raman studies of single-walled carbon nanotubes grown by local catalyst heating[J].Chem Phys Lett,2008,457(1-3):206
24张芳,张澜庭,单爱党,等.NbSi2在1023K氧化动力学和氧化行为的高温原位观察[J].中国科学E辑:技术科学,2006,36(3):235
25 Adella V,Cheesemana C R,et al.Characterising the sinte-ring behaviour of pulverised fuel ash using heating stage mi-croscopy[J].Mater Charact,2007,58(10):980
26 Aldo R Boccaccinia,Reinhard Conradt.Isotropic shrinkageof plateletcontainingglass powder compacts during isother-mal sintering[J].Int J Inorg Mater,2001,3(2):101
27 Dweck J,Morais L C,Fonseca M V A,et al.Calcinedsludge sintering evalution by heating microscopy thermalanalysis[J].J Therm Anal Calorim,2009,95(3):985
28Boccaccini A R,et al.Use of heating microscopy to assesssintering anisotropy in layered glass metal powder compacts[J].Adv Appl Ceram,2006,105(5):232
29 Tarek K Khalil,Aldo R Boccaccini.Heating microscopystudy of the sintering behaviour of glass powder compacts inthe binary system SiO2-TiO2[J].Mater Lett,2002,56(3):317
30 Markus Eberstein,Stefan Reinsch,Joachim Deubener.Sin-tering of glass matrix composites with small rigid inclusions[J].J Eur Ceram Soc,2009,29(12):2469
31Smilja Markovic',Dragan Uskokovic'.The master sinteringfor BaTi0.975Sn0.025O3/BaTi0.85Sn0.15O3functionally gradedmaterials[J].J Eur Ceram Soc,2009,29(11):2309
32Emamy M,Mahta M,Rasizadeh J.Formation of TiB2parti-cles during dissolution of TiAl3 in Al-TiB2 metal matrixcomposite using an in situ technique[J].Compos Sci Techn,2006,66(7-8):1063
33Zafeiropoulos N E,Baillie C A,Matthews F L.A study oftranscrystallinity and its effect on the interface in flax fibrereinforced compositematerials[J].Compos Part A,2001,32(3-4):525
34Rankin J,Sheldon B W.In situ TEM sintering of nano-sizedZrO2particles[J].Mater Sci Eng A,1995,204(1-2):48
35Olson E A,Efremov Yu M,et al.Size-dependent melting ofBi nanoparticles[J].J Appl Phys,2005,97(3):030041
36 Mitome M.In-situ observation of melting of fine lead parti-cles by high-resolution electron microscopy[J].Surf SciLett,1999,442(1):953