摘要
通过影响因素试验、最低检出限试验、精密度与准确度试验等,创新性地对甲基橙分光光度法测定光气中游离氯进行了研究。结果表明,甲基橙分光光度法检出范围宽,精密度与准确度较高,适用于光气中游离氯含量的测定。
Methyl Orange Spectrometry which could determine the free chlorine content in phosgene was discussed,by effect factors testing,the lowest detectable concentration precision,recovery rate experiments.Finally,it was indicated that the method had wide testing range,high sensitivity,accuracy and precision.It was applicable for testing the free chlorine content in phosgene.
引文
[1]张坤鹏.MDI行业中光气合成反应的研究概况[J].广州化工,2010,38(7):63-64.
[2]谢有亮,种丽娜,孙桂珍.甲基橙分光光度法测定氯气方法的条件优化[J].广西轻工业,2010,26(2):8-9.