烤烟香型的定量判别及其与产区的对应关系
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- 英文论文题名：Quantitative determination for flavorof flue-cured tobacco and correspondence between flavor and producing areas
- 论文作者：李超 ; 鲍明亮 ; 秦云华 ; 李娥贤 ; 吴亿勤 ; 杨光宇 ; 张承明
- 英文论文作者：LI Chao ; BAOMing-liang ; Qin Yun-hua ; LIE-xian ; WU Yi-qin ; YANG Guang-yu ; ZHANGCheng-ming ; Cigarette Product Quality Inspection Institute ; Technology Center of Yunnan Tobacco Industry Co. ; Ltd. ; Labstat international ULC ; Yunnan Academy of Agricultural Sciences ; Institute of Biotechnology and Genetic Resources
- 年：2016
- 作者机构：云南中烟工业有限责任公司技术中心卷烟产品质量检测中心;Labstat国际ULC;云南省农业科学研究院生物技术与种质资源研究所;
- 论文关键词：烤烟烟叶 ; 化学组成 ; 多元因子分析 ; 判别分析 ; 对应分析
- 英文论文关键词：Flue-cured tobacco ; Chemical components ; Multivariate factor analysis ; Discriminant analysis ; correspondence analysis
- 会议召开时间：2016-12-01
- 会议录名称：中国烟草学会2016年度优秀论文汇编——烟草工业主题
- 语种：中文
- 分类号：TS47
- 学会代码：ZGYG
- 学会名称：中国烟草学会
- 页数：16
- 文件大小：1716k
- 原文格式：D
摘要
为研究烤烟化学组成与其香型间的关系,通过抽样法收集了2012年国内14省29市/州500个烟叶样品。参照行业及文献标准测定影响其品质的117种化学指标,对各指标采用因子分析(Multiple Factor Analysis,MFA)降维处理,因子得分构建Bayes香型定量判别模型并验证,同时对香型与产区进行对应分析。结果表明:原始指标可提出24个公因子,其对原变量的总方差解释率为83.697%;定量判别模型能依据巨豆三烯酮、呋喃、碱等类物质的含量对烟叶香型进行很好的预测,交叉验证正确率≥89.5%,外部验证正确率≥97.0%;经因子得分加权的香型与产区对应分析结果与感官评吸结果总体一致,各省份香型特质排序为:清香:云>闽>蜀;中间香:渝>黔>黑>鄂;浓香:豫>皖>粤>赣>陕>鲁>湘。判别模型对快速和客观的评价烟叶品质具有重要现实意义。
To study the relationship between the chemical composition of flue-cured tobacco and its flavor, we collected 500 tobacco samples from domestic 14 provinces or 29 regions of 2012 by the sampling method. Referring to the relevant industry standards and literature methods, we 117 kinds of chemical indicators, which significantly affected the quality of flue-cured tobacco,used-Factor analysis(Multiple Factor Analysis, MFA) to dimension reduction, constructed flavor quantitative scores Bayes discriminant model and verified the model. Then we made correspondence analysis between the flavor and producing areas. The results showed that: Original indicators can be picked up 24 common factors, the total variance of the original variables explained was 83.697%. Based on detected content of megastigmatrienone, furan, alkali and other substances, quantitative discriminant model can predict flavor for tobacco samples well, the correct rate of cross validation ≥ 89.5%, and the correct rate of external validation ≥ 97.0% After scores weighted, corresponding analytical results between flavor and producing areas are consistent with the sensory evaluation results overall, provinces flavor qualities Sort: light flavor: Yun> Min> Shu; intermediate flavor: Chongqin> Qian>Hei> E; strong flavor: Yu> Wan> Yue>Gan> Shan> Lu> Xiang. Discriminant model has important practical significance for fast and objective evaluation of the quality of tobacco.
To study the relationship between the chemical composition of flue-cured tobacco and its flavor, we collected 500 tobacco samples from domestic 14 provinces or 29 regions of 2012 by the sampling method. Referring to the relevant industry standards and literature methods, we 117 kinds of chemical indicators, which significantly affected the quality of flue-cured tobacco,used-Factor analysis(Multiple Factor Analysis, MFA) to dimension reduction, constructed flavor quantitative scores Bayes discriminant model and verified the model. Then we made correspondence analysis between the flavor and producing areas. The results showed that: Original indicators can be picked up 24 common factors, the total variance of the original variables explained was 83.697%. Based on detected content of megastigmatrienone, furan, alkali and other substances, quantitative discriminant model can predict flavor for tobacco samples well, the correct rate of cross validation ≥ 89.5%, and the correct rate of external validation ≥ 97.0% After scores weighted, corresponding analytical results between flavor and producing areas are consistent with the sensory evaluation results overall, provinces flavor qualities Sort: light flavor: Yun> Min> Shu; intermediate flavor: Chongqin> Qian>Hei> E; strong flavor: Yu> Wan> Yue>Gan> Shan> Lu> Xiang. Discriminant model has important practical significance for fast and objective evaluation of the quality of tobacco.
引文
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[21]YC/T 162-2011烟草及烟草制品氯的测定连续流动法[s].YC/T 162-2011Tobacco and tobacco products-Determination of chlorine-continuous flow method[s].
[22]YC/T 173-2003烟草及烟草制品钾的测定火焰光度法[s].YC/T 173-2003Tobacco and tobacco products-Determination of potassium-Flame photometry[s].
[23]YC/T 159-2002烟草及烟草制品水溶性糖的测定连续流动法[s].YC/T 159-2002Tobacco and tobacco products-Determination of water-soluble sugarscontinuous flow method[s].
[24]YC/T 160-2002烟草及烟草制品总植物碱的测定连续流动法[s].YC/T 160-2002Tobacco and tobacco products-Determination of total alkaloids-continuous flow method[s].
[25]YC/T 161-2002烟草及烟草制品总氮的测定连续流动法[s].YC/T 161-2002Tobacco and tobacco products-Determination of total nitrogen-continuous flow method[s].
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[2]张槐苓,葛翠英,穆怀静,等.烟草分析与检验[M].郑州:河南科学技术出版社,1994:103-111.ZHANG Huailing,GE Cuiying,MU Huaijing,et al.Tobacco analysis and test[M].Zhengzhou:Henan Science and Technology Press,1994:103-111.
[3]谢剑平.烟草香原料[M].北京:化学工业出版社,2009:70-447.XIE Jianping.Tobacco fragrance raw materials[M].Beijing:Chemical Industry Press,2009:70-447.
[4]陆龙建,陈磊,余苓,等.多元因子分析在卷烟风格特征剖析中的应用[J].烟草科技,2012,(10):36-40.LU Longjian,CHEN Lei,YU Ling,et al.Application of Multiple Factor Analysis(MFA)in Cigarettes Style Character Analyzing[J].Tobacco Science&Technology,2012,(10):36-40.
[5]常爱霞,张建平,杜咏梅,等.烤烟香型相关化学成分主导的不同产区烟叶聚类分析[J].中国烟草学报,2010,16(2):14-19.CHANG Aixia,ZHANG Jianping,DU Yongmei,et al.Cluster analysis of flue-cured tobacco leaves from different growingareas according to the chemical components correlating with aroma types[J].Acta Tabacaria Sinica,2010,16(2):14-19.
[6]谢剑平,赵明月,吴鸣,等.白肋烟重要香味物质组成分析的研究[J].烟草科技,2002(10):3-16.XIE Jianping,ZHAO Mingyue,WU Ming,et al.Studies on Some Important Aroma Compositions in Burley Tobacco[J].Tobacco Science&Technology,2002,(10):3-16.
[7]刘百战,宗若雯,岳勇,等.国内外部分白肋烟香味成分的对比分析[J].中国烟草学报,2000,6(2):1-5.LIU Baizhan,ZONG Ruowen,YUE Yong,et al.Comparison of aroma and flavor constituents of some domesticand foreign burley tobacco[J].Acta Tabacaria Sinica,2000,6(2):1-5.
[8]邵岩,宋春满,邓建华,等.云南与津巴布韦烤烟致香物质的相似性分析[J].中国烟草学报,2007,14(4):19-25.SHAO Yan,SONG Chunman,DENG Jianhua,et al.Similarity analysis of aromatic compounds between flue-curedtobacco leaves from Yunnan and Zimbabwei[J].Acta Tabacaria Sinica,2007,14(4):19-25.
[9]李伟,陈江华,詹军,等.烤烟香型间致香物质组成比例及其差异分析[J].中国烟草学报,2013,19(2):1-6.LI Wei,CHEN Jianghua,ZHAN Jun,et al.Differential analysis of aroma component proportion invarious aroma style flue-cured tobacco leaves[J].Acta Tabacaria Sinica,2013,19(2):1-6.
[10]杜咏梅,张建平,王树声,等.主导烤烟香型风格及感官质量差异的主要化学指标分析[J].中国烟草科学,2010,31(5):7-12.DU Yongmei,ZHANG Jianping,WANG SHusheng,et al.Major Chemical Indices Leading the Difference among Different Flavor Typesand Sensory Quality Grades of Flue-cured Tobacco[J].Chinese Tobacco Science,2010,31(5):7-12.
[11]詹军,周芳芳,邓国宾,等.基于化学成分和致香物质的烤烟上部烟叶香型判别分析[J].湖南农业大学学报:自然科学版,2013,39(3):232-241.ZHAN Jun,ZHOU Fangfang,DENG Guobin,et al.Discriminant analysis of aroma types of upper leaf in flue-cured tobaccobased on chemical constituents and aroma components[J].Journal of Hunan Agricultural University(Natural Sciences),2013,39(3):232-241.
[12]李雪君,郭芳阳,李耀宇,等.浓香型风格烤烟品种的筛选研究[J].河南农业科学,2010(11):45-49.LI Xuejun,GUO Fangyang,LI Yaoyu,et al.Screening of full aroma type Tobacco Varieties[J].Journal of Henan Agricultural Sciences,2010,(11):45-49.
[13]李宏光,周玲红,罗经仁.湖南浓香型特色烟叶品种筛选研究[J].作物研究,2013,27(6):568-571.LI Hongguang,ZHOU Linghong,LUO Jingren.Screening of full aroma type tobacco varieties in Hunan Luzhou Features[J].Corp Research,2013,27(6):568-571.
[14]唐远驹.关于烤烟香型问题的探讨[J].中国烟草科学,2011,32(3):1-7.TANG Yuanju.On Aroma Type of Flue-cured Tobacco[J].Chinese Tobacco Science,2011,32(3):1-7.
[15]王文胜,马戎.浓香型产区烟叶主要化学成分与风格品质特色及其关系研究[J].中国烟草科学,2013,34(5):28-32.WANG Wensheng,MA Rong.Major Chemical Components and Quality and Style and their Relationships in Full Flavor Tobacco Growing Regions[J].Chinese Tobacco Science,2013,34(5):28-32.
[16]何晓群.多元统计分析[M].北京:中国人民大学出版社,2012:143-154.HE Xiaoqun.Multivariate Statistical Analysis[M].Beijing:China Renmin University Press,2012:143-154.
[17][美]约翰逊,威克恩著,陆璇译.实用多元统计分析[M].北京:清华大学出版社,2001:103-17.Johnson R A,Wichern D W.Practical multivariate statistical analysis[M].Beijing:Tsinghua University Press,2001:103-17.
[18]Peedin G F,Effects of nitrogen rate and ripeness at harvest on some agronomic and chemical characteristics of flue-cured tobacc[C].Coresta,1995,1.
[19]Cai Jibao,Liu Baizhan,Ling Ping,et al.Analysis of freeand bound volatiles by gas chromatography and gaschromatography-mass spectrometry[J].J Chromatogr A,2002,947(2):267-275.
[20]李兴波,闫克玉,丁海燕,等.河南烤烟(40级)细胞壁物质含量及其规律性研究[J].郑州轻工业学院学报,1999,14(3):27-30.LI Xingbo,YAN Keyu,DING Haiyan,et al.Henan flue-cured tobacco(40)and regularity of cell wall material content[J].Journal of Zhengzhou Institute of Light Industry,1999,14(3):27-30.
[21]YC/T 162-2011烟草及烟草制品氯的测定连续流动法[s].YC/T 162-2011Tobacco and tobacco products-Determination of chlorine-continuous flow method[s].
[22]YC/T 173-2003烟草及烟草制品钾的测定火焰光度法[s].YC/T 173-2003Tobacco and tobacco products-Determination of potassium-Flame photometry[s].
[23]YC/T 159-2002烟草及烟草制品水溶性糖的测定连续流动法[s].YC/T 159-2002Tobacco and tobacco products-Determination of water-soluble sugarscontinuous flow method[s].
[24]YC/T 160-2002烟草及烟草制品总植物碱的测定连续流动法[s].YC/T 160-2002Tobacco and tobacco products-Determination of total alkaloids-continuous flow method[s].
[25]YC/T 161-2002烟草及烟草制品总氮的测定连续流动法[s].YC/T 161-2002Tobacco and tobacco products-Determination of total nitrogen-continuous flow method[s].
[26]YC/T251-2008烟草及烟草制品葡萄糖、果糖、蔗糖的测定离子色谱法[s].YC/T251-2008Tobacco and tobacco products-glucose,fructose-sucrose Ion Chromatography[s].
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