关键制丝工艺对烟气成分中挥发性成分的影响
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- 英文论文题名：Effects of key process in the primary processing of cigarette production on volatile components of cigarette smoke
- 论文作者：张宏宇 ; 刘春波 ; 张涛 ; 徐文秀 ; 何沛 ; 申钦鹏 ; 杨光宇 ; 刘志华 ; 缪明明
- 英文论文作者：ZHANG Hong-yu ; LIU Chun-bo ; ZHANG Tao ; XU Wen-xiu ; HE Pei ; SHEN Qin-peng ; YANG Guang-yu ; LIU Zhi-hua ; MIAO Ming-ming ; Key Lab of Tobacco Chemistry of Yunnan ; Research&Development Center ; China Tobacco Yunnan Industrial Co. ; LTD ; College of Chemical Engineering ; Kunming University of Science and Technology ; Kunming Medical University ; School of Pharmaceutical Science&Yunnan Key Laboratory of Pharmacology for Natural Products
- 年：2016
- 作者机构：云南中烟工业有限责任公司技术中心云南省烟草化学重点实验室;昆明理工大学化学与工程学院;昆明医科大学药学院云南省天然药物药理重点实验室;
- 论文关键词：GC-MS ; 工艺参数 ; 挥发性成分 ; 致香成分
- 英文论文关键词：GC-MS ; processing parameter ; volatile component ; aroma component
- 会议召开时间：2016-12-01
- 会议录名称：中国烟草学会2016年度优秀论文汇编——烟草工业主题
- 语种：中文
- 分类号：TS452
- 学会代码：ZGYG
- 学会名称：中国烟草学会
- 页数：6
- 文件大小：395k
- 原文格式：D
摘要
采用气相色谱-质谱联用仪(GC-MS)测定了不同制丝工艺参数(松散回潮的热风温度、切丝宽度、HT工作蒸汽流量、烘丝热风温度和排潮风门开度)条件下制成的卷烟样品烟气成分中的挥发性成分。结果表明:酯类物质的释放总量在这些工艺参数条件下存在极显著差异的水平,说明酯类物质的释放总量在5种工艺参数不同条件下的变化是极明显的。综合分析部分致香成分和简单酚类的释放总量,选取样品2与样品4的工艺参数条件进行对比可知较高的松散回潮热风温度和烘丝热风温度更加有利于增加卷烟烟气中挥发性成分的释放量;在增加卷烟香吃味方面样品4的工艺参数条件为最佳生产条件,在该工艺条件下生产出的卷烟样品其烟气成分中致香成分的释放总量最多。
Using GC-MS for analysing the volatile components of cigarette smoke in the different processing parameters about primary processing of cigarette production(hot air temperature in ordering cylinder,cut width of tobacco,steam flow rate in HT,hot air temperature in dryer,and exhaust vane opening in dryer).The results showed that:1)The whole releasing amounts of esters had highly significant difference in these processing parameters,it showed that the whole releasing amounts of esters in cigarette smoke had extremely obvious changes under the condition of five different processing parameters;2) Comprehensive analysis about the whole releasing amounts of partly aroma components and simple construction of phenolic compounds,the higher hot air temperature in ordering cylinder and hot air temperature in dryer were used for increasing the volatile components of cigarette smoke by comparing sample 2 with sample 4;3) In terms of increasing the aroma and taste of cigarette,the technological parameters of sample 4 was optimum production conditions,in this production conditions,the whole releasing amounts of the aroma components was maximum quantity in cigarette smoke.
Using GC-MS for analysing the volatile components of cigarette smoke in the different processing parameters about primary processing of cigarette production(hot air temperature in ordering cylinder,cut width of tobacco,steam flow rate in HT,hot air temperature in dryer,and exhaust vane opening in dryer).The results showed that:1)The whole releasing amounts of esters had highly significant difference in these processing parameters,it showed that the whole releasing amounts of esters in cigarette smoke had extremely obvious changes under the condition of five different processing parameters;2) Comprehensive analysis about the whole releasing amounts of partly aroma components and simple construction of phenolic compounds,the higher hot air temperature in ordering cylinder and hot air temperature in dryer were used for increasing the volatile components of cigarette smoke by comparing sample 2 with sample 4;3) In terms of increasing the aroma and taste of cigarette,the technological parameters of sample 4 was optimum production conditions,in this production conditions,the whole releasing amounts of the aroma components was maximum quantity in cigarette smoke.
引文
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[13]陈昆燕,薛芳,曾建,等.重点工序工艺参数与卷烟主流烟气中巴豆醛释放量的关系研究[J].江西农业学报,2009,21(12):40-42.
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[24]殷艳华.GC/MS法检测24种烤烟烟气中的角鲨烯含量[J].广东农业科学,2012,(3):105-107.
[25]者为,杨斯宛,王明峰,等.烟草和烟气中酚类物质检测技术研究进展[J].云南化工,2010,37(5):64-69.
[26]刘静,侯英,杨蕾,等.烟草中多酚热裂解产物研究[J].化学研究与应用,2011,23(1):63-65.
[2]胡建军,周冀衡,熊燕,等.烘丝工艺参数对烘后叶丝质量影响的研究[J].中国烟草学报,2007,13(6):24-29.
[3]叶春文,杨明权,王兵,等.烘丝工艺参数对卷烟感官质量的影响[J].烟草科技,2005,11:7-9.
[4]何蓉,李东亮,周学政,等.卷烟“HT+烘丝”工艺参数对叶丝常规化学成分的影响[J].河北农业科学,2011,15(1):70-72.
[5]王道铨,林志平,代宁光,等.不同膨胀温度对卷烟主流烟气7种Hofmann成分释放量的影响[J].安徽农业科学,2012,40(12):7389-7391.
[6]于存峰,于录,杨雷,等.模块加工中叶丝宽度组合对卷烟质量的影响[J].烟草科技,2011,(6):9-11.
[7]白晓莉,邹泉,董伟,等.工艺加工对再造烟叶致香成分、有害成分和感官质量的影响[J].烟草科技,2009,10:12-20.
[8]薛芳,李东亮,陈昆燕,等.卷烟加工重点工序工艺参数与卷烟主流烟气中苯酚释放量的关系研究[J].江西农业大学学报,2010,32(6):1307.1312.
[9]谭兰兰,施丰成,薛芳,等.卷烟制丝工艺参数对主流烟气中苯并[a]芘释放量的影响[J].安徽农业科学,2010,38(1):165-167.
[10]陈昆焱.烟梗切丝宽度对梗丝工艺质量的影响研究[J].安徽农业科学,2013,41(1):307.350.
[11]邱光明,谭兰兰,汪长国,等.制丝工艺参数对卷烟减害降焦的影响研究[J].湖南农业科学,2013,(1):101.114.
[12]谭兰兰,施丰成,薛芳,等.卷烟制丝工艺参数对主流烟气中苯并[a]芘释放量的影响[J].安徽农业科学,2010,38(1):165.167.
[13]陈昆燕,薛芳,曾建,等.重点工序工艺参数与卷烟主流烟气中巴豆醛释放量的关系研究[J].江西农业学报,2009,21(12):40-42.
[14]谢卫,黄朝章,苏明亮,等.辅助材料设计参数对卷烟7种烟气有害成分含量及其危害性指数的影响[J].烟草科技,2013,1:31-38.
[15]Xue F,Li D,Dai Y,et a1.Relationship analysis of seven harmful ingredients emission in microwave loose cigarette process parameters and cigarette mainstream smoke[J].Asian J Chem,2012,24(3):1023-1028.
[16]张涛,苏明亮,赵伟,等.制丝工艺参数对9种主流烟气成分释放量的影响[J].烟草科技,2014,8:32-37.
[17]Anderson M J,Whitcomb P J,Kraber S L.et a1.Hand-book for experimenters[M].Minneapolis:Stat-Ease Inc,2009.
[18]Bischof W,Miller F.Optimal designs which are efficient for lack of fit tests[J].Ann Stat,2006,34(4):2015-2025.
[19]Nguyen N K,Miller A J.A review of some exchange algo-rithms for constructing discrete D-optimal design[J].Comput Stat Data An,1992,14(4):489-498.
[20]De Aguiar P F,Bourguignon B,Khots M S,et a/.D-optimal designs[J].Chemometr Intell Lab,1995,30(2):199-210.
[21]Hardin R H,Sloane N J A.A new approach to the con-struction of optimal designs[J].J Stat Plan Infer,1993,37(3):339-369.
[22]Atkinson A C,Donev A N,Tobias R D.Optimum experimental design,with SAS[M].Oxford University Press Ine,2007.
[23]米冠杰,顾文博,孙文梁,等.卷烟烟气重要酸性香味成分的分离制备与鉴定[J].烟草科技,2013,(10):49-54.
[24]殷艳华.GC/MS法检测24种烤烟烟气中的角鲨烯含量[J].广东农业科学,2012,(3):105-107.
[25]者为,杨斯宛,王明峰,等.烟草和烟气中酚类物质检测技术研究进展[J].云南化工,2010,37(5):64-69.
[26]刘静,侯英,杨蕾,等.烟草中多酚热裂解产物研究[J].化学研究与应用,2011,23(1):63-65.