电沉积铁镍合金制备及其电磁屏蔽性能研究
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摘要
随着电子行业和通信行业的迅猛发展,电磁辐射已成为继大气污染、水质污染、噪音污染后的社会第四大公害。为减少电磁辐射,保证设备的可靠性,电磁屏蔽材料得到迅猛发展。铁镍合金由于其优异的磁性能在低频段得到广泛应用,随着电磁屏蔽材料朝着重量轻、厚度薄、频率宽的方向发展,铁镍合金由于整体重量较大限制其应用。本篇论文尝试铁镍合金以电沉积薄膜的形式应用于电磁屏蔽,实现器件功能一体化,满足复杂异形元器件和小型元器件的全表面覆盖,从而达到减重和全频段屏蔽的效果。主要内容如下：
1、介绍了电磁兼容发展、目前研究的电磁屏蔽材料和电磁屏蔽理论,从而引出研究电沉积铁镍合金薄膜应用于电磁屏蔽的意义。
2、详细研究了电沉积铁镍合金的工艺,发现调整溶液Fe2+和Ni2+离子比得到了不同铁镍百分比的镀层,并对电沉积参数对于铁镍合金组织结构的影响进行研究,确定电沉积设计铁镍合金成份的镀层的合理参数。
3、研究了不同铁镍合金成分复合材料磁性能,发现饱和磁化强度、矫顽力、最大磁导率等磁性参数均随着成分变化呈现出明显的规律性,并对该规律进行了解释,得到磁性能相对优异的铁镍合金成份镀层。
4、由于材料的磁导率和矫顽力均为组织敏感参数,通过热处理改变组织结构时,这些参数会发生明显的变化。研究300℃～900℃不同热处理温度对以铜为基体电沉积铁镍合金复合材料磁性能的影响,从而发现不同温度下磁性能变化的规律及其原因,得到优化的热处理工艺以及热处理工艺的设计原则。
5、成功将电沉积铁镍合金应用于电磁屏蔽,测量从静磁场到1.5GHz频率下铁镍合金电磁屏蔽性能,测量结果表明电沉积铁镍合金增加了低频段的电磁屏蔽性能,得到在全频段均有一定电磁屏蔽效能的电磁屏蔽复合材料。
6、以高导电铜箔和高导磁钴基非晶电磁屏蔽复合材料为基础,通过运用Schelkunoff传输线理论分析和实际测量结果的比较,从而定性了解结构对于电磁屏蔽性能的影响,为多层电磁屏蔽结构设计打下基础。
With the rapid development of information technology and electron technology, electromagnetic radiation which follows air pollution, water pollution and noise pollution has become the dangerous pollution to all the society. To decrease the electromagnetic radiation and ensure the reliability of equipments, the electromagnetic shielding materials have been developed in recent years. Fe-Ni alloy is widely applied in low frequency for its excellent magnetic performance. But Fe-Ni alloy is limited by its weight. So the electrodeposited Fe-Ni foils are studied to be applied in electromagnetic shielding to decrease the weight.
In charter1, the development of electromagnetic compatibility, the electromagnetic shielding materials and the related theory are introduced. And it is introduced why the electrodeposited Fe-Ni foils are applied in electromagnetic shielding.
In charter2, the processing parameters of electrodeposited Fe-Ni alloy are studied. Different composition electrodeposited FeNi foils can be obtained by adjusting the radio of Fe2+:Ni2+in the solution. The influence of electrodeposition processing parameters to the structure of Fe-Ni foils is studied. From the above study, the proper processing parameters of electrodeposition Fe-Ni foil are decided.
In charter3, the magnetic properties of different composition electrodeposited Fe-Ni foils are studied. The measurement results indicate that the variation of saturation magnetization, coercivity, and magnetic permeability with composition in foils follows some rules. From the rules, the electrodeposited Fe-Ni foils which process excellent magnetic performance are decided.
Because the magnetic permeability and coercivity are sensitive to the structure, these parameters vary with the structure which can be changed through heat treatment. The magnetic properties of the Fe-Ni foils which are electrodeposited on copper matrix vary with the different heat treatments. In charter4, the heat treatment process of electrodeposited Fe-Ni is studied. The magnetic properties of the Fe-Ni foils which are annealed between300℃and900℃are tested by LakeShore7410VSM. Some rules can be learned in the magnetic performance data. The measurement results indicate how to choose the better heat treatment process.
In charter5, the electrodeposited Fe-Ni alloy is applied to shield the electromagnetic radiation. The electromagnetic shielding performances of electrodeposited Fe-Ni alloy in the broadband-frequency range of0～1.5GHz are tested. The measurement results indicate that the electromagnetic shielding performances in low frequency are improved. The electromagnetic shielding composite materials which are used in all frequency can be made by electrodeposition FeNi.
In charter6, electromagnetic shielding composite materials which are made of copper foil and amorphous foil are studied through Schelkunoff transmission line theory. From the theory and measurement results, the influence of the structure to electromagnetic performance is studied.
1、介绍了电磁兼容发展、目前研究的电磁屏蔽材料和电磁屏蔽理论,从而引出研究电沉积铁镍合金薄膜应用于电磁屏蔽的意义。
2、详细研究了电沉积铁镍合金的工艺,发现调整溶液Fe2+和Ni2+离子比得到了不同铁镍百分比的镀层,并对电沉积参数对于铁镍合金组织结构的影响进行研究,确定电沉积设计铁镍合金成份的镀层的合理参数。
3、研究了不同铁镍合金成分复合材料磁性能,发现饱和磁化强度、矫顽力、最大磁导率等磁性参数均随着成分变化呈现出明显的规律性,并对该规律进行了解释,得到磁性能相对优异的铁镍合金成份镀层。
4、由于材料的磁导率和矫顽力均为组织敏感参数,通过热处理改变组织结构时,这些参数会发生明显的变化。研究300℃～900℃不同热处理温度对以铜为基体电沉积铁镍合金复合材料磁性能的影响,从而发现不同温度下磁性能变化的规律及其原因,得到优化的热处理工艺以及热处理工艺的设计原则。
5、成功将电沉积铁镍合金应用于电磁屏蔽,测量从静磁场到1.5GHz频率下铁镍合金电磁屏蔽性能,测量结果表明电沉积铁镍合金增加了低频段的电磁屏蔽性能,得到在全频段均有一定电磁屏蔽效能的电磁屏蔽复合材料。
6、以高导电铜箔和高导磁钴基非晶电磁屏蔽复合材料为基础,通过运用Schelkunoff传输线理论分析和实际测量结果的比较,从而定性了解结构对于电磁屏蔽性能的影响,为多层电磁屏蔽结构设计打下基础。
With the rapid development of information technology and electron technology, electromagnetic radiation which follows air pollution, water pollution and noise pollution has become the dangerous pollution to all the society. To decrease the electromagnetic radiation and ensure the reliability of equipments, the electromagnetic shielding materials have been developed in recent years. Fe-Ni alloy is widely applied in low frequency for its excellent magnetic performance. But Fe-Ni alloy is limited by its weight. So the electrodeposited Fe-Ni foils are studied to be applied in electromagnetic shielding to decrease the weight.
In charter1, the development of electromagnetic compatibility, the electromagnetic shielding materials and the related theory are introduced. And it is introduced why the electrodeposited Fe-Ni foils are applied in electromagnetic shielding.
In charter2, the processing parameters of electrodeposited Fe-Ni alloy are studied. Different composition electrodeposited FeNi foils can be obtained by adjusting the radio of Fe2+:Ni2+in the solution. The influence of electrodeposition processing parameters to the structure of Fe-Ni foils is studied. From the above study, the proper processing parameters of electrodeposition Fe-Ni foil are decided.
In charter3, the magnetic properties of different composition electrodeposited Fe-Ni foils are studied. The measurement results indicate that the variation of saturation magnetization, coercivity, and magnetic permeability with composition in foils follows some rules. From the rules, the electrodeposited Fe-Ni foils which process excellent magnetic performance are decided.
Because the magnetic permeability and coercivity are sensitive to the structure, these parameters vary with the structure which can be changed through heat treatment. The magnetic properties of the Fe-Ni foils which are electrodeposited on copper matrix vary with the different heat treatments. In charter4, the heat treatment process of electrodeposited Fe-Ni is studied. The magnetic properties of the Fe-Ni foils which are annealed between300℃and900℃are tested by LakeShore7410VSM. Some rules can be learned in the magnetic performance data. The measurement results indicate how to choose the better heat treatment process.
In charter5, the electrodeposited Fe-Ni alloy is applied to shield the electromagnetic radiation. The electromagnetic shielding performances of electrodeposited Fe-Ni alloy in the broadband-frequency range of0～1.5GHz are tested. The measurement results indicate that the electromagnetic shielding performances in low frequency are improved. The electromagnetic shielding composite materials which are used in all frequency can be made by electrodeposition FeNi.
In charter6, electromagnetic shielding composite materials which are made of copper foil and amorphous foil are studied through Schelkunoff transmission line theory. From the theory and measurement results, the influence of the structure to electromagnetic performance is studied.
引文
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