豆腐皮废甜浆中大豆低聚糖的分离纯化研究
|
摘要
近年来,随着科学技术的不断发展,低聚糖的生理功能越来越受到广大学者的关注。大豆低聚糖是大豆籽粒中含有的可溶性寡糖的总称,占大豆中总碳水化合物的7-10%。研究发现大豆低聚糖的摄入对于调整肠道菌群平衡、预防许多疾病、增强机体免疫力、延缓衰老等有着重要的作用,研究认为大豆低聚糖的主要作用在于促进双歧杆菌的增殖。有人认为,低聚糖摄入人体后会引起隔气、肠鸣、腹痛等肠胃胀气现象,然而现代安全性检验证明大豆低聚糖不是引起胀气的直接原因,食用大豆低聚糖具有良好的安全性。
在豆腐皮的生产过程中,大豆经浸泡、磨浆、过滤和煮浆后,通过保温蒸发,表面结皮,每隔一定时间收获产品。随着豆腐皮的不断形成,留下粘稠状的浓浆,即甜浆。甜浆是豆腐皮生产过程的终端副产物,其中含有较高浓度的低聚糖。目前甜浆一般被用来做动物饲料;或者重新倒入煮浆池,与新鲜的豆浆一起保温揭皮,但是这样生产出来的豆腐皮质地较脆、易折断,且颜色褐黄,无光泽,膜也较厚,筋性不好。本研究的目的是系统探索从甜浆中提取大豆低聚糖的路线方案,对甜浆资源进行再利用,拓宽大豆低聚糖的生产途经,为工业上的进一步应用提供理论基础和指导。
本研究采用HPLC方法对豆腐皮生产过程中大豆低聚糖的物料平衡进行了跟踪测定。结果表明,低聚糖损失于浸泡阶段、过滤阶段、成皮阶段,损失的低聚糖含量分别为1.43%、48.5%、24.18%(重量比)。浸泡对低聚糖含量的影响不大,蔗糖、棉子糖、水苏糖分别损失0.91%、0.31%和0.21%;过滤是导致低聚糖损失的重要阶段,蔗糖、棉子糖和水苏糖损失量分别占大豆中低聚糖总量的21.68%、10.76%、16.06%,成品保留有原料中14.66%的低聚糖,副产品甜浆含有原料中11.23%的低聚糖,是一种十分有潜力的大豆低聚糖提取来源。
本研究系统分析了工厂采样甜浆的成分。结果显示:总糖占干重的50%以上,其中大部分物质是低聚糖,蔗糖、棉子糖、水苏糖浓度分别为51.42、6.36、34.16 mg/ml,占甜浆干重的40%左右;可溶性蛋白质占甜浆干重的近17%,功能性物质如总黄酮和皂苷含量浓度分别为0.07、0.5 mg/ml,分别占甜浆干重的0.03%、0.22%。SDS-PAGE电泳图谱显示,主要的蛋白带有9条,其分子量大小分别为:76.36、50.37、41.35、37.44、27.14、25.78、19.94、17.62、13.64 kDa。甜浆成分的分析表明,功能性低聚糖含量远远高于大豆乳清废水。从甜浆中分离提取大豆低聚糖,得率和综合能耗可能远低于以乳清废水等为原料的提取工艺。
采用PES膜对大豆低聚糖粗提液进行超滤研究。要保证超滤的正常运行,甜浆溶液必须经过适当的前处理。结果表明:pH值为4.5、温度为70℃、加热5 min、CaCl_2浓度为10%是最佳的前处理方式。经过前处理的甜浆溶液中蛋白浓度降到3.99 mg/ml,蛋白质的去除率达到89%以上。超滤单因素实验采用MWCO 10000 kDa的PES超滤膜进行。结果表明,甜浆中大豆低聚糖的提取最佳方案为:压力1.75Ba,超滤温度为45℃,pH值7.0。正交试验表明,MWCO对蛋白质去除率和低聚糖保留率影响最大。对于蛋白质来说,MWCO为3000 kDa的膜蛋白质去除率最高,但是低聚糖透过率和渗透通量却处于所有实验中的最低水平;而MWCO为10000 kDa的膜低聚糖透过率最大,且渗透通量最高,蛋白质截留率偏低。50℃超滤温度对二者都比较适宜。综合渗透通量、膜衰减系数、蛋白质截留率和低聚糖透过率四方面因素考虑,认为最佳操作条件为:操作压力为1.5 Ba、温度为50℃、pH值为7.0,膜的截留分子量为10000 kDa。通过这样的操作可以截留73%的蛋白质,低聚糖透过率达到85%以上。
超滤后的大豆低聚糖溶液具有很高的含盐量,必须经过脱盐处理以达到大豆低聚糖产品的相关标准。一定浓度的NaCl溶液脱盐实验证明本研究中所使用的电渗析器工作性能稳定。本实验所用的电渗析装置极限电流密度的经验模型表达式为:I_(lim)=4.13v~(0.112)c~(0.033)。电渗析单因素试验结果表明,大豆低聚糖溶液的最佳脱盐方案为:20 V左右的操作电压、60 L/h左右的流量、稀释15倍。正交实验确定了最佳工艺条件,即电压为20V、流量为60 L/h、稀释18倍。对低聚糖保留率影响最大的因素是电压,其次是流量,再次是稀释倍数。通过最佳的操作条件进行脱盐可以成功脱除大豆低聚糖溶液中95%以上盐类,保留90%左右的低聚糖。
大豆低聚糖粗提液具有很深的颜色,本研究采用树脂脱色法对其中的色素进行脱除。以静态吸附法从10种树脂中筛选了对大豆低聚糖粗溶液脱色效果较好树脂,并探讨了吸附动力学及其机制。大孔吸附树脂DM-130和AB-8具有较高吸附量,脱色率达到70%以上,解吸率近100%。与AB-8相比,DM-130对糖的吸附较小,是脱色的较合适树脂。温度对树脂脱色效果的影响结果表明,树脂对色素的吸附更容易在低温下发生,说明吸附过程是放热的、自发的。室温20℃是脱色效果较好的温度。当树脂-糖液比例在0.13g/ml左右时可以达到较高的脱色率,超过这个比例时脱色率变化不明显。树脂对色素的吸附等温线更符合Freundlich等温线模型,说明树脂对色素的吸附是单层吸附,且树脂表面发生对多种成分的吸附。吸附动力学模型的分析表明,树脂对色素的吸附符合pseudo-second-order模型,说明吸附行为是化学吸附,也是限速步骤。粒子内扩散模型说明吸附过程是先发生了表面吸附,然后发生粒子内扩散。动态吸附实验认为最佳流速为1 ml/min,乙醇洗脱液的浓度为50%。
Recently, with the development of science and technology researchers have paid considerable interest in biological functions of oligosaccharides. Soybean oligosaccharides are soluble carbohydrate in soybean seeds and account for 7-10 % of the total carbohydrates in soybean. Researches have found that the intake of soybean oligosaccharides have important functions on the balance of microflora in intestine, prevention of many illness, enhancing body immunity, prevention of aging, etc. This was attributed by some researchers to promotion of bifidobacterium proliferation by soybean oligosaccharides. Researches had tested that oligosaccharides led to flatus and bellyache. However moden safe tests have shown that soybean oligosaccharides is not the direct reason of flatus and it is safe to take soybean oligosaccharides.
The production of soybean sheet from soybean follows a traditional process: After soaking milling, filtering, and boiling, soybean sheet is formed in the milk surface kept at certain temperature, and could be harvested at some time interval. With the harvest of soybean sheet thick and yellow slurry was left, namely the sweet slurry. Sweet slurry contains a considerable amount of soybean oligosaccharides. Normally it is used as feedstuff for animals or fed back to the soymilk pool to produce next batch of soybean sheet. However soybean sheet produced by this method was not in good merchant quality, for it was thick, easily broken, dark color with less luster. The aim of this research was to explore the method for separation and purification of soybean oligosaccharides from sweet slurry, thus to tap the potential of the sweet slurry resource and to provide alternatives for the production of soybean oligosaccharides. The research results may provide theory basis and guidence for value-added industry utilization of sweet slurry.
HPLC method was used in this research to trace the flow of soybean oligosaccharides during the production of soybean sheet. The results showed oligosaccharides losses were lost in soaking, blanding and filtrating, sheet forming stages, representing 1.43 %、48.5 %、24.18 % (on weight). Soaking did not show much influence on oligosaccharides content. Surcose, raffinose and stachyose losses were 0.91 %、0.31 % and 0.21 % respectively. Blanding and filtrating was the most important step for oligosaccharides losses compared with other steps. Surcose, raffinose and stachyose losses were 21.68 %、10.76 %、16.06 % relative to the total oligosaccharides in soybean seeds. The final product soybeansheet contains 14.66 % of the total oligosaccharides. Still 11.23 % of oligosaccharides were in the sweet slurry.
The component of the sweet slurry sampled from factory was analysed in this research. Results indicated that the total carbohydrate accounted for 50 % of the dry matter in sweet slurry and most of them were oligosaccharides, which represented 40 % of the total dry weight. Soluble protein accounted for 17 % of the total dry weight. Functional substance such as toal flavone and saponins concentration were 0.07 and 0.5 mg/ml respectively, representing 0.03 %、0.22 % (dry weight). SDS-PAGE result showed nine protein bands in the electrophoresis graph, and the molecule weight was 76.36、50.37s 41.35、37.44、27.14、25.78、19.94、17.62、13.64 kDa respectively. The analysis of the sweet slurry showed functional oligosaccharides content was much higher than that in soybean whey water. And the recovery percentage and total energy consumption were far lower than from the whey water.
UF experiment was conducted with PES membrane. The sweet slurry must be pretreated in order to guarantee the proper function of UF. The pretreatment experiment showed that the best pretreatment condition was pH 4.5, 70℃, heating 5 min and 10 % CaCl_2 concentration. After the pretreatment the protein concentration was dropped to 3.99 mg/ml and 89 % of protein was removed. Single factor trials used MWCO 10000 kDa PES membrane. The results showed that the optimum conditions for extracting oligosaccharides from sweet slurry were: 1.75 Ba TMP, 45℃temperature and pH 7.0. Orthogonal intersection trials revealed that MWCO became the major affecting factor on oligosaccharides retention and protein removal. Membrane with MWCO 3000 kDa was best for protein removal while oligosaccharides retention and permeate flux were the lowest in all trials. The oligosaccharides retention and permeate flux attained the highest level with MWCO 10000 kDa membrane, while the protein removal was relatively low. Temperature of 50℃was good for both protein removal and oligosaccharides retention. Considering the efficiency of protein removal, oligosaccharides retention, permeate flux and membrane decline, the optimum conditions for UF were 1.5 Ba pressure, 50℃temperature, pH 7.0, MWCO 10000 kDa. After this treatment 73 % of protein was removed and more than 85 % of oligosaccharides were retained.
The permeate fluid after UF contains large quantities of salts and must be removed to meet the oligosaccharides product standard. Electrodialysis (ED) was employed for the desalination process. NaCl solution was used first to test the stability of the ED apparatus. NaCl desalination trial showed that the ED setup was stable. The experience model for limited current density (LCD) of the ED apparatus employed in this experiment was I_(lim)=4.13 v~(0.112)c~(0.033). Single factor trial of ED showed that the optimum conditions for desalination was 20 V operating voltage, 60 L/h flow rate and diluting 15 times. Orthogonal intersection trials revealed that 20 V operating voltage, 60 L/h flow rate and diluting 18 times were the best condition for desalination and oligosaccharides retention. Operating voltage was the major affecting factor of oligosaccharides retention, then the flow rate and finally the diluting times. After ED more than 95 % salt in the crude soybean oligosaccharides solution was removed and 90 % of oligosaccharides was retained.
The crude soybean oligosaccharides solution was in dark color. Resins were used in the experiment to remove color. Static adsorption method was used to screen the best resin for decolorization from 10 resins and adsorption kinetic of coloured impurities onto resins was also studied. The results showed that more than 70 % of the pigments were removed in the final product by the macroporous adsorption resin DM-130 and AB-8 and the desorption was almost completely. Comparaed with AB-8, resin DM-130 had relatively less adsorption of sugar solution and it was the best resin for decoloration. The adsorption process was favored at lower temperature, indicating the process was exothermic and spontaneous. And room temperaure of about 20℃was better for decolorization. When the ratio of resin mass/oligosaccharides solution volumn was approximately 0.13 g/ml higher decolorization efficiency could be obtained in our experiment. Decolorization efficiency did not change much when resin mass-oligosaccharides solution volumn ratio was higher than 0.13 g/ml. The adsorption isotherm better agreed with the Freundlich model, indicating the monolayer sorption of coloured impurities onto macroporous resins and that the impurities were of multi-component nature rather than single component. Adsorption kinetic of coloured impurities onto resins fitted the pseudo-second-order kinetic model, this indicated that the adsorption process was chemical adsorption which was the speed limiting step. The intraparticle diffusion model showed that the adsorption process occurred by both surface sorption and intraparticle diffusion. The kinetic data showed the best flow speed was 1 ml/min, and the concentration of ethanol washing solution was 50 %.
在豆腐皮的生产过程中,大豆经浸泡、磨浆、过滤和煮浆后,通过保温蒸发,表面结皮,每隔一定时间收获产品。随着豆腐皮的不断形成,留下粘稠状的浓浆,即甜浆。甜浆是豆腐皮生产过程的终端副产物,其中含有较高浓度的低聚糖。目前甜浆一般被用来做动物饲料;或者重新倒入煮浆池,与新鲜的豆浆一起保温揭皮,但是这样生产出来的豆腐皮质地较脆、易折断,且颜色褐黄,无光泽,膜也较厚,筋性不好。本研究的目的是系统探索从甜浆中提取大豆低聚糖的路线方案,对甜浆资源进行再利用,拓宽大豆低聚糖的生产途经,为工业上的进一步应用提供理论基础和指导。
本研究采用HPLC方法对豆腐皮生产过程中大豆低聚糖的物料平衡进行了跟踪测定。结果表明,低聚糖损失于浸泡阶段、过滤阶段、成皮阶段,损失的低聚糖含量分别为1.43%、48.5%、24.18%(重量比)。浸泡对低聚糖含量的影响不大,蔗糖、棉子糖、水苏糖分别损失0.91%、0.31%和0.21%;过滤是导致低聚糖损失的重要阶段,蔗糖、棉子糖和水苏糖损失量分别占大豆中低聚糖总量的21.68%、10.76%、16.06%,成品保留有原料中14.66%的低聚糖,副产品甜浆含有原料中11.23%的低聚糖,是一种十分有潜力的大豆低聚糖提取来源。
本研究系统分析了工厂采样甜浆的成分。结果显示:总糖占干重的50%以上,其中大部分物质是低聚糖,蔗糖、棉子糖、水苏糖浓度分别为51.42、6.36、34.16 mg/ml,占甜浆干重的40%左右;可溶性蛋白质占甜浆干重的近17%,功能性物质如总黄酮和皂苷含量浓度分别为0.07、0.5 mg/ml,分别占甜浆干重的0.03%、0.22%。SDS-PAGE电泳图谱显示,主要的蛋白带有9条,其分子量大小分别为:76.36、50.37、41.35、37.44、27.14、25.78、19.94、17.62、13.64 kDa。甜浆成分的分析表明,功能性低聚糖含量远远高于大豆乳清废水。从甜浆中分离提取大豆低聚糖,得率和综合能耗可能远低于以乳清废水等为原料的提取工艺。
采用PES膜对大豆低聚糖粗提液进行超滤研究。要保证超滤的正常运行,甜浆溶液必须经过适当的前处理。结果表明:pH值为4.5、温度为70℃、加热5 min、CaCl_2浓度为10%是最佳的前处理方式。经过前处理的甜浆溶液中蛋白浓度降到3.99 mg/ml,蛋白质的去除率达到89%以上。超滤单因素实验采用MWCO 10000 kDa的PES超滤膜进行。结果表明,甜浆中大豆低聚糖的提取最佳方案为:压力1.75Ba,超滤温度为45℃,pH值7.0。正交试验表明,MWCO对蛋白质去除率和低聚糖保留率影响最大。对于蛋白质来说,MWCO为3000 kDa的膜蛋白质去除率最高,但是低聚糖透过率和渗透通量却处于所有实验中的最低水平;而MWCO为10000 kDa的膜低聚糖透过率最大,且渗透通量最高,蛋白质截留率偏低。50℃超滤温度对二者都比较适宜。综合渗透通量、膜衰减系数、蛋白质截留率和低聚糖透过率四方面因素考虑,认为最佳操作条件为:操作压力为1.5 Ba、温度为50℃、pH值为7.0,膜的截留分子量为10000 kDa。通过这样的操作可以截留73%的蛋白质,低聚糖透过率达到85%以上。
超滤后的大豆低聚糖溶液具有很高的含盐量,必须经过脱盐处理以达到大豆低聚糖产品的相关标准。一定浓度的NaCl溶液脱盐实验证明本研究中所使用的电渗析器工作性能稳定。本实验所用的电渗析装置极限电流密度的经验模型表达式为:I_(lim)=4.13v~(0.112)c~(0.033)。电渗析单因素试验结果表明,大豆低聚糖溶液的最佳脱盐方案为:20 V左右的操作电压、60 L/h左右的流量、稀释15倍。正交实验确定了最佳工艺条件,即电压为20V、流量为60 L/h、稀释18倍。对低聚糖保留率影响最大的因素是电压,其次是流量,再次是稀释倍数。通过最佳的操作条件进行脱盐可以成功脱除大豆低聚糖溶液中95%以上盐类,保留90%左右的低聚糖。
大豆低聚糖粗提液具有很深的颜色,本研究采用树脂脱色法对其中的色素进行脱除。以静态吸附法从10种树脂中筛选了对大豆低聚糖粗溶液脱色效果较好树脂,并探讨了吸附动力学及其机制。大孔吸附树脂DM-130和AB-8具有较高吸附量,脱色率达到70%以上,解吸率近100%。与AB-8相比,DM-130对糖的吸附较小,是脱色的较合适树脂。温度对树脂脱色效果的影响结果表明,树脂对色素的吸附更容易在低温下发生,说明吸附过程是放热的、自发的。室温20℃是脱色效果较好的温度。当树脂-糖液比例在0.13g/ml左右时可以达到较高的脱色率,超过这个比例时脱色率变化不明显。树脂对色素的吸附等温线更符合Freundlich等温线模型,说明树脂对色素的吸附是单层吸附,且树脂表面发生对多种成分的吸附。吸附动力学模型的分析表明,树脂对色素的吸附符合pseudo-second-order模型,说明吸附行为是化学吸附,也是限速步骤。粒子内扩散模型说明吸附过程是先发生了表面吸附,然后发生粒子内扩散。动态吸附实验认为最佳流速为1 ml/min,乙醇洗脱液的浓度为50%。
Recently, with the development of science and technology researchers have paid considerable interest in biological functions of oligosaccharides. Soybean oligosaccharides are soluble carbohydrate in soybean seeds and account for 7-10 % of the total carbohydrates in soybean. Researches have found that the intake of soybean oligosaccharides have important functions on the balance of microflora in intestine, prevention of many illness, enhancing body immunity, prevention of aging, etc. This was attributed by some researchers to promotion of bifidobacterium proliferation by soybean oligosaccharides. Researches had tested that oligosaccharides led to flatus and bellyache. However moden safe tests have shown that soybean oligosaccharides is not the direct reason of flatus and it is safe to take soybean oligosaccharides.
The production of soybean sheet from soybean follows a traditional process: After soaking milling, filtering, and boiling, soybean sheet is formed in the milk surface kept at certain temperature, and could be harvested at some time interval. With the harvest of soybean sheet thick and yellow slurry was left, namely the sweet slurry. Sweet slurry contains a considerable amount of soybean oligosaccharides. Normally it is used as feedstuff for animals or fed back to the soymilk pool to produce next batch of soybean sheet. However soybean sheet produced by this method was not in good merchant quality, for it was thick, easily broken, dark color with less luster. The aim of this research was to explore the method for separation and purification of soybean oligosaccharides from sweet slurry, thus to tap the potential of the sweet slurry resource and to provide alternatives for the production of soybean oligosaccharides. The research results may provide theory basis and guidence for value-added industry utilization of sweet slurry.
HPLC method was used in this research to trace the flow of soybean oligosaccharides during the production of soybean sheet. The results showed oligosaccharides losses were lost in soaking, blanding and filtrating, sheet forming stages, representing 1.43 %、48.5 %、24.18 % (on weight). Soaking did not show much influence on oligosaccharides content. Surcose, raffinose and stachyose losses were 0.91 %、0.31 % and 0.21 % respectively. Blanding and filtrating was the most important step for oligosaccharides losses compared with other steps. Surcose, raffinose and stachyose losses were 21.68 %、10.76 %、16.06 % relative to the total oligosaccharides in soybean seeds. The final product soybeansheet contains 14.66 % of the total oligosaccharides. Still 11.23 % of oligosaccharides were in the sweet slurry.
The component of the sweet slurry sampled from factory was analysed in this research. Results indicated that the total carbohydrate accounted for 50 % of the dry matter in sweet slurry and most of them were oligosaccharides, which represented 40 % of the total dry weight. Soluble protein accounted for 17 % of the total dry weight. Functional substance such as toal flavone and saponins concentration were 0.07 and 0.5 mg/ml respectively, representing 0.03 %、0.22 % (dry weight). SDS-PAGE result showed nine protein bands in the electrophoresis graph, and the molecule weight was 76.36、50.37s 41.35、37.44、27.14、25.78、19.94、17.62、13.64 kDa respectively. The analysis of the sweet slurry showed functional oligosaccharides content was much higher than that in soybean whey water. And the recovery percentage and total energy consumption were far lower than from the whey water.
UF experiment was conducted with PES membrane. The sweet slurry must be pretreated in order to guarantee the proper function of UF. The pretreatment experiment showed that the best pretreatment condition was pH 4.5, 70℃, heating 5 min and 10 % CaCl_2 concentration. After the pretreatment the protein concentration was dropped to 3.99 mg/ml and 89 % of protein was removed. Single factor trials used MWCO 10000 kDa PES membrane. The results showed that the optimum conditions for extracting oligosaccharides from sweet slurry were: 1.75 Ba TMP, 45℃temperature and pH 7.0. Orthogonal intersection trials revealed that MWCO became the major affecting factor on oligosaccharides retention and protein removal. Membrane with MWCO 3000 kDa was best for protein removal while oligosaccharides retention and permeate flux were the lowest in all trials. The oligosaccharides retention and permeate flux attained the highest level with MWCO 10000 kDa membrane, while the protein removal was relatively low. Temperature of 50℃was good for both protein removal and oligosaccharides retention. Considering the efficiency of protein removal, oligosaccharides retention, permeate flux and membrane decline, the optimum conditions for UF were 1.5 Ba pressure, 50℃temperature, pH 7.0, MWCO 10000 kDa. After this treatment 73 % of protein was removed and more than 85 % of oligosaccharides were retained.
The permeate fluid after UF contains large quantities of salts and must be removed to meet the oligosaccharides product standard. Electrodialysis (ED) was employed for the desalination process. NaCl solution was used first to test the stability of the ED apparatus. NaCl desalination trial showed that the ED setup was stable. The experience model for limited current density (LCD) of the ED apparatus employed in this experiment was I_(lim)=4.13 v~(0.112)c~(0.033). Single factor trial of ED showed that the optimum conditions for desalination was 20 V operating voltage, 60 L/h flow rate and diluting 15 times. Orthogonal intersection trials revealed that 20 V operating voltage, 60 L/h flow rate and diluting 18 times were the best condition for desalination and oligosaccharides retention. Operating voltage was the major affecting factor of oligosaccharides retention, then the flow rate and finally the diluting times. After ED more than 95 % salt in the crude soybean oligosaccharides solution was removed and 90 % of oligosaccharides was retained.
The crude soybean oligosaccharides solution was in dark color. Resins were used in the experiment to remove color. Static adsorption method was used to screen the best resin for decolorization from 10 resins and adsorption kinetic of coloured impurities onto resins was also studied. The results showed that more than 70 % of the pigments were removed in the final product by the macroporous adsorption resin DM-130 and AB-8 and the desorption was almost completely. Comparaed with AB-8, resin DM-130 had relatively less adsorption of sugar solution and it was the best resin for decoloration. The adsorption process was favored at lower temperature, indicating the process was exothermic and spontaneous. And room temperaure of about 20℃was better for decolorization. When the ratio of resin mass/oligosaccharides solution volumn was approximately 0.13 g/ml higher decolorization efficiency could be obtained in our experiment. Decolorization efficiency did not change much when resin mass-oligosaccharides solution volumn ratio was higher than 0.13 g/ml. The adsorption isotherm better agreed with the Freundlich model, indicating the monolayer sorption of coloured impurities onto macroporous resins and that the impurities were of multi-component nature rather than single component. Adsorption kinetic of coloured impurities onto resins fitted the pseudo-second-order kinetic model, this indicated that the adsorption process was chemical adsorption which was the speed limiting step. The intraparticle diffusion model showed that the adsorption process occurred by both surface sorption and intraparticle diffusion. The kinetic data showed the best flow speed was 1 ml/min, and the concentration of ethanol washing solution was 50 %.
引文
Abdel-Gawad AS. Effect of domestic processing on oligosaccharide content of some dry legume seeds. Food Chemistry, 1993, 46: 25-31.
Achaerandio I, Guell C, Lopez F. Continuous vinegar decolorization with exchange resins. J Food Eng, 2002,51:311-317.
Adlerberth I. The establishment of a normal intestinal microflora in the newborn infant. In Hanson LA, Yolken RB. (Eds.), Probiotics, other nutritional factors, and intestinal flora. 42nd Nestle nutrition workshop. New York: Lippincot Williams & Wilkins. 1997: 63-78.
Aimar P, Baklouti S, Sanchez V et al. membrane-solute interactions: influence on pure solvent transfer during ultrafiltration. J Membr Sci, 1986, 29: 207-224.
Akinyele 10, Akinlosotu A. Effect of soaking, dehulling and fermentation on the oligosaccharides and nutrient content of cowpeas (Vigna unguiculata). Food Chem, 1991, 41: 43-53.
Akoum O, Richfield D, Jaffrin MY, et al. Recovery of trypsin inhibitor by soy milk ultrafiltration using a rotating disk system. Desalination, 2006, 191: 438-445.
Alander M, Matto J, Kneifel W, et al. Effect of galacto-oligosaccharide supplementation on human faecal microflora and on survival and persistence of Bifidobacterium lactis Bb-12 in the gastrointestinal tract. Int Dairy J, 2001, 11: 817-825.
Alibhai Z, Mondor M, Moresoli C, et al. Production of soy protein concentrates/isolates: traditional and membrane technologies. Desalination, 2006, 191: 51-358.
Al-Kaisey MT, Alwan AKH, Mohammad MH, et al. Effect of gamma irradiation on antinutritional factors in broad bean. Radiat Phys Chem, 2003, 67: 493-496.
Andersson HB, Ellegard LH, Bosaeus IG. Nondigestibility characteristics of inulin and oligofructose in humans. J Nutr, 1999, 129: 1428S-30S.
Archer S, Meng S, Wu J, et al. Butyrate inhibits colon carcinoma cell growth through two distinct pathways. Surgery, 1998,124:248-253.
Atungulu G, Koide S, Sasaki S, et al. Ion-exchange membrane mediated electrodialysis of scallop broth: Ion, free amino acid and heavy metal profiles. J Food Eng, 2007, 78: 1285-1290.
Ayala-Bribiesca E, Pourcelly G, Bazinet L. Nature identification and morphology characterization of cation-exchange membrane fouling during conventional electrodialysis. J Colloid Interface Sci, 2006, 300: 663-672.
Baltrusaityte V, Venskutonis PR, Ceksteryte V. Radical scavenging activity of different floral origin honey and beebread phenolic extracts. Food Chem, 2007, 101: 502-514.
Bau HM, Villanme C, Nicolos JP, et al. Effect of germination on chemical composition, biochemical constitutes and antinutritional factors of soy bean (Glycine max) seeds. J Sci Food Agr, 1997, 73: 1-9.
Bento LSM. Sugar decolorization by ion-exchange resins with regenerant recovery. Int Sugar J, 1990, 92: 116-125.
Bento LSM. Proc. AVH Assoc.-6th Symposium Reins, 1999: 23-27.
Beolchini F, Veglio F, Barba D. Microflltration of bovine and ovine milk for the reduction of microbial content in a tubular membrane: a preliminary investigation. Desalination, 2004, 161: 251-258.
Berdous D, Akretche DE, et al. Recoveryof metals by Donnan dialysis with ion exchange textiles. Desalination, 2002, 144: 212-218.
Bielecka M, Biedrzycka E, Majkowska A, et al. Effect of non-digestible oligosaccharides on gut microecosystem in rats. Food Res Int, 2002,35: 139-144.
Bland EJ, Keshavarz T, Bucke C. The influence of small oligosaccharides on the immune system. Carbohydr Res, 2004, 339: 1673-1678.
Boniardi N, Rota R, Nano G, et al. Analysis of the sodium lactate concentration process by electrodialysis. Sep Technol, 1996, 6(1): 43-54.
Bouhidel KE, Lakehal A. Influence of voltage and flow rate on electrodeionization (EDI) process efficiency. Desalination, 2006, 193: 411-421.
Brand J, Bull S, Miller J, et al. The oligosaccharide composition of human milk: temporal and individual variations in monosaccharide components. J Pediatr Gastroenterol Nutr, 1994, 19(4): 371-6.
Brassart D, Schiffrin EJ. The use of probiotics to reinforce mucosal defence mechanisms. Trends Food Sci Technol, 1997, 8:321-326.
Buedo AP, Elustondo MP, Urbicain MJ. Amino acid loss in peach juice concentrate during storage. Innovative Food Sci Emerging Technol, 2001, 1: 281-288.
Cai BX. Study of membrane separation processes of a betaine-like medicinal solution. Desalination, 2006, 191:432-437.
Calle EV, Rusles J, Dornierb M, et al. Deacidification of the clarified passion fruit juice. Desalination, 2002, 149:357-361.
Carabasa M, Ibarz A, Garza S et al. Removal of Dark Compounds from Clarified Fruit Juices by Adsorption Processes. J Food Eng, 1998, 37: 25-41.
Cassano A, Donato L, Drioli E. Ultrafiltration of kiwifruit juice: Operating parameters, juice quality and membrane fouling. J Food Eng, 2007, 79: 613-621.
Chabani M, Amrane A, Bensmaili A. Kinetic modelling of the adsorption of nitrates by ion exchange resin. Chemical Eng J, 2006, 125: 111-117.
Chairat M, Rattanaphani S, Bremner JB, et al. Adsorption kinetic study of lac dyeing on cotton. Dyes Pigments, 2008, 76: 435-439.
Chaturvedi P, Warren CD, Ruiz-Palacios GM, et al. Milk oligosaccharide profiles by reversed-phase HPLC of their perbenzoylated derivatives. Anal Biochem, 1997,251: 89-97.
Cheang B, Zydney AL. A two-stage ultrafiltration process for fractionation of whey protein isolate. J Membr Sci, 2004, 231: 159-167.
Cheryan M. Ultrafiltration and Microfiltration Handbook, CRC Press, Boca Raton, FL, 1998.
Chitra US, Rao PV. Phytic acid, in vitro protein digestibility, dietary fiber and minerals of pulses as influenced by processing methods. Plant Foods Human Nutr, 1996,47: 163-172.
Chiu TY, Lara Dominguez MV, James AE. Critical flux and rejection behaviour of non- circular- channelled membranes Influence of some operating conditions. Sep Purif Technol, 2006, 50: 212-219.
Choi EY, Choi JH, Moon SH. An electrodialysis model for determination of the optimal current density. Desalination, 2002, 153: 399-404.
Chou CC, Hou JW. Growth of bifidobacteria in soymilk and their survival in the fermented soymilk drinkduring storage. Int J Food Microbiol, 2000, 56: 113-121.
Chumchuere S, Robinson RK. Selection of starter cultures for the fermentation of soya milk. Food Microbiol, 1999, 16: 129-137.
Ciucanu I, Caprita R. Per-O-methylation of neutral carbohydrates directly from aqueous samples for gas chromatography and mass spectrometry analysis. Anal Chim Acta, 2007, 585: 81-85.
Coppa G, Gabrielli O, Giorgi P, et al. Preliminary study of breastfeeding and bacterial adhesion to uroepithelial cells. Lancet, 1990, 335: 569-571.
Costa AR, de Pinho MN. Comparison of the performance of ultrafiltration and nanofiltration in surface water treatment. Desalination, 2006, 199: 73-75.
Crittenden RG, Playne MJ. Production, properties and applications of food-grade oligosaccharides. Trends Food Sci Technol, 1996, 7: 353-361.
Cui ZW, Sun LJ, Chen W, et al. Preparation of dry honey by microwave-vacuum drying. J Food Eng, 2008, 84:582-590.
Cummings JH, Englyst HN. Fermentation in the human large intestine and the available substrates. Am J Clin Nutr, 1987,45: 1243-1255.
Cummings JH, Macfarlane GT. The control and consequences of bacterial fermentation in the human colon. J Appl Bacteriol, 1991, 70: 443-459.
Cummings JH, Roberfroid MB and members of the Paris Carbohydrate Group, et al. A new look at dietary carbohydrate: chemistry, physiology and health. Eur J Clin Nutr, 1997, 51: 417-423.
Czermak P, Ebrahimi M, Grau K, et al. Membrane-assisted enzymatic production of galactosyl- oligosaccharides from lactose in a continuous process. J Membr Sci, 2004, 232: 85-91.
Deguchi Y, Matsumoto K, Ito T and Watanuki, M. Effects of P, 1-4 galactooligosaccharides administration on defecation of healthy volunteers with constipation tendency. Japanese J Nutr, 1997, 55: 13-22.
De Fatima Viana S, Monteze Guimaraes V, 1 Chamel Jose. Hydrolysis of oligosaccharides in soybean flour by soybean α-galactosidase. Food Chem, 2005, 93: 665-670.
Egounlety M, Aworh, OC. Effect of soaking, dehulling, cooking and fermentation with Rhizopus oligosporus on the oligosaccharides, trypsin inhibitor, phytic acid and tannins of soybean (Glycine max Merr.), cowpea (Vigna unguiculata L. Walp) and groundbean (Macrotyloma geocarpa Harms). J Food Eng, 2003, 56: 249-254.
Ekvall J, Stegmark R, Nyman M. Content of low molecular weight carbohydrates in vining peas (Pisumsativum) related to harvest time, size and brine grade. Food Chem, 2006, 94: 513-519.
Elmidaoui A, Chay L, Tahaikt M, et al. Demineralisation for beet sugar solutions using an electrodialysis pilot plant to reduce melassigenic ions. Desalination, 2006, 189: 209-214.
Engfer MB, Stahl B, Finke B, et al. Human milk oligosaccharides are resistant to enzymatic hydrolysis in the upper gastrointestinal tract. Am J Clin Nutr, 2000, 71(6): 1589- 96.
Enevoldsen AD, Hansen E, Jonsson G. Enzyme recovery by crossflow electro-ultrafiltration. Desalination, 2006, 199:55-56.
Fane AG, Fell CJD, McDonogh RM et al. the fouling of membranes, 11~(th) Australasian Chemical Engineering Conference, Brisbane, 1983: 729-737. Fuller R, Gibson GR. Modification of the intestinal microflora using probiotics and prebiotics. Scandinavian J Gastroenterol, 1997, 32: 28-31.
Fishbein L, Kaplan M, Gough M. Fructo-oligosaccharides: a review. Vet Hum Toxicol, 1988, 30: 104-107.
Fourmentin S, Outirite M, Blach P, et al. Solubilisation of chlorinated solvents by cyclodextrin derivatives A study by static headspace gas chromatography and molecular modelling. J Haz Mater, 2007, 141: 92-97.
Freger V, Arnot TC, Howell JA. Separation of concentrated organic/inorganic salt mixtures by nanofiltration. J Membr Sci, 2000, 178: 185-193.
Frenzel 1, Holdik H, Stamatialis DF, et al. Chromic acid recovery by electro-electrodialysis I. Evaluation of anion-exchange membrane. J Membr Sci, 2005, 261: 49-57.
Frisa J, Price KR, Fenwick GR, et al. Improved method for the analysis of α-galactosides in pea seeds by capillary zone eletrophoresis comparation with high-performance liquid chromatography- triple - pulsed amperometric detection. J Chromatogr, 1996, 719: 213-219.
Fukumoto LR, Delaquis P, Girard B. Microfiltration and ultrafiltration ceramic membranes for apple juice clarification. J Food Sci, 1998, 63(5): 845-850.
Fukushima Y, Kawata Y, Hara H, et al. Effect of probiotic formula on intestinal immunoglobulin A production in healthy children. Int J Food Microbiol, 1998, 42: 39-44.
Fuller R, Gibson GR. Modification of the intestinal microflora using probiotics and prebiotics. Scand J Gastroenterol, 1997, 32 (Suppl): 28-31.
Garcia A, Alvarez S, Riera F. Sunflower oil miscella degumming with polyethersulfone membranes Effect of process conditions and MWCO on fluxes and rejections. J Food Eng, 2006, 74: 516-522.
Garcia Agudo JA, Garcia Cubero MT, Gonzalez Benito G, et al. Removal of coloured compounds from sugar solutions by adsorption onto anionic resins: equilibrium and kinetic study. Sep Purif Technol, 2002, 29: 199-205.
Gennadios A, McHugh TH, Weller CL et al. Edible coatings and films based on proteins. In: Krochta JM, Baldwin EA and Nisperos-Carriedo M (Eds.), Edible coatings and films to improve food quality. Technomic Publishing Company, Lancaster, PA, 1994, 201-277.
Gesan-Guiziou G, Jimenez A, Arcelin C. Cake properties in dead-end ultrafiltration of casein micelles determination of critical operating conditions. Desalination, 2006, 199: 20-22.
Gibson GR, Roberfroid MB. Dietary modulation of the human colonic microbiota: introducing the concept ofprebiotics. JNutr, 1995, 125: 1401-1412.
Gode F, Pehlivan E. Removal of chromium (III) from aqueous solutions using Lewatit S 100: The effect of pH, time, metal concentration and temperature. J Haz Mat, 2006, B136: 330-337.
Godevac D, Vujisic L, Mojovic M, et al. Evaluation of antioxidant capacity of Allium ursinum L. volatile oil and its effect on membrane fluidity. Food Chem, 2008, 107: 1692-1700.
Gomes A, Malcata F. Bifidobacterium spp. and Lactobacillus acidophilus: Biological, biochemical, technology and therapeutical properties relevant for use as probiotics. Trends Food Sci Technol, 1999, 10: 139-157.
Gong Y, Dai LM, Wang XL, et al. Effects of transport properties of ion-exchange membranes on desalination of 1,3-propanediol fermentation broth by electrodialysis. Desalination, 2006, 191: 193-199.
Gong Y, Tang Y, Wang XL, et al. The possibility of the desalination of actual 1,3-propanediol fermentation broth by electrodialysis. Desalination, 2004, 161: 169-178.
Gopal PK, Prasad J, Gill HS. Effects of the consumption of Bifidobacterium lactis HN019 (DR10TM) and galacto-oligosaccharides on the microflora of the gastrointestinal tract in human subjects. Nutr Res, 2003, 23:1313-1328.
Gote M, Umalkar H, Khan I, et al. Thermostable α-galactosidase from Bacillus stearothermophilus (NCIM 5146) and its application in the removal of flatulence causing factors from soymilk. Proc Biochem, 2004, 39: 1723-1729.
Goulas AK, Kapasakalidis PG, Sinclair HR, et al. Purification of oligosaccharides by nanofiltration. J Membr Sci, 2002, 209: 321-335.
Gokmen V, Serpen A. Equilibrium and kinetic studies on the adsorption of dark colored compounds from apple juice using adsorbent resin. J Food Eng, 2002, 53: 221-227.
Grandison AS. Application of ion-exchange in food processing. Food Technol Int Europe, 1994: 53-57.
Grebenyuk VD, Chebotareva RD, Peters S, et al. Surface modification of anion-exchange electrodialysis membranes to enhance anti-fouling characteristics. Desalination, 1998, 115: 313-329.
Guadix A, S(?)rensen E, Papageorgiou LG, et al. Optimal design and operation of continuous ultrafiltration plants. J Membr Sci, 2004, 235: 131-138.
Guigoz Y, Rochat F, Perruisseau-Carrier G, et al. Effects of oligosaccharide on the faecal flora and nonspecific immune system in elderly people. Nutr Res, 2002, 22: 13-25.
Guimaraes VM, De Rezende ST, Moreira MA, et al. Characterization of a-galactosidases from germinating soybean seed and their use for hydrolysis of oligosaccharides. Phytochem, 2001, 58: 67-73.
Gupta, Y. P. Nutritive valueof soybean. Int J Tropical Agric, 1987, 5: 247-279.
Hamada JS. Large-scale high-performance liquid chromatography of enzymes for food applications. J Chromatogr, 1997,760:81-87.
Hameed BH, Ahmad A A, Aziz N. Isotherms, kinetics and thermodynamics of acid dye adsorption on activated palm ash. Chem Eng J, 2007, 133: 195-203.
Herman EM, Shannon L M. Accumulation and subcellular localization of a-galactosidase hemagglutinin in developing soybean cotyledons. Plant Physiol, 1985, 77: 886-890.
Hemwimon S, Pavasant P, Shotipruk A. Microwave-assisted extraction of antioxidative anthraquinones from roots of Morinda citrifolia. Sep Purif Technol, 2007, 54: 44-50.
Hidaka H, Tashiro Y, Eida T. Proliferation of bifidobacteria by oligosaccharides and their useful effect on human health. Bifidobact Microflora, 1991, 10(1): 65 - 79.
Hirata M, Gao M, Toorisaka et al. Production of lactic acid by continuous electrodialysis fermentation with a glucose concentration controller. Biochemical Eng J, 2005, 25: 159-163.
Ho CC, Zydney AL. A combined pore blockage and cake filtration model for protein fouling during microfiltration. J Colloid Interf Sci, 2000, 232: 389-399.
Ho YS, Mckay G. Pseudo-second-order model for sorption process. Process Biochem, 1999, 34: 451-465.
Houdijk JGM, Bosch MW, Verstegen MWA, et al. Effects of dietary oligosaccharides on the growth performance and faecal characteristics of young growing pigs. Animal Feed Sci Technol, 1998, 71: 35-48.
Hwang KJ, Chou FY, Tung KL. Effects of operating conditions on the performance of cross-flow microfiltration of fine particle/protein binary suspension. J Membr Sci, 2006, 274: 183-191.
Hwang KJ, Yu YH, Lu WM. Cross-flow microfiltration of submicron microbial suspension. J Membr Sci, 2001,194:229-243.
Ishibashi N, Shimamura S. Bifidobacteria: Research and development in Japan. Food Technol, 1993, 6:126-136.
Iyer V, Salunkhe DK, Sathe SK, et al. Quick cooking of beans (Phaseolus vulgaris, L.): phytates, oligosaccharides, antienzymes. Quality Plant Foods Human Nutr, 1980, 30: 45-52.
Jensen PE, Ottosen LM, C Ferreira, et al. Kinetics of electrodialytic extraction of Pb and soil cations from a slurry of contaminated soil fines. J Hazardous Materials, 2006, 138(3): 493-499.
Jeon YJ, Kim SK. Production of chitooligosaccharides using an ultrafiltration membrane reactor and their antibacterial activity. Carbohydrate Polymers, 2000, 41: 133-141.
Kaneko T, Mori H, Iwata M, et al. Growth stimulator for bifidobacteria produced by Propionibacterium freudenreichii and several intestinal bacteria. J Dairy Sci, 1994, 77: 393-404.
KanthaD. Role of bifidobacteria in nutrition, medicine and technology. Nutr Res, 1999, 19(11): 1559-1597.
Kapiki A, Costalos C, Oikonomidou C, et al. The effect of a fructo-oligosaccharide supplemented formula on gut flora of preterm infants. Early Hum Dev, 2007, 83: 335-339.
Karthikeyan T, Rajgopal S, Miranda LR. Chromium (VI) adsorption from aqueous solution by Hevea Brasilinesissawdust activated carbon. J Haz Mat B, 2005, 124, 192-199.
Kim DW, Kim TS, Jeong YK, et al. Adsorption kinetics and behaviors of cellulase components on microcrystalline cellulose. J Ferment Bioeng, 1992, 73: 461-466.
Kim 1C, Kim JH, Lee KH, et al. Phospholipids separation (degumming) from crude vegetable oil by polyimide ultrafiltration membrane. J Membr Sci, 2002, 205: 113-123.
Kim JS, Laskowich ER, Arumugham RG, et al. Determination of saccharide content in pneumococcal polysaccharides and conjugate vaccines by GC-MSD. Anal Biochem, 2005, 347: 262-274.
Kim KJ, Fane AG, Fell CJD, et al. Fouling mechanisms of menbranes during protein ultrafiltration. J Membr Sci, 1992,68:79-91.
Kinsella JE. Functional properties of soy proteins. J Am Oil Chemists' Society 1979, 56: 242-258.
Krishna Kumar NS, Yea MK, Cheryan M. Ultrafiltration of soy protein concentrate: performance and modelling of spiral and tubular polymeric modules. J Membr Sci, 2004, 244: 235-242.
Krol JJ, Wessling M, Strathmann H, et al. Concentration polarization with monopolar ion exchange membranes: current-voltage curves and water dissociation. J Membr Sci, 1999, 162: 145-154.
Kuberkar VT, Davis RH. Microfiltration of protein-cell mixtures with crossflushing or backflushing. J Membr Sci, 2001, 183: 1-14.
Kumar KV, Kumaran A. Removal of methylene blue by mango seed kernel powder. Biochem Eng J, 2005, 27, 83-93.
Kunz C, Rudloff S. Biological functions of oligosaccharides in human milk. Acta Paediatr, 1993, 82:903-12.
Lacour S, Bollinger JC, Serpaud B, et al. Removal of heavy metals in industrial wastewaters byion- exchanger grafted textiles. Anal Chim Acta, 2001, 428: 121-132.
Lacour S, Serpaud B, Bollinger JC. Performance of ion-exchanger grafted textiles for industrial water treatment in dynamic reactors. Water Res, 2004, 38: 4045-4054.
Langmuir I. The adsorption of gases on plane surfaces of glass, mica and platinum. J American Chem Society, 1918, 40: 1361-1402.
Lasekan OO, Idowu MA, Lasekan W. Effect of germination and degree of grind (coarse/fine) on the extract and sugar contents of sorghum malts. Food chem, 1995, 53: 125-128.
Lee DN, Miranda MG, Merson RL. Scanning electron microscope studies of membrane deposits from whey ultrafiltration. J Food Technol, 1975,10: 139.
Lee H, Amy G, Cho J, et al. Cleaning strategies for flux recovery of an ultrafiltration membrane fouled by natural organic matter. Wat Res, 2001, 35(14): 3301-3308.
Lee HJ, Sarfert F, Strathmann H, et al. Designing of an electrodialysis desalination plant. Desalination,2002, 142:267-286.
Lee HJ, Strathmann H, Moon SH. Determination of the limiting current density in electrodialysis desalination as an empirical function of linear velocity. Desalination, 2006, 190: 43-50.
Lee HJ, Strathmann H, Moon SH. Determination of the limiting current density in electrodialysis desalination as an empirical function of linear velocity. Desalination, 2006,190: 43-50.
Li H, Bo C, Zhang Z et al. Focused microwave-assisted solvent extraction and HPLC determination of effective constituents in Eucommiaulmodies Oliv.(E. ulmodies). Talanta, 2004, 63: 659-665.
Li ZY, Youravong W, H-Kittikun A. Separation of proteases from yellowWn tuna spleen by ultraWltration. Bioresour Technol, 2006, 97: 2364-2370.
Lin CJ, Shirazi S, Rao P, et al. Effects of operational parameters on cake formation of CaSO_4 in nanofiltration. Water Res, 2006, 40: 806-816.
Lin WF, Chen CH. Clarification of cane juice by ion exchange resins. Taiwan Sugar, 1991, 38: 17-22.
Lobo A, Cambiella A, Benito JM, et al. Ultrafiltration of oil-in-water emulsions with ceramic membranes: Influence of pH and crossflow velocity. J Membr Sci, 2006, 278: 328-334.
Longe OG. Carbohydrate composition of different varieties of cowpea (Vigna unguiculata). Food Chem, 1980, 6: 153-161.
Lowell CA, Kuo TM. Oligosaccharide metabolism and accumulation in developing soybean seeds. Crop Sci, 1989,29:459-465.
Lozano MJ, Martin J. Aspectos nutricionales de la lactancia materna. Acta Pediatr Esp 1998, 56(1): 24-32.
Lopez Leiva MH, Guzman M. Formation of Oligosaccharides during enzymic hydrolysis of milk whey permeates. Process Biochem, 1995, 30(8): 757-762.
Lundquist B, Nord CE, Winberg J. The composition of the faecal microflora in breastfed and bottle fed infants from birth to eight weeks. Acta Paediatrica Scand, 1985, 30: 470-475.
Lyndon R. Commercialization of Adsorbertechnology in the fruit juice industry. Fruit Process, 1996, 6:130-134.
Machaiah JP, Pednekar MD. Carbohydrate composition of low dose radiation-processed legumes and reduction in flatulence factors. Food Chem, 2002, 79: 293-301.
Marathe SA, Rao VS, Thomas P. Nutritional value and acceptability of irradiated legumes- in Proceedings of International Conference on Application of Radioisotopes and Radiation in Industrial Development (ICARID-98). 1998: 219-222.
Marshall AD, Munro PA, Tragardh G. The effect of protein fouling in microfiltration and ultrafiltration on permeate flux, protein retention and selectivity: A literature review. Desalination, 1993, 91: 65-108.
Martinez-Ferez A, Rudloff S, Guadix A, et al. Goats' milk as a natural source of lactose-derived oligosaccharides: isolation by membrane technology. Int Dairy J, 2006, 16: 173-181.
Martins, SIFS, Van Boekel, MAJS. A kinetic model for the glucose/glycine maillard reaction pathways. Food Chem, 2005, 90: 257-269.
Martinez-Villaluenga C, Frias J, Vidal-Valverde C. Raffinose family oligosaccharides and sucrose contents in 13 Spanish lupin cultivars. Food Chem, 2005, 91: 645-649.
Martinez-Villaluenga C, Frias J, Vidal-Valverde C. Raffinose family oligosaccharides and sucrose contents in 13 Spanish lupin cultivars. Food Chem 2005, 91: 645-649.
Maxwell FJ, Duncan SH, Hold G, et al. Isolation, growth on prebiotics andprobiotic potential of novel bifidobacteria from pigs. Anaerobe, 2004, 10: 33-39.
Ma CY, Liu WS, Kwok KC, et al. Isolation and characterization of proteins from soymilk residue (okara). Food Res Int, 1997, 29: 799-805.
Meenakshi S, Viswanathan N. Identification of selective ion-exchange resin for fluoride sorption. J Colloid Interface Sci, 2007, 308: 438-450.
Messina M, Barnes S. The role of soybean products in reducing cancer risks. J Natl Cancer Inst, 1991, 83:541-6.
Metsamuuronen S, Nystrom M. Evaluation of six flat sheet ultrafiltration membranes for fractionation of whey proteins. Desalination, 2006, 200: 290-291.
Miguel H., Leiva L, Guzman M. Formation of oligosaccharides during enzymic hydrolysis of milk whey permeates. Proc Biochem, 1995, 30(8): 757-762.
Mikkelsen LL, Jakobsen M, Jensen BB. Effects of dietary oligosaccharides on microbial diversity and fructo-oligosaccharide degrading bacteria in faeces of piglets post-weaning. Animal Feed Sci Technol, 2003, 109: 133-150.
Mikkelsen LL, Jensen BB. Effect of fructo-oligosaccharides and transgalacto-oligosaccharides on microbial populations and microbial activity in the gastrointestinal tract of piglets post-weaning. Animal Feed Sci Technol, 2004, 117: 107-119.
Mitchell DA, Doelle HW, Greenfield PF. Agar plate growth studies of Rhizopus oligosporus and Aspergillus oryzae to determine their suitability for solid state fermentation. Appl Microbial Biotechnol, 1988,28:598-602.
Mitsuoka, T. Intestinal Flora and Aging. Nutr Rev, 1992, 50: 438-446.
Mondor M, Girard B, Moresoli C. Modeling flux behavior for membrane filtration of apple juice, Food Res Int, 2000, 33: 539-548.
Morales FJ, Jimenez-Perez, S. Peroxyl radical scavenging activity of melanoidins in aqueous systems. Eur Food Res Technol, 2004, 218: 515-520.
Mosenthin R, Bauer E. The potential use of prebiotics in pig nutrition. Asian-Australas J Anim Sci, 2000,13:315-325.
Mountzouris KC, Xypoleas I, Kouseris I, et al. Nutrient digestibility, faecal physicochemical characteristics and bacterial glycolytic activity of growing pigs fed a diet supplemented with oligofructose or trans-galactooligosaccharides. Livestock Sci, 2006, 105: 168 - 175.
Moure A, Dominguez H, Parajo JC. Antioxidant properties of ultrafiltration-recovered soy protein fractions from industrial effluents and their hydrolysates. Process Biochem, 2006, 41: 447-456.
Moure A, Sineiro J, Dominguez H. Extraction and functionality of membrane-concentrated protein from defatted Rosa rubiginosa seeds. Food Chem, 2001, 74: 327-339.
Mourouzidis-Mourouzis SA, Karabelas AJ. Whey protein fouling of microfiltration ceramic membranes-Pressure effects. J Membr Sci, 2006, 282: 124-132.
Mubarak AE. Nutritional composition and antinutritional factors of mung bean seeds (Phaseolus aureus) as affected by some home traditional processes. Food Chem, 2005, 89: 489-495.
Mulimani VH, Devendra S. Effect of soaking, cooking and crude α-galactosidase treatment on the oligosaccharide content of red gram flour. Food Chem, 1998, 61: 475-479.
Mulimani VH, Thippeswamy S, Ramalingam S. Enzymatic degration of oligosaccharides in soybean flours. Food Chem, 1997, 59: 279-282.
Mulyowidarso RK, Fleet GH and Buckle KA.Changes in the concentration of carbohydrates during the soaking of soybeans for tempe production. Int J Food Sci Technol, 1991, 26: 595-606.
Mul AJ, Perry FG. The role of fructo-oligosaccharides in animal nutrition. In: Garnsworthy, P.C., Cole, D.J.A. (Eds.), Recent Advances in Animal Nutrition, Nottingham University Press, Loughborough. 1994:57-79.
Nakao S, Kimura S. Models of membrance transport phenomena and their application for ultrafiltration Data. J. Chem Eng Japan, 1982, 15: 200.
Newburg DS. Do the binding properties of oligosaccharides in milk protect human infants from gastrointestinal bacteria? J Nutr, 1997, 127: 980S- 4S.
Noomhorm A, Kupongsak S, Chandrkrachang S. Deacetylated chitin used as adsorbent in production of clarified pineapple syrup. J Sci Food Agric, 1998, 76: 226-232.
Noordman TR, Kooiker K, Bel W, et al. Concentration of aqueous extracts of defatted soy flour by ultrafiltration. Effect of suspended particles on the filtration flux. J Food Eng, 2003, 58: 135-141.
Obendorf RL. Oligosaccharides and galactosyl cyclitols in seed desiccation tolerance. Seed Sci Res, 1997, 7: 63-74.
Olguin MC, Hisano N, D'Ottavio AE, et al. Nutritional and antinutritional aspects of an Argentinian soy flour assessed on weanling rats. J Food Compos Anal, 2003, 16: 441-449.
Onigbinde AO, Akinyele IO. Oligosaccharide content of 20 varieties of cowpeas in Nigeria. J Food Sci, 1983,48:1250-1251,1254.
Onyenekwe PC, Njoku GC, Ameh DA. Effect of cowpea (Vigna unguiculata) processing methods on flatus causing oligosaccharides. Nutr Res, 2000, 20(3):349-358.
Ozturk N, Bektas TE. Nitrate removal from aqueous solution by adsorption onto various materials. J Haz Mat, 2004, B112: 155-162.
Pafylias I, Cheryan M, Mehaia MA, et al. Microfiltration of milk with ceramic membranes. Food Res Int, 1996,29:141-146.
Pagliero C, Ochoa N, Marchese J, et al. Vegetable oil degumming with polyimide and polyvinilidenfluoride ultrafiltration membranes. J Chemical Technol Biotechnol, 2004, 79: 148-152.
Pan X, Niu G, Liu H. Microwave-assisted extraction of tea polyphenols and tea caffeine from green tea leaves. Chem Eng Proc, 2003, 42: 129-133.
Pan XJ, Niu HZ, Jia GH, et al. Microwave-assisted extraction of glycyrrhizic acid from licorice root. Biochem Eng J, 2000, 5: 173-177.
Pan XJ, Niu HZ, Liu Hui. Comparison of microwave-assisted extraction and conventional extraction techniques for the extraction of tanshinones from Salvia miltiorrhiza bunge. Biochem Eng J, 2002, 12:71-77.
Passounaud M, Bollinger JC, Serpaud B, et al Water nitrate removal with ion-exchanger grafted textiles. Environ Technol, 2000, 21: 745-753.
Patil G, Raghavarao KSMS. Integrated membrane process for the concentration of anthocyanin. J Food Eng, 2007, 78: 1233-1239.
Paugam L, Rabiller-Baudry M, Delaunay D. Physico-chemical effect of simple alkaline and acid solutions in cleaning sequences of spiral ultrafiltration membranes fouled by skim milk. Desalination, 2006,200: 192-194.
Pohl P. Application of ion-exchange resins to the fractionation of metals in water. Trends Anal Chem, 2006, 25:31-43.
Pool-Zobel B, Van Loo J, Rowland I et al. Experimental evidences on the potential of prebiotic fructans to reduce the risk of colon cancer. Br J Nutr, 2002, 87: S273-81.
Poulin JF, Araya-Farias M, Amiot J, et al. Separation of bioactive peptides by electrodialysis with ultrafiltration membrane. Desalination, 2006, 200: 620.
Pouliot M, Pouliot Y, Britten M, et al. Effects of pH and ionic environment on the permeability and rejective properties of an alumina microfiltration membrane for whey proteins. J Membr Sci, 1994, 95:125-134.
Pradhan J, Das SN, Thakur RS. Adsorption of Hexavalent Chromium from Aqueous Solution by Using Activated Red Mud. J Colloid Interf Sci, 1999, 217(1): 137-141.
Prinyawiwatkul W, Beuchat LR, McWatters KH, et al. Changes in fatty acid, simple sugar, and oligosaccharide content of cowpea (Vigna unguiculata) flour as a result of soaking, boiling, and fermentation with Rhizopus microsporus var. oligosporus. Food Chem, 1996, 57: 405-413.
Qiu N, Guo S, Chang Y. Study upon kinetic process of apple juice adsorption decolouration by using adsorbent resin. J Food Eng, 2007, 81: 243-249.
Rai P, Majumdar GC, Das Gupta S, et al. Effect of various pretreatment methods on permeate flux and quality during ultrafiltration of mosambi juice. J Food Eng, 2007, 78: 561-568.
RautenbachR.膜工艺-组件和装置设计基础.1998.第一版.北京：化学工业出版社.
Reddy NR, Salunkhe DK. Changes in oligosaccharide during germination and cooking of Black Gram and fermentation of Black Gram/Rice Blend. Cereal Chem, 1980, 57: 356-360.
Redondo-Cuenca A, Villanueva-Suarez MJ, Rodriguez-Sevilla MD, et al. Chemical composition and dietary fibre of yellow and green commercial soybeans (Glycine max). Food Chem, 2006, 101: 1216-1222.
Refstie S, Sahlstrom S, E Brathen, et al. Lactic acid fermentation eliminates indigestible carbohydrates and antinutritional factors in soybean meal for Atlantic salmon (Salmo salar). Aquaculture, 2005, 246: 331-345.
Rhim, JW, Gennadios A, Handa A, et al. Solubility, tensile, and color properties of modified soy protein films. J Agric Food Chem, 2000, 48: 4937-4941.
Rivero-Urgell M, Santamaria-Orleans A. Oligosaccharides: application in infant food. Early Hum Dev, 2001,65 Suppl.:S43-S52.
Rodriguez M, Gonzalez-Munoz MJ, Luque S, et al. Extractive ultrafiltration for the removal of carboxylic acids. J Membr Sci, 2006, 274: 209-218.
Rowland IR, Rummey CJ, Coutts JT. Effect of Bifidobacterium longum and inulin on gut bacterial metabolism and carcinogen-induced aberrant crypt foci in rats. Carcinogenesis, 1998, 19: 281-285.
Ruiz-Lopez MA, Garcia-Lopez PM, Castaneda-Vazquez H, et al. Chemical composition and antinutrient content of three lupinus species from Jalisco, Mexico. J Food Compos Anal, 2000, 13: 193-199.
Ruiz-Matute AI, Sanz ML, Martinez-Castro I. Use of gas chromatography-mass spectrometry for identification of a new disaccharide in honey. J Chromatogr A, 2007, 1157: 480-483.
Ruiz-Teran F, Owens JD. Fate of oligosaccharides during production of soya bean tempe. J Sci Food Agric, 1999,79:249-252.
Saavedra JM, Bauman NA, Oung 1, et al. Feeding of Bifidobacterium bifidum and Streptococcus thermophilus to infants in hospital for prevention of diarrhea and shedding of rotavirus. Lancet, 1994,344: 1046-1049.
Sadrzadeh M, Razmi A, Mohammadi T. Separation of different ions from wastewater at various operating conditions using electrodialysis. Sep Purif Technol, 2007, 54(2): 147-156.
Sako T, Matsumoto K, Tanaka R. Recent progress on research and applications of non-digestible galacto-oligosaccharides. Int Dairy J, 1999, 9: 69-80.
Saltzman JR, Russell RM. The aging gut. Nutritional issues. Gastroenterol Clin North Am 1998, 27:309-24.
Sata T, Kawamura K, Higa M, et al. Electrodialytic transport properties of cation exchange membranes in the presence of cyclodextrins. J Membr Sci, 2001, 183: 201-212.
Sayed Razavi SK, Harris JL, Sherkat F. Fouling and cleaning of membranes in the ultrafilation of the aqueous extract of soy flour. J Membr Sci, 1996, 114: 93-104.
Sayed Razavi SK, Harris JL. Shear controlled model of the ultrafilation of soy suspensions. J Membr Sci, 1996,118:279-288.
Sanchez-Mata MC, Camara Hurtado MM, Diez-Marques C. Effect of domestic processes and water hardness on soluble sugars content of chickpeas (Cicer arietinum L.). Food Chem, 1999, 65: 331 -338.
Scalabrini P, Rossi M, Spettoli P, et al. Characterization of Bifidobacterium strains for use in soymilk fermentation. Int J Food Microbiol, 1998, 39: 213-219.
Schiffrin EJ, Brassart D, Servin AL, et al. Immune modulation of blood leukocytes in humans by lactic acid bacteria: criteria for strain selection. Am J Clin Nutr, 1997, 66: 515S-S20.
Schiffrin EJ, Rochat F, Link-Amster H, et al. Immuno-modulation of human blood cells following theingestion of lactic acid bacteria. J Dairy Sci, 1995, 78: 491-497.
Scordino M, Mauro AD, Passerini A. Highly purified sugar concentrate from a residue of citrus pigments recovery process. LWT, 2007, 40: 713-721.
Seo WG, Pae HO, Kim NY, et al. Synergistic cooperation between water soluble chitosan oligomers and interferon-g for induction of nitric oxide synthesis and tumoricidal activity in murine peritoneal macrophages. Cancer Lett, 2000, 159: 189-95.
Serpen A, Atac B, Gokmen V. Adsorption of Maillard reaction products from aqueous solutions and sugar syrups using adsorbent resin. J Food Eng, 2007, 82: 342-350.
Shallo HE, Rao A, Ericson AP, et al. Preparation of soy protein concentrate by ultrafiltration. J Food Sci, 2001,66:242-246.
Shu YY, Ko MY, Chang YS. Microwave-assisted extraction of ginsenosides from ginseng root. Microchem J, 2003,74: 131-139.
Sinniah UR, Ellis RH, John P. Irrigation and Seed Quality Development in Rapid-cycling Brassica: Soluble Carbohydrates and Heat-stable Proteins. Ann Botany, 1998, 82: 647-655.
Snir R, Koehler PE, Sims KA, et al. pH and cations influence permeability of marsh grapefruit pectinerase on polysulfone ultrafiltration membrane. J Agric Chem, 1995, 43: 1155-1162.
Stark AH, Madar Z. In vitro production of shortchain fatty acids by bacterial fermentation of dietary fiber compared with effects of those fibers on hepatic sterol synthesis in rats. J Nutr, 1993, 123: 2166-2173.
Strathmann H. Electrodialysis and its application in the chemical process industry,.Sep Purif Meth, 1985,14(1): 44-66.
Strathmann H. Ion-exchange Membrane Separation Processes, Elsevier, Amsterdam, 2004.
Strickling JA, Harmon DL, Dawson KA, et al. Evaluation of oligosaccharide addition to dog diets: influences on nutrient digestion and microbial populations. Animal Feed Sci Technol, 2000, 86: 205-219.
Silva HC, Braga GL. Effect of soaking and cooking on the oligosaccharide content of dry beans (Phaseolus vulgaris L.). J Food Sci, 1982, 47: 924-925.
Somiari RI, Balogh E. Effect of soaking, cooking and crude α-galactosidase treatment on the oligosaccharide content of cowpea flours. J Sci Food Agric, 1993, 61: 339-343.
Susanto H, Ulbricht M. Insights into polysaccharide fouling of ultrafiltration Membranes. Desalination, 2006,200:181-182.
Tang CH, Wu H, Chen Z, et al. Formation and properties of glycinin-rich and β-conglycinin-rich soy protein isolate gels induced by microbial transglutaminase. Food Res Int, 2006, 39: 87-97.
Tanka Y. Concentration polarization in ion-exchange membrane electrodialysis-the events arising in a flowing solution in a desalting cell. J Membr Sci, 2003, 216: 149-164.
Taper HS, Roberfroid M. Influence of inulin and oligofructose on breast cancer and tumor growth. J Nutr, 1999, 129:1488S-1491S.
Tomomatsu H. Health effects of oligosaccharides. Food Technol, 1994, 10: 61-65.
Tomomatsu H. Health effects of oligosaccharides. Food Technol, 1994, 48(10): 61- 5.
Torres MR, FR Marin, Ramos AJ. Study of operating conditions in concentration of chicken blood plasma proteins by ultrafiltration. J Food Eng, 2002, 54: 215-219.
Trugo LC, Farah A, Cabral L. Oligosaccharides distribution in Brazilian soya bean cultivars. Food Chem, 1995,52:385-387.
Trugo LC, Ramos LA, Trugo NMF,et al. Oligosaccharide composition and trypsin inhibitor activity of Phaseolus vulgaris and e.ect of germination on the α-galactoside composition and fermentation in human colon. Food Chem, 1990, 36: 53-61.
Uwaegbute AC, Iroegbu CU, Eke O. Chemical and sensory evaluation of germinated cowpeas (Vigna unguiculata) and their products. Food Chem, 2000, 68: 141-146.
Ushikubo FY, Watanabe AP, Viotto LA. Effects of operating conditions and enzyme treatment on fouling and polarized layer formation during umbu (Spondias tuberosa An. Cam.) juice microfiltration. Desalination, 2006, 200: 546-548.
Unlu N, Ersoz M. Removal of heavy metal ions by using dithiocarbamatedsporopollenin. Sep Purif Technol, 2007, 52: 461-469.
De Van Lisdonk CAC, Van Paassen JAM, Schippers JC, et al. Monitoring scaling in nanofiltration and reverse osmosis membrane systems. Desalination, 2000, 132: 101-108.
Valerdi-Perez R, Ibanez-Mengual JA. Current-voltage curves for an electrodialysis reversal pilot plant: determination of limiting currents. Desalination, 2001, 141: 23-37.
Vaccari G, Lodi G, Tamburini E, et al. Chromatographic Separations in Sugar Analysis and Processes Detection of oligosaccharides in sugar products using planar chromatography. Food Chem, 2001, 74: 99-110.
Vegas R, Moure A, Dominguez H, et al. Purification of oligosaccharides from rice husk autohydrolysis liquors by ultra- and nano-filtration. Desalination, 2006, 199: 541-543.
Velazquez M, Davies C, Marett R, et al. Effect of oligosaccharides and fibre substitutes on short-chain fatty acid production by human faecal microflora. Anaerobe, 2000, 6: 87-92.
Vera E, Dornier M, Ruales J, et al. Comparison between different ion exchange resins for the deacidification of passion fruit juice. J Food Eng, 2003, 57: 199-207.
Vera E, Ruales J, Dornier M, et al. Comparison of different methods for deacidification of clarified passion fruit juice. J Food Eng, 2003, 59: 361-367.
Vera E, Sandeaux J, Persin F, et al. Deacidification of clarified tropical fruit juices by electrodialysis. Part I. Influence of operating conditions on the process performances. J Food Eng, 2007, 78: 1427-1438.
Vera E, Sandeaux J, Persin F, et al. Deacidification of clarified tropical fruit juices by electrodialysis. Part II. Characteristics of the deacidified juices. J Food Eng, 2007, 78: 1439-1445.
Vera E, Ruales J, Dornier M, et al. Comparison of different methods for deacidification of clarified passion fruit juice. J Food Eng, 2003, 59: 361-367.
Vijayakumari K, Siddhuraju P, Janardhanan K. Effect of soaking, cooking and autoclaving on phytic acid and oligosaccharide contents of the tribal pulse, Mucuna monosperma DC. ex. Wight. Food Chem, 1996, 55: 173-177.
Voragen AGJ. Technological aspects of functional foodrelated carbohydrates. Trends in Food Sci & Tech 1998,9:328-335.
Vyas PV, Shah BG. Separation of inorganic and organic acids from glyoxal by electrodialysis. Desalination, 2001, 140(1): 47-54.
Wang N, Daun JK. Effects of variety and crude protein content on nutrients and anti-nutrients in lentils (Lens culinaris). Food Chem, 2006, 95: 493-502.
Wang N, Lewis MJ, Brennan JG, et al. Effect of processing methods on nutrients and anti-nurtitional factors in cowpea. Food Chem, 1997, 58: 59-68.
Wang X, Zhang C, Ouyang P. The possibility of separating saccharides from a NaCl solution by using nanofiltration in diafiltration mode. J Membr Sci, 2002, 204: 271-281.
Wisniewski J, Suder S. Water recovery from etching effluents for the purpose of rinsing stainless steel. Desalination, 1995, 101: 245-253.
Wisniewski J,Rozanska A.Donnan dialysis with anion-exchange membranes as a pretreatment step before electrodialytic desalination.Desalination,2006,191:210-218.
Xu L,Lamb K,Layton L,Kumar A.A membrane-based process for recovering isoflavones from a waste stream of soy processing.Food Res Int,2004,37:867-874.
Xu Y,Lebrun RE.Comparison of nanofiltration properties of two membranes using electrolyte and non-electrolyte solutes.Desalination,1999,122:95-106.
Xu T.Ion exchange membranes:State of their development and perspective.J Mere Sci,2005,263:1-29
Yazicigil Z,Oztekin Y.Boron removal by electrodialysis with anion-exchange membranes.Desalination,2006,190:71-78.
Zhang F,Chert B,Xiao S,et al.Optimization and comparison of different extraction techniques for sanguinarine and chelerythrine in fruits ofMacleaya cordata(Willd).R Br Sep PurifTechnol,2005,42:283-290.
Zydney AL.Protein separation using membrane filtration:New opportunities for whey fractionation.Int Dairy J,1998,243-250.
曹凤芹,王少庸,刘荣.利用大豆废水提取功能性因子工艺技术.大豆通报,2005,4:25-26.
车向荣,岳文斌,臧建军等.功能性低聚糖对断奶仔猪腹泻的防治及生产性能的影响.中国兽医学报,2003,23(3):292-294.
陈浚,电渗析法处理含铅废水的研究,浙江工业大学,硕士学位论文,2004,05.01
陈文仙.腐竹生产与检验.福建轻纺,2005,3:15-19.
程桂石,汪群慧,齐虹等.pH值对电渗析法回收厨房垃圾发酵液中乳酸的影响.化工学报,2005,56(111):2200-2203.
崔岸,朱峰,黄惠华等.超滤法生产大豆分离蛋白的研究.食品科学,1996,17(11):18-22.
崔洪斌等.大豆生物活性物质的开发与应用.北京:中国轻工业出版社,2001,3:48-113.
董红兵.大豆加工中副产品的开发与应用(一)-大豆低聚糖的开发与应用.武汉商业服务学院学报,2003,12(4):13-14.
董玉枝.大豆低聚糖对高脂质过氧化的影响.中国老年杂志,1996,16:242-243.
冯志彪.大豆低聚糖及其在食品工业中的应用.山西食品工业,1998,4:5-8.
冯振宁,钟振声,王文铂.用离子色谱法提纯低聚糖的研究.广东化工,2004,4:38-40.
江洁,王文侠,栾广忠.大豆深加工技术.北京:中国轻工业出版社,2004:263-427.
甘林火,翁连进.氨基酸溶液脱盐技术的进展.福建化工,2002,4:72-73.
高安全,吴景远,梁伟.膜分离技术在大豆乳清回收中的应用.过滤与分离,2001,11(3):26-27.
高文宏,石彦国,高大维等.超滤法提取大豆低聚糖前处理的研究.中围粮油学报,2000,15(5):49-52.
高文宏,石彦国,李国基等.超滤法提取大豆低聚糖的研究.食品与发酵工业,2000,26(6):6-11.
高文宏,石彦国,李国基等.大豆低聚糖提取中超滤膜的选择.食品科学,2000,21(5):15-20.
高伟星,柳森.用超滤法提取大豆低聚糖的研究.大连民族学院学报,2005,7(1):95.
高以恒,叶凌碧.膜分离技术基础.北京:科学出版社,1989,236.
高英,单安山.大豆寡糖在肉仔鸡日粮中的应用.饲料研究,2004,5:11-13.
郭本恒,孔保华.保健与功能食品.哈尔滨:黑龙江科技出版社,1996:155.
郭敏亮,姜涌明.考马斯亮蓝显色液组分对蛋白质测定的影响.生物化学与生物物理进展,1996,23(6):558-561.
郭尧君.蛋白质电泳实验技术第二版.北京:科学技术出版社,2005:92-112.
郭尽力.大豆低聚糖的提取工艺研究.烟台大学学报(自然科学与工程版),2004,17(4):298-302.
郝健,刘德华.1,3-丙二醇发酵液电渗析法脱盐.过程工程学报,2005,5(1):36-39.
郝岩平,姜金斗,杨秀茹.HPLC法测定食品中大豆低聚糖的含量.中国甜菜糖业,2003,1:8-11.
何小维,薛新顺,罗发兴等.功能性大豆低聚糖分离纯化研究概况.食品研究与开发,2005,26(4):184-188.
黄海,杨瑞金,王璋.低聚木糖液脱色树脂的选择.食品与机械,2001(5):31-32.
黄海,杨瑞金,王璋.低聚木糖的脱色工艺.无锡轻工大学学报,2002,21(2):125-130.
黄进,夏继涛,张声华.大豆异黄酮、皂甙和低聚糖提取工艺研究.粮食与饲料工业,2002,9:36-38.
黄祥斌,于淑娟,高大维.几种离子交换树脂用于糖浆脱色的比较研究.食品科学,2001,22(4):11-13.
金丰秋,金其荣.低聚糖在饲料中的应用.中国饲料,1999,5:16.
金其荣,徐勤.大豆低聚糖生产、生理功能及其应用.食品科学,1994,11:7-12.
金华丽.大豆低聚糖制取及纯化工艺的研究.郑州工程学院学报,2001(2):35-38.
赖凤英,陈焕章,林福兰.离子交换树脂对糖浆脱色效能的评价.中国甜菜糖业,2000,6:12-14.
赖凤英,陈焕章,林福兰.用吸附等温线评价离子交换树脂的脱色效能.广西蔗糖,2000,2:31-33.
赖凤英,林庆生,许喜林等.活性炭对糖浆脱色效能的研究.中国甜菜糖业,1999,10:2-5.
兰建丽.大豆低聚糖生产工艺技术.大豆通报,2001,4:20-21.
李刚,焦凌霞,严晓艳.脱脂豆粕中大豆低聚糖制备工艺的研究.安徽农业科学,2006,15:3798-3814.
李耕,吴大宇,戴智河.膜技术在浓缩天然大豆低聚糖中的应用.膜科学与技术,2002,22(1):29-31.
丽娟,姚军虎,张周.功能性低聚糖及其在断奶仔猪饲养中的应用.饲料博览,2004,11:38-39.
李诗龙.腐竹食品的现代加工技术.粮油加工与食品机械,2005,3:72-75.
李里特.大豆加工与利用.北京:化学工业出版社,2003.
李玲,许多,赵国良等.大豆中生物物质的分离与分析的研究(Ⅰ)—用ODS柱高效液相色谱法测定大豆中的低聚糖.食品与发酵工业,1995,3:44-47.
李晓炼,刘志同,叶光.膜分离技术提取大豆乳清中的低聚糖.食品科技,1999,4:19-21.
李应彪,童军茂,翟金兰.膜及膜分离技术在食品工业中的应用.粮油加工与食品机械,2000,3(2):30-31.
梁冰,熊德鑫.双歧杆菌QJ405、乳杆菌QJ405在试管内对肠道致病菌抑杀效果的初步报告.中国微生态杂志,2000,12(5):269-271.
刘昌胜,邬行彦.超滤过程中操作条件的优化.膜科学与技术,1995,15(4):12-15.
刘国信,刘录声.膜法分离技术及其应用.北京:中国环境科学出版社.1991:115-177.
刘莉.超滤膜法处理大豆乳清废水工艺的研究.哈尔滨工业大学工程硕士学位论.20030901.
刘军,栾居科,李文涛.大豆低聚糖、乳清蛋白的提取.中国油脂,2002,27(4):45-49.
刘俏,范圣第.超滤处理豆腐废水阻力的研究.环境污染治理技术与设备,2005,6(2):49-52.
刘贤杰,陈福明.电渗析技术在酱油脱盐中的应用.中国调味品,2004,4:17-21.
刘祥.大豆低聚糖对肠道菌群结构调节的研究.中国微生态学杂志,2003,12:10-13.
刘欣,冯杰.大豆低聚糖的生理功能及其应用.中国饲料,2005,6:15-16.
刘永宁,范云鸽,施荣富等.交联聚丙烯酰多胺树脂的合成及脱色性能的研究.化学试剂,1994,16(4):215-217.
刘峥.微波法提取大豆中低聚糖的研究.食品研究与开发,2002,23(2):24-26.
马莺.大豆低聚糖的提取及酶改性的研究(博士论文).东北农业大学,2000.
马莺,骆承痒.大豆低聚糖生产中大豆乳清的预处理和超滤技术(Ⅱ).中国商办工业.2001,4:48-49.
马莺,骆承痒,吴昊.高效液相色谱法测定大豆乳清中大豆低聚糖.分析化学,1999,27(3):367.
马莺,骆承庠,肖志刚.超滤法提取大豆低聚糖的研究.粮油食品科技,2000,8(5):17-19.
毛跟年,柯蕾,李彦军等.离子交换法分离纯化麦芽低聚糖.食品工业科技,2005,26(4):127-128.
潘见,陈强,谢慧明等.大孔树脂对葛根黄酮的吸附分离特性研究.农业工程学报,1999,15(1):236-240.
钱庭宝,刘维林,李金和.吸附树脂及其应用.北京:化学工业出版社.1990,587-595.
秦志荣,于淑娟,高大维.糖浆脱色阴离子交换树脂再生新方法的研究.中国甜菜糖业,1999,8:10-13.
邵刚.膜法水处理技术(第2版).北京:冶金工业出版社,2001.
史锋.生物化学实验.杭州:浙江大学出版社,2002:1-3.
史宣明,赖本丽.大豆低聚糖的精制.中国油脂.2005,30(5):39-40.
石彦国.大豆制品工艺学.北京:中国轻工业出版社,2005:30-90.
唐宇,龚燕,王晓琳等.1,3-丙二醇发酵液电渗析脱盐的中试研究.化工进展,2004,23(1):84-87.
唐宇,龚燕,王晓琳等.1,3-丙二醇发酵液电渗析脱盐工艺的优化.水处理技术,2005,31(4):41-45.
田心健,钟世荣,张伟.酸沉淀法制取大豆低聚糖的工艺研究.四川轻化工学院学报,2001,14(3):75-78.
田三德,孙鹏.大豆低聚糖的生产及应用.实用技术,2003,10:18-19.
汪莉,苏军,苏宁.低聚糖对蛋雏鸡生长性能、免疫器官发育及粪臭的影响.黑龙江畜牧兽医,2001,11:9-11.
汪莉,苏宁,苏军等.低聚糖对蛋雏鸡生长性能及粪臭的影响.家畜生态,2002,23(1):30-32.
汪莉,罗淑琴,苏宁等.低聚糖对蛋雏鸡生长性能及粪臭的影响.畜牧与兽医,2002,34(6):6-8.
王炳南.用膜集成技术分离大豆低聚糖.水处理技术,2005,31(1):72-74.
王全军.低聚糖在动物饲养中的应用.中国饲料,2000,16:15-17.
王树勖,王立蓉.反渗透技术研究现状.甘肃科技,2005,21(12):187-188.
王水兴,夏慧玲,吴凌伟,晏有生.树脂法分离低聚木糖的研究.中国食品添加剂,2004,11:36-38.
王素敏.大豆低聚糖对大鼠血脂和抗氧化作用的影响.营养学报,1997,19(4):10-13.
王平,李立新,曹培刚等.浅谈反渗透脱盐的预处理.河北电力技术,2004,23(2):36-39.
王文侠,翟丽萍,张文超等.大豆低聚糖的制备工艺研究.中国乳品工业,1999,127(12):10-12.
王晓,张孝范.保健功能因子大豆低聚糖及其开发.西部粮油科技.1999,24(1):31-33.
王晓琳,张澄洪,欧阳平凯.应用纳滤膜分离糖和盐的实验研究.膜科学与技术,2001,21(1):44-48.
王晓忠,刘跃泉,任宏志.利用膜分离技术对大豆乳清废水综合利用.粮食与油脂,2004,4:45.
王学松.膜分离技术及其应用.北京:科学技术出版社,1994,7-10.
王元凤,金征宇.D315树脂分离茶多糖工艺的研究.农业工程学报,2005,21(10):147-150.
王湛.膜分离技术基础.北京:化学工业出版社,2000:1-6.
翁利荣,罗发兴,黄强等.低聚木糖脱色技术研究概括.食品科技,2004,7:51-54.
伍军,艾启俊,于同泉等.大豆黄浆水处理过程中超滤膜的选择.北京农学院学报,2003,18(3):223-225.
伍军,艾启俊,于同泉.应用纳滤膜分离大豆黄浆水的研究.粮油加工与食品机械,2004,3:56-60.
伍军,艾启俊,于同泉等.大豆黄浆水处理过程中超滤膜的选择.北京农学院学报,2003,18(3):17-19.
向东,王国政,赖凤英等.活性炭对南瓜粗多糖液的脱色研究.河南科学,2004,22(6):780-782.
辛嘉英.从豆腐黄浆水中提取大豆低聚糖.今日科技,1995,2:14.
熊泽,唐明,邵伟.大豆低聚糖的提取及其对乳酸菌生长影响的研究.现代食品科技,2005,4:25-27.
徐晓云,潘思轶,谢笔钧等.树脂法精制沙棘籽原花色素的研究.农业工程学报,2005,21(1):152-154.
徐勇,余世袁,勇强等.活性炭对低聚木糖的脱色.南京林业大学学报(自然科学版),2003,27(2):7-10.
徐忠,张洪微,韩玉洁.离子交换树脂对高麦芽糖浆的分离纯化研究.化学与黏合,2005,27(5):286-288.
徐忠,张亚丽.活性炭脱色对大豆低聚糖质量的影响.化学与粘合,2001,6:270-271.
徐超斗,梁爱君,祝业等.大豆低聚糖对免疫功能的促进作用.解放军药学学报,2005,21(1):37-39.
徐秀容,龚月生.低聚糖对早期断奶仔猪消化道微生物区系的调节作用.饲料工业,1999,20(6):31-32.
薛连海.气相色谱法测定大豆中低聚糖含量.分析化学,2003,31(3):382.
薛文通,王浩.功能性低聚糖-大豆低聚糖.食品研究与开发,2003,24(3):3-5.
姚文华,尹卓容.大枣多糖脱色的工业化试验.食品工业,2006,5:41-43.
杨汝德,张玲华,林晓珊等.大豆低聚糖的制取及其促生作用的研究.食品工业,1996,3:5-8.
杨云,刘福勤,冯卫生,孟江,田润涛.碱法提取大枣渣多糖及活性炭脱色的工艺研究.食品与发酵工业,2004,30(7):30-33.
叶桂安,杨希山.双歧杆菌及肠致病性大肠杆菌粘附的细胞膜通透性研究.中国微生态杂志,2000,12(3):132-133.
袁其朋,张恭孝,姜焱.树脂及活性碳吸附技术回收大豆乳清中的异黄酮和低聚糖.大豆科学,2003,22(1):6-10.
袁其朋,马润宇.膜分离技术处理大豆乳清废水.水处理技术,2001,27(3):161-163.
岳振峰,陈小霞,彭志英等.功能性低聚糖分离纯化方法概述.郑州工程学院学报,2001,22(1):89-92.
尤新.功能性低聚糖生产与应用.北京:中国轻工业出版社.2004:1-182.
张保平.饲用抗生素的替代品—低聚糖.河南畜牧兽医 2000,21(4):11-12.
张延坤,刘国忠.大豆低聚糖及其在食品工业的应用.食品工业,1999,3:5-8.
张延坤,房玉水,邓峰.用高效液相色谱法测定棉籽蛋白中的棉籽糖.食品工业,1996,3:58-59.
张延坤,张东祥,刘国忠等.高效液相色谱法测定大豆低聚糖.食品工业,2000,2:45-46.
张振红,黄仁录.大豆低聚糖的研究及其在饲料中的应用.兽药与饲料添加剂,2005,10(4):14-16.
赵冬梅,刘凌,张京健.豆制品生产中高浓度废水的检测与分析.食品与发酵工业,2006,32(1):
赵贵兴,陈霞,刘忠云等.大豆低聚糖制备工艺的研究.黑龙江农业科学,2002(2):13-15.68-71.
赵婧,冯骉.氨基酸溶液电渗析脱盐过程中的研究.2005,26(8):57-60.
赵丽颖,符群.膜分离技术在大豆乳清废水回收中应用.粮食与油脂,2002,9:48-49.
钟振声,冯焱,孙立杰等.柱色谱法对大豆低聚糖浆脱色效果的研究.精细化工,2006,23(6):565-568.
钟振声,冯三马,孙立杰等.柱色谱法对大豆低聚糖浆脱色效果的研究.精细化工,2006,23(6):565-567.
钟振声,王文铂.用离子交换树脂祛除低聚糖中的葡萄糖.化学与生物工程.2004,4:36-37.
周尽花,周春山.大孔吸附树脂法柚皮果胶脱色工艺研究.离子交换与吸附,2005,21(6):542-550.
周中凯.新型饲料添加剂—功能性低聚糖.广东饲料,1999,1:29-32.
周中凯,夏英.饲料用低聚糖的研究与认识.饲料研究,1999,3:3-6.
Achaerandio I, Guell C, Lopez F. Continuous vinegar decolorization with exchange resins. J Food Eng, 2002,51:311-317.
Adlerberth I. The establishment of a normal intestinal microflora in the newborn infant. In Hanson LA, Yolken RB. (Eds.), Probiotics, other nutritional factors, and intestinal flora. 42nd Nestle nutrition workshop. New York: Lippincot Williams & Wilkins. 1997: 63-78.
Aimar P, Baklouti S, Sanchez V et al. membrane-solute interactions: influence on pure solvent transfer during ultrafiltration. J Membr Sci, 1986, 29: 207-224.
Akinyele 10, Akinlosotu A. Effect of soaking, dehulling and fermentation on the oligosaccharides and nutrient content of cowpeas (Vigna unguiculata). Food Chem, 1991, 41: 43-53.
Akoum O, Richfield D, Jaffrin MY, et al. Recovery of trypsin inhibitor by soy milk ultrafiltration using a rotating disk system. Desalination, 2006, 191: 438-445.
Alander M, Matto J, Kneifel W, et al. Effect of galacto-oligosaccharide supplementation on human faecal microflora and on survival and persistence of Bifidobacterium lactis Bb-12 in the gastrointestinal tract. Int Dairy J, 2001, 11: 817-825.
Alibhai Z, Mondor M, Moresoli C, et al. Production of soy protein concentrates/isolates: traditional and membrane technologies. Desalination, 2006, 191: 51-358.
Al-Kaisey MT, Alwan AKH, Mohammad MH, et al. Effect of gamma irradiation on antinutritional factors in broad bean. Radiat Phys Chem, 2003, 67: 493-496.
Andersson HB, Ellegard LH, Bosaeus IG. Nondigestibility characteristics of inulin and oligofructose in humans. J Nutr, 1999, 129: 1428S-30S.
Archer S, Meng S, Wu J, et al. Butyrate inhibits colon carcinoma cell growth through two distinct pathways. Surgery, 1998,124:248-253.
Atungulu G, Koide S, Sasaki S, et al. Ion-exchange membrane mediated electrodialysis of scallop broth: Ion, free amino acid and heavy metal profiles. J Food Eng, 2007, 78: 1285-1290.
Ayala-Bribiesca E, Pourcelly G, Bazinet L. Nature identification and morphology characterization of cation-exchange membrane fouling during conventional electrodialysis. J Colloid Interface Sci, 2006, 300: 663-672.
Baltrusaityte V, Venskutonis PR, Ceksteryte V. Radical scavenging activity of different floral origin honey and beebread phenolic extracts. Food Chem, 2007, 101: 502-514.
Bau HM, Villanme C, Nicolos JP, et al. Effect of germination on chemical composition, biochemical constitutes and antinutritional factors of soy bean (Glycine max) seeds. J Sci Food Agr, 1997, 73: 1-9.
Bento LSM. Sugar decolorization by ion-exchange resins with regenerant recovery. Int Sugar J, 1990, 92: 116-125.
Bento LSM. Proc. AVH Assoc.-6th Symposium Reins, 1999: 23-27.
Beolchini F, Veglio F, Barba D. Microflltration of bovine and ovine milk for the reduction of microbial content in a tubular membrane: a preliminary investigation. Desalination, 2004, 161: 251-258.
Berdous D, Akretche DE, et al. Recoveryof metals by Donnan dialysis with ion exchange textiles. Desalination, 2002, 144: 212-218.
Bielecka M, Biedrzycka E, Majkowska A, et al. Effect of non-digestible oligosaccharides on gut microecosystem in rats. Food Res Int, 2002,35: 139-144.
Bland EJ, Keshavarz T, Bucke C. The influence of small oligosaccharides on the immune system. Carbohydr Res, 2004, 339: 1673-1678.
Boniardi N, Rota R, Nano G, et al. Analysis of the sodium lactate concentration process by electrodialysis. Sep Technol, 1996, 6(1): 43-54.
Bouhidel KE, Lakehal A. Influence of voltage and flow rate on electrodeionization (EDI) process efficiency. Desalination, 2006, 193: 411-421.
Brand J, Bull S, Miller J, et al. The oligosaccharide composition of human milk: temporal and individual variations in monosaccharide components. J Pediatr Gastroenterol Nutr, 1994, 19(4): 371-6.
Brassart D, Schiffrin EJ. The use of probiotics to reinforce mucosal defence mechanisms. Trends Food Sci Technol, 1997, 8:321-326.
Buedo AP, Elustondo MP, Urbicain MJ. Amino acid loss in peach juice concentrate during storage. Innovative Food Sci Emerging Technol, 2001, 1: 281-288.
Cai BX. Study of membrane separation processes of a betaine-like medicinal solution. Desalination, 2006, 191:432-437.
Calle EV, Rusles J, Dornierb M, et al. Deacidification of the clarified passion fruit juice. Desalination, 2002, 149:357-361.
Carabasa M, Ibarz A, Garza S et al. Removal of Dark Compounds from Clarified Fruit Juices by Adsorption Processes. J Food Eng, 1998, 37: 25-41.
Cassano A, Donato L, Drioli E. Ultrafiltration of kiwifruit juice: Operating parameters, juice quality and membrane fouling. J Food Eng, 2007, 79: 613-621.
Chabani M, Amrane A, Bensmaili A. Kinetic modelling of the adsorption of nitrates by ion exchange resin. Chemical Eng J, 2006, 125: 111-117.
Chairat M, Rattanaphani S, Bremner JB, et al. Adsorption kinetic study of lac dyeing on cotton. Dyes Pigments, 2008, 76: 435-439.
Chaturvedi P, Warren CD, Ruiz-Palacios GM, et al. Milk oligosaccharide profiles by reversed-phase HPLC of their perbenzoylated derivatives. Anal Biochem, 1997,251: 89-97.
Cheang B, Zydney AL. A two-stage ultrafiltration process for fractionation of whey protein isolate. J Membr Sci, 2004, 231: 159-167.
Cheryan M. Ultrafiltration and Microfiltration Handbook, CRC Press, Boca Raton, FL, 1998.
Chitra US, Rao PV. Phytic acid, in vitro protein digestibility, dietary fiber and minerals of pulses as influenced by processing methods. Plant Foods Human Nutr, 1996,47: 163-172.
Chiu TY, Lara Dominguez MV, James AE. Critical flux and rejection behaviour of non- circular- channelled membranes Influence of some operating conditions. Sep Purif Technol, 2006, 50: 212-219.
Choi EY, Choi JH, Moon SH. An electrodialysis model for determination of the optimal current density. Desalination, 2002, 153: 399-404.
Chou CC, Hou JW. Growth of bifidobacteria in soymilk and their survival in the fermented soymilk drinkduring storage. Int J Food Microbiol, 2000, 56: 113-121.
Chumchuere S, Robinson RK. Selection of starter cultures for the fermentation of soya milk. Food Microbiol, 1999, 16: 129-137.
Ciucanu I, Caprita R. Per-O-methylation of neutral carbohydrates directly from aqueous samples for gas chromatography and mass spectrometry analysis. Anal Chim Acta, 2007, 585: 81-85.
Coppa G, Gabrielli O, Giorgi P, et al. Preliminary study of breastfeeding and bacterial adhesion to uroepithelial cells. Lancet, 1990, 335: 569-571.
Costa AR, de Pinho MN. Comparison of the performance of ultrafiltration and nanofiltration in surface water treatment. Desalination, 2006, 199: 73-75.
Crittenden RG, Playne MJ. Production, properties and applications of food-grade oligosaccharides. Trends Food Sci Technol, 1996, 7: 353-361.
Cui ZW, Sun LJ, Chen W, et al. Preparation of dry honey by microwave-vacuum drying. J Food Eng, 2008, 84:582-590.
Cummings JH, Englyst HN. Fermentation in the human large intestine and the available substrates. Am J Clin Nutr, 1987,45: 1243-1255.
Cummings JH, Macfarlane GT. The control and consequences of bacterial fermentation in the human colon. J Appl Bacteriol, 1991, 70: 443-459.
Cummings JH, Roberfroid MB and members of the Paris Carbohydrate Group, et al. A new look at dietary carbohydrate: chemistry, physiology and health. Eur J Clin Nutr, 1997, 51: 417-423.
Czermak P, Ebrahimi M, Grau K, et al. Membrane-assisted enzymatic production of galactosyl- oligosaccharides from lactose in a continuous process. J Membr Sci, 2004, 232: 85-91.
Deguchi Y, Matsumoto K, Ito T and Watanuki, M. Effects of P, 1-4 galactooligosaccharides administration on defecation of healthy volunteers with constipation tendency. Japanese J Nutr, 1997, 55: 13-22.
De Fatima Viana S, Monteze Guimaraes V, 1 Chamel Jose. Hydrolysis of oligosaccharides in soybean flour by soybean α-galactosidase. Food Chem, 2005, 93: 665-670.
Egounlety M, Aworh, OC. Effect of soaking, dehulling, cooking and fermentation with Rhizopus oligosporus on the oligosaccharides, trypsin inhibitor, phytic acid and tannins of soybean (Glycine max Merr.), cowpea (Vigna unguiculata L. Walp) and groundbean (Macrotyloma geocarpa Harms). J Food Eng, 2003, 56: 249-254.
Ekvall J, Stegmark R, Nyman M. Content of low molecular weight carbohydrates in vining peas (Pisumsativum) related to harvest time, size and brine grade. Food Chem, 2006, 94: 513-519.
Elmidaoui A, Chay L, Tahaikt M, et al. Demineralisation for beet sugar solutions using an electrodialysis pilot plant to reduce melassigenic ions. Desalination, 2006, 189: 209-214.
Engfer MB, Stahl B, Finke B, et al. Human milk oligosaccharides are resistant to enzymatic hydrolysis in the upper gastrointestinal tract. Am J Clin Nutr, 2000, 71(6): 1589- 96.
Enevoldsen AD, Hansen E, Jonsson G. Enzyme recovery by crossflow electro-ultrafiltration. Desalination, 2006, 199:55-56.
Fane AG, Fell CJD, McDonogh RM et al. the fouling of membranes, 11~(th) Australasian Chemical Engineering Conference, Brisbane, 1983: 729-737. Fuller R, Gibson GR. Modification of the intestinal microflora using probiotics and prebiotics. Scandinavian J Gastroenterol, 1997, 32: 28-31.
Fishbein L, Kaplan M, Gough M. Fructo-oligosaccharides: a review. Vet Hum Toxicol, 1988, 30: 104-107.
Fourmentin S, Outirite M, Blach P, et al. Solubilisation of chlorinated solvents by cyclodextrin derivatives A study by static headspace gas chromatography and molecular modelling. J Haz Mater, 2007, 141: 92-97.
Freger V, Arnot TC, Howell JA. Separation of concentrated organic/inorganic salt mixtures by nanofiltration. J Membr Sci, 2000, 178: 185-193.
Frenzel 1, Holdik H, Stamatialis DF, et al. Chromic acid recovery by electro-electrodialysis I. Evaluation of anion-exchange membrane. J Membr Sci, 2005, 261: 49-57.
Frisa J, Price KR, Fenwick GR, et al. Improved method for the analysis of α-galactosides in pea seeds by capillary zone eletrophoresis comparation with high-performance liquid chromatography- triple - pulsed amperometric detection. J Chromatogr, 1996, 719: 213-219.
Fukumoto LR, Delaquis P, Girard B. Microfiltration and ultrafiltration ceramic membranes for apple juice clarification. J Food Sci, 1998, 63(5): 845-850.
Fukushima Y, Kawata Y, Hara H, et al. Effect of probiotic formula on intestinal immunoglobulin A production in healthy children. Int J Food Microbiol, 1998, 42: 39-44.
Fuller R, Gibson GR. Modification of the intestinal microflora using probiotics and prebiotics. Scand J Gastroenterol, 1997, 32 (Suppl): 28-31.
Garcia A, Alvarez S, Riera F. Sunflower oil miscella degumming with polyethersulfone membranes Effect of process conditions and MWCO on fluxes and rejections. J Food Eng, 2006, 74: 516-522.
Garcia Agudo JA, Garcia Cubero MT, Gonzalez Benito G, et al. Removal of coloured compounds from sugar solutions by adsorption onto anionic resins: equilibrium and kinetic study. Sep Purif Technol, 2002, 29: 199-205.
Gennadios A, McHugh TH, Weller CL et al. Edible coatings and films based on proteins. In: Krochta JM, Baldwin EA and Nisperos-Carriedo M (Eds.), Edible coatings and films to improve food quality. Technomic Publishing Company, Lancaster, PA, 1994, 201-277.
Gesan-Guiziou G, Jimenez A, Arcelin C. Cake properties in dead-end ultrafiltration of casein micelles determination of critical operating conditions. Desalination, 2006, 199: 20-22.
Gibson GR, Roberfroid MB. Dietary modulation of the human colonic microbiota: introducing the concept ofprebiotics. JNutr, 1995, 125: 1401-1412.
Gode F, Pehlivan E. Removal of chromium (III) from aqueous solutions using Lewatit S 100: The effect of pH, time, metal concentration and temperature. J Haz Mat, 2006, B136: 330-337.
Godevac D, Vujisic L, Mojovic M, et al. Evaluation of antioxidant capacity of Allium ursinum L. volatile oil and its effect on membrane fluidity. Food Chem, 2008, 107: 1692-1700.
Gomes A, Malcata F. Bifidobacterium spp. and Lactobacillus acidophilus: Biological, biochemical, technology and therapeutical properties relevant for use as probiotics. Trends Food Sci Technol, 1999, 10: 139-157.
Gong Y, Dai LM, Wang XL, et al. Effects of transport properties of ion-exchange membranes on desalination of 1,3-propanediol fermentation broth by electrodialysis. Desalination, 2006, 191: 193-199.
Gong Y, Tang Y, Wang XL, et al. The possibility of the desalination of actual 1,3-propanediol fermentation broth by electrodialysis. Desalination, 2004, 161: 169-178.
Gopal PK, Prasad J, Gill HS. Effects of the consumption of Bifidobacterium lactis HN019 (DR10TM) and galacto-oligosaccharides on the microflora of the gastrointestinal tract in human subjects. Nutr Res, 2003, 23:1313-1328.
Gote M, Umalkar H, Khan I, et al. Thermostable α-galactosidase from Bacillus stearothermophilus (NCIM 5146) and its application in the removal of flatulence causing factors from soymilk. Proc Biochem, 2004, 39: 1723-1729.
Goulas AK, Kapasakalidis PG, Sinclair HR, et al. Purification of oligosaccharides by nanofiltration. J Membr Sci, 2002, 209: 321-335.
Gokmen V, Serpen A. Equilibrium and kinetic studies on the adsorption of dark colored compounds from apple juice using adsorbent resin. J Food Eng, 2002, 53: 221-227.
Grandison AS. Application of ion-exchange in food processing. Food Technol Int Europe, 1994: 53-57.
Grebenyuk VD, Chebotareva RD, Peters S, et al. Surface modification of anion-exchange electrodialysis membranes to enhance anti-fouling characteristics. Desalination, 1998, 115: 313-329.
Guadix A, S(?)rensen E, Papageorgiou LG, et al. Optimal design and operation of continuous ultrafiltration plants. J Membr Sci, 2004, 235: 131-138.
Guigoz Y, Rochat F, Perruisseau-Carrier G, et al. Effects of oligosaccharide on the faecal flora and nonspecific immune system in elderly people. Nutr Res, 2002, 22: 13-25.
Guimaraes VM, De Rezende ST, Moreira MA, et al. Characterization of a-galactosidases from germinating soybean seed and their use for hydrolysis of oligosaccharides. Phytochem, 2001, 58: 67-73.
Gupta, Y. P. Nutritive valueof soybean. Int J Tropical Agric, 1987, 5: 247-279.
Hamada JS. Large-scale high-performance liquid chromatography of enzymes for food applications. J Chromatogr, 1997,760:81-87.
Hameed BH, Ahmad A A, Aziz N. Isotherms, kinetics and thermodynamics of acid dye adsorption on activated palm ash. Chem Eng J, 2007, 133: 195-203.
Herman EM, Shannon L M. Accumulation and subcellular localization of a-galactosidase hemagglutinin in developing soybean cotyledons. Plant Physiol, 1985, 77: 886-890.
Hemwimon S, Pavasant P, Shotipruk A. Microwave-assisted extraction of antioxidative anthraquinones from roots of Morinda citrifolia. Sep Purif Technol, 2007, 54: 44-50.
Hidaka H, Tashiro Y, Eida T. Proliferation of bifidobacteria by oligosaccharides and their useful effect on human health. Bifidobact Microflora, 1991, 10(1): 65 - 79.
Hirata M, Gao M, Toorisaka et al. Production of lactic acid by continuous electrodialysis fermentation with a glucose concentration controller. Biochemical Eng J, 2005, 25: 159-163.
Ho CC, Zydney AL. A combined pore blockage and cake filtration model for protein fouling during microfiltration. J Colloid Interf Sci, 2000, 232: 389-399.
Ho YS, Mckay G. Pseudo-second-order model for sorption process. Process Biochem, 1999, 34: 451-465.
Houdijk JGM, Bosch MW, Verstegen MWA, et al. Effects of dietary oligosaccharides on the growth performance and faecal characteristics of young growing pigs. Animal Feed Sci Technol, 1998, 71: 35-48.
Hwang KJ, Chou FY, Tung KL. Effects of operating conditions on the performance of cross-flow microfiltration of fine particle/protein binary suspension. J Membr Sci, 2006, 274: 183-191.
Hwang KJ, Yu YH, Lu WM. Cross-flow microfiltration of submicron microbial suspension. J Membr Sci, 2001,194:229-243.
Ishibashi N, Shimamura S. Bifidobacteria: Research and development in Japan. Food Technol, 1993, 6:126-136.
Iyer V, Salunkhe DK, Sathe SK, et al. Quick cooking of beans (Phaseolus vulgaris, L.): phytates, oligosaccharides, antienzymes. Quality Plant Foods Human Nutr, 1980, 30: 45-52.
Jensen PE, Ottosen LM, C Ferreira, et al. Kinetics of electrodialytic extraction of Pb and soil cations from a slurry of contaminated soil fines. J Hazardous Materials, 2006, 138(3): 493-499.
Jeon YJ, Kim SK. Production of chitooligosaccharides using an ultrafiltration membrane reactor and their antibacterial activity. Carbohydrate Polymers, 2000, 41: 133-141.
Kaneko T, Mori H, Iwata M, et al. Growth stimulator for bifidobacteria produced by Propionibacterium freudenreichii and several intestinal bacteria. J Dairy Sci, 1994, 77: 393-404.
KanthaD. Role of bifidobacteria in nutrition, medicine and technology. Nutr Res, 1999, 19(11): 1559-1597.
Kapiki A, Costalos C, Oikonomidou C, et al. The effect of a fructo-oligosaccharide supplemented formula on gut flora of preterm infants. Early Hum Dev, 2007, 83: 335-339.
Karthikeyan T, Rajgopal S, Miranda LR. Chromium (VI) adsorption from aqueous solution by Hevea Brasilinesissawdust activated carbon. J Haz Mat B, 2005, 124, 192-199.
Kim DW, Kim TS, Jeong YK, et al. Adsorption kinetics and behaviors of cellulase components on microcrystalline cellulose. J Ferment Bioeng, 1992, 73: 461-466.
Kim 1C, Kim JH, Lee KH, et al. Phospholipids separation (degumming) from crude vegetable oil by polyimide ultrafiltration membrane. J Membr Sci, 2002, 205: 113-123.
Kim JS, Laskowich ER, Arumugham RG, et al. Determination of saccharide content in pneumococcal polysaccharides and conjugate vaccines by GC-MSD. Anal Biochem, 2005, 347: 262-274.
Kim KJ, Fane AG, Fell CJD, et al. Fouling mechanisms of menbranes during protein ultrafiltration. J Membr Sci, 1992,68:79-91.
Kinsella JE. Functional properties of soy proteins. J Am Oil Chemists' Society 1979, 56: 242-258.
Krishna Kumar NS, Yea MK, Cheryan M. Ultrafiltration of soy protein concentrate: performance and modelling of spiral and tubular polymeric modules. J Membr Sci, 2004, 244: 235-242.
Krol JJ, Wessling M, Strathmann H, et al. Concentration polarization with monopolar ion exchange membranes: current-voltage curves and water dissociation. J Membr Sci, 1999, 162: 145-154.
Kuberkar VT, Davis RH. Microfiltration of protein-cell mixtures with crossflushing or backflushing. J Membr Sci, 2001, 183: 1-14.
Kumar KV, Kumaran A. Removal of methylene blue by mango seed kernel powder. Biochem Eng J, 2005, 27, 83-93.
Kunz C, Rudloff S. Biological functions of oligosaccharides in human milk. Acta Paediatr, 1993, 82:903-12.
Lacour S, Bollinger JC, Serpaud B, et al. Removal of heavy metals in industrial wastewaters byion- exchanger grafted textiles. Anal Chim Acta, 2001, 428: 121-132.
Lacour S, Serpaud B, Bollinger JC. Performance of ion-exchanger grafted textiles for industrial water treatment in dynamic reactors. Water Res, 2004, 38: 4045-4054.
Langmuir I. The adsorption of gases on plane surfaces of glass, mica and platinum. J American Chem Society, 1918, 40: 1361-1402.
Lasekan OO, Idowu MA, Lasekan W. Effect of germination and degree of grind (coarse/fine) on the extract and sugar contents of sorghum malts. Food chem, 1995, 53: 125-128.
Lee DN, Miranda MG, Merson RL. Scanning electron microscope studies of membrane deposits from whey ultrafiltration. J Food Technol, 1975,10: 139.
Lee H, Amy G, Cho J, et al. Cleaning strategies for flux recovery of an ultrafiltration membrane fouled by natural organic matter. Wat Res, 2001, 35(14): 3301-3308.
Lee HJ, Sarfert F, Strathmann H, et al. Designing of an electrodialysis desalination plant. Desalination,2002, 142:267-286.
Lee HJ, Strathmann H, Moon SH. Determination of the limiting current density in electrodialysis desalination as an empirical function of linear velocity. Desalination, 2006, 190: 43-50.
Lee HJ, Strathmann H, Moon SH. Determination of the limiting current density in electrodialysis desalination as an empirical function of linear velocity. Desalination, 2006,190: 43-50.
Li H, Bo C, Zhang Z et al. Focused microwave-assisted solvent extraction and HPLC determination of effective constituents in Eucommiaulmodies Oliv.(E. ulmodies). Talanta, 2004, 63: 659-665.
Li ZY, Youravong W, H-Kittikun A. Separation of proteases from yellowWn tuna spleen by ultraWltration. Bioresour Technol, 2006, 97: 2364-2370.
Lin CJ, Shirazi S, Rao P, et al. Effects of operational parameters on cake formation of CaSO_4 in nanofiltration. Water Res, 2006, 40: 806-816.
Lin WF, Chen CH. Clarification of cane juice by ion exchange resins. Taiwan Sugar, 1991, 38: 17-22.
Lobo A, Cambiella A, Benito JM, et al. Ultrafiltration of oil-in-water emulsions with ceramic membranes: Influence of pH and crossflow velocity. J Membr Sci, 2006, 278: 328-334.
Longe OG. Carbohydrate composition of different varieties of cowpea (Vigna unguiculata). Food Chem, 1980, 6: 153-161.
Lowell CA, Kuo TM. Oligosaccharide metabolism and accumulation in developing soybean seeds. Crop Sci, 1989,29:459-465.
Lozano MJ, Martin J. Aspectos nutricionales de la lactancia materna. Acta Pediatr Esp 1998, 56(1): 24-32.
Lopez Leiva MH, Guzman M. Formation of Oligosaccharides during enzymic hydrolysis of milk whey permeates. Process Biochem, 1995, 30(8): 757-762.
Lundquist B, Nord CE, Winberg J. The composition of the faecal microflora in breastfed and bottle fed infants from birth to eight weeks. Acta Paediatrica Scand, 1985, 30: 470-475.
Lyndon R. Commercialization of Adsorbertechnology in the fruit juice industry. Fruit Process, 1996, 6:130-134.
Machaiah JP, Pednekar MD. Carbohydrate composition of low dose radiation-processed legumes and reduction in flatulence factors. Food Chem, 2002, 79: 293-301.
Marathe SA, Rao VS, Thomas P. Nutritional value and acceptability of irradiated legumes- in Proceedings of International Conference on Application of Radioisotopes and Radiation in Industrial Development (ICARID-98). 1998: 219-222.
Marshall AD, Munro PA, Tragardh G. The effect of protein fouling in microfiltration and ultrafiltration on permeate flux, protein retention and selectivity: A literature review. Desalination, 1993, 91: 65-108.
Martinez-Ferez A, Rudloff S, Guadix A, et al. Goats' milk as a natural source of lactose-derived oligosaccharides: isolation by membrane technology. Int Dairy J, 2006, 16: 173-181.
Martins, SIFS, Van Boekel, MAJS. A kinetic model for the glucose/glycine maillard reaction pathways. Food Chem, 2005, 90: 257-269.
Martinez-Villaluenga C, Frias J, Vidal-Valverde C. Raffinose family oligosaccharides and sucrose contents in 13 Spanish lupin cultivars. Food Chem, 2005, 91: 645-649.
Martinez-Villaluenga C, Frias J, Vidal-Valverde C. Raffinose family oligosaccharides and sucrose contents in 13 Spanish lupin cultivars. Food Chem 2005, 91: 645-649.
Maxwell FJ, Duncan SH, Hold G, et al. Isolation, growth on prebiotics andprobiotic potential of novel bifidobacteria from pigs. Anaerobe, 2004, 10: 33-39.
Ma CY, Liu WS, Kwok KC, et al. Isolation and characterization of proteins from soymilk residue (okara). Food Res Int, 1997, 29: 799-805.
Meenakshi S, Viswanathan N. Identification of selective ion-exchange resin for fluoride sorption. J Colloid Interface Sci, 2007, 308: 438-450.
Messina M, Barnes S. The role of soybean products in reducing cancer risks. J Natl Cancer Inst, 1991, 83:541-6.
Metsamuuronen S, Nystrom M. Evaluation of six flat sheet ultrafiltration membranes for fractionation of whey proteins. Desalination, 2006, 200: 290-291.
Miguel H., Leiva L, Guzman M. Formation of oligosaccharides during enzymic hydrolysis of milk whey permeates. Proc Biochem, 1995, 30(8): 757-762.
Mikkelsen LL, Jakobsen M, Jensen BB. Effects of dietary oligosaccharides on microbial diversity and fructo-oligosaccharide degrading bacteria in faeces of piglets post-weaning. Animal Feed Sci Technol, 2003, 109: 133-150.
Mikkelsen LL, Jensen BB. Effect of fructo-oligosaccharides and transgalacto-oligosaccharides on microbial populations and microbial activity in the gastrointestinal tract of piglets post-weaning. Animal Feed Sci Technol, 2004, 117: 107-119.
Mitchell DA, Doelle HW, Greenfield PF. Agar plate growth studies of Rhizopus oligosporus and Aspergillus oryzae to determine their suitability for solid state fermentation. Appl Microbial Biotechnol, 1988,28:598-602.
Mitsuoka, T. Intestinal Flora and Aging. Nutr Rev, 1992, 50: 438-446.
Mondor M, Girard B, Moresoli C. Modeling flux behavior for membrane filtration of apple juice, Food Res Int, 2000, 33: 539-548.
Morales FJ, Jimenez-Perez, S. Peroxyl radical scavenging activity of melanoidins in aqueous systems. Eur Food Res Technol, 2004, 218: 515-520.
Mosenthin R, Bauer E. The potential use of prebiotics in pig nutrition. Asian-Australas J Anim Sci, 2000,13:315-325.
Mountzouris KC, Xypoleas I, Kouseris I, et al. Nutrient digestibility, faecal physicochemical characteristics and bacterial glycolytic activity of growing pigs fed a diet supplemented with oligofructose or trans-galactooligosaccharides. Livestock Sci, 2006, 105: 168 - 175.
Moure A, Dominguez H, Parajo JC. Antioxidant properties of ultrafiltration-recovered soy protein fractions from industrial effluents and their hydrolysates. Process Biochem, 2006, 41: 447-456.
Moure A, Sineiro J, Dominguez H. Extraction and functionality of membrane-concentrated protein from defatted Rosa rubiginosa seeds. Food Chem, 2001, 74: 327-339.
Mourouzidis-Mourouzis SA, Karabelas AJ. Whey protein fouling of microfiltration ceramic membranes-Pressure effects. J Membr Sci, 2006, 282: 124-132.
Mubarak AE. Nutritional composition and antinutritional factors of mung bean seeds (Phaseolus aureus) as affected by some home traditional processes. Food Chem, 2005, 89: 489-495.
Mulimani VH, Devendra S. Effect of soaking, cooking and crude α-galactosidase treatment on the oligosaccharide content of red gram flour. Food Chem, 1998, 61: 475-479.
Mulimani VH, Thippeswamy S, Ramalingam S. Enzymatic degration of oligosaccharides in soybean flours. Food Chem, 1997, 59: 279-282.
Mulyowidarso RK, Fleet GH and Buckle KA.Changes in the concentration of carbohydrates during the soaking of soybeans for tempe production. Int J Food Sci Technol, 1991, 26: 595-606.
Mul AJ, Perry FG. The role of fructo-oligosaccharides in animal nutrition. In: Garnsworthy, P.C., Cole, D.J.A. (Eds.), Recent Advances in Animal Nutrition, Nottingham University Press, Loughborough. 1994:57-79.
Nakao S, Kimura S. Models of membrance transport phenomena and their application for ultrafiltration Data. J. Chem Eng Japan, 1982, 15: 200.
Newburg DS. Do the binding properties of oligosaccharides in milk protect human infants from gastrointestinal bacteria? J Nutr, 1997, 127: 980S- 4S.
Noomhorm A, Kupongsak S, Chandrkrachang S. Deacetylated chitin used as adsorbent in production of clarified pineapple syrup. J Sci Food Agric, 1998, 76: 226-232.
Noordman TR, Kooiker K, Bel W, et al. Concentration of aqueous extracts of defatted soy flour by ultrafiltration. Effect of suspended particles on the filtration flux. J Food Eng, 2003, 58: 135-141.
Obendorf RL. Oligosaccharides and galactosyl cyclitols in seed desiccation tolerance. Seed Sci Res, 1997, 7: 63-74.
Olguin MC, Hisano N, D'Ottavio AE, et al. Nutritional and antinutritional aspects of an Argentinian soy flour assessed on weanling rats. J Food Compos Anal, 2003, 16: 441-449.
Onigbinde AO, Akinyele IO. Oligosaccharide content of 20 varieties of cowpeas in Nigeria. J Food Sci, 1983,48:1250-1251,1254.
Onyenekwe PC, Njoku GC, Ameh DA. Effect of cowpea (Vigna unguiculata) processing methods on flatus causing oligosaccharides. Nutr Res, 2000, 20(3):349-358.
Ozturk N, Bektas TE. Nitrate removal from aqueous solution by adsorption onto various materials. J Haz Mat, 2004, B112: 155-162.
Pafylias I, Cheryan M, Mehaia MA, et al. Microfiltration of milk with ceramic membranes. Food Res Int, 1996,29:141-146.
Pagliero C, Ochoa N, Marchese J, et al. Vegetable oil degumming with polyimide and polyvinilidenfluoride ultrafiltration membranes. J Chemical Technol Biotechnol, 2004, 79: 148-152.
Pan X, Niu G, Liu H. Microwave-assisted extraction of tea polyphenols and tea caffeine from green tea leaves. Chem Eng Proc, 2003, 42: 129-133.
Pan XJ, Niu HZ, Jia GH, et al. Microwave-assisted extraction of glycyrrhizic acid from licorice root. Biochem Eng J, 2000, 5: 173-177.
Pan XJ, Niu HZ, Liu Hui. Comparison of microwave-assisted extraction and conventional extraction techniques for the extraction of tanshinones from Salvia miltiorrhiza bunge. Biochem Eng J, 2002, 12:71-77.
Passounaud M, Bollinger JC, Serpaud B, et al Water nitrate removal with ion-exchanger grafted textiles. Environ Technol, 2000, 21: 745-753.
Patil G, Raghavarao KSMS. Integrated membrane process for the concentration of anthocyanin. J Food Eng, 2007, 78: 1233-1239.
Paugam L, Rabiller-Baudry M, Delaunay D. Physico-chemical effect of simple alkaline and acid solutions in cleaning sequences of spiral ultrafiltration membranes fouled by skim milk. Desalination, 2006,200: 192-194.
Pohl P. Application of ion-exchange resins to the fractionation of metals in water. Trends Anal Chem, 2006, 25:31-43.
Pool-Zobel B, Van Loo J, Rowland I et al. Experimental evidences on the potential of prebiotic fructans to reduce the risk of colon cancer. Br J Nutr, 2002, 87: S273-81.
Poulin JF, Araya-Farias M, Amiot J, et al. Separation of bioactive peptides by electrodialysis with ultrafiltration membrane. Desalination, 2006, 200: 620.
Pouliot M, Pouliot Y, Britten M, et al. Effects of pH and ionic environment on the permeability and rejective properties of an alumina microfiltration membrane for whey proteins. J Membr Sci, 1994, 95:125-134.
Pradhan J, Das SN, Thakur RS. Adsorption of Hexavalent Chromium from Aqueous Solution by Using Activated Red Mud. J Colloid Interf Sci, 1999, 217(1): 137-141.
Prinyawiwatkul W, Beuchat LR, McWatters KH, et al. Changes in fatty acid, simple sugar, and oligosaccharide content of cowpea (Vigna unguiculata) flour as a result of soaking, boiling, and fermentation with Rhizopus microsporus var. oligosporus. Food Chem, 1996, 57: 405-413.
Qiu N, Guo S, Chang Y. Study upon kinetic process of apple juice adsorption decolouration by using adsorbent resin. J Food Eng, 2007, 81: 243-249.
Rai P, Majumdar GC, Das Gupta S, et al. Effect of various pretreatment methods on permeate flux and quality during ultrafiltration of mosambi juice. J Food Eng, 2007, 78: 561-568.
RautenbachR.膜工艺-组件和装置设计基础.1998.第一版.北京：化学工业出版社.
Reddy NR, Salunkhe DK. Changes in oligosaccharide during germination and cooking of Black Gram and fermentation of Black Gram/Rice Blend. Cereal Chem, 1980, 57: 356-360.
Redondo-Cuenca A, Villanueva-Suarez MJ, Rodriguez-Sevilla MD, et al. Chemical composition and dietary fibre of yellow and green commercial soybeans (Glycine max). Food Chem, 2006, 101: 1216-1222.
Refstie S, Sahlstrom S, E Brathen, et al. Lactic acid fermentation eliminates indigestible carbohydrates and antinutritional factors in soybean meal for Atlantic salmon (Salmo salar). Aquaculture, 2005, 246: 331-345.
Rhim, JW, Gennadios A, Handa A, et al. Solubility, tensile, and color properties of modified soy protein films. J Agric Food Chem, 2000, 48: 4937-4941.
Rivero-Urgell M, Santamaria-Orleans A. Oligosaccharides: application in infant food. Early Hum Dev, 2001,65 Suppl.:S43-S52.
Rodriguez M, Gonzalez-Munoz MJ, Luque S, et al. Extractive ultrafiltration for the removal of carboxylic acids. J Membr Sci, 2006, 274: 209-218.
Rowland IR, Rummey CJ, Coutts JT. Effect of Bifidobacterium longum and inulin on gut bacterial metabolism and carcinogen-induced aberrant crypt foci in rats. Carcinogenesis, 1998, 19: 281-285.
Ruiz-Lopez MA, Garcia-Lopez PM, Castaneda-Vazquez H, et al. Chemical composition and antinutrient content of three lupinus species from Jalisco, Mexico. J Food Compos Anal, 2000, 13: 193-199.
Ruiz-Matute AI, Sanz ML, Martinez-Castro I. Use of gas chromatography-mass spectrometry for identification of a new disaccharide in honey. J Chromatogr A, 2007, 1157: 480-483.
Ruiz-Teran F, Owens JD. Fate of oligosaccharides during production of soya bean tempe. J Sci Food Agric, 1999,79:249-252.
Saavedra JM, Bauman NA, Oung 1, et al. Feeding of Bifidobacterium bifidum and Streptococcus thermophilus to infants in hospital for prevention of diarrhea and shedding of rotavirus. Lancet, 1994,344: 1046-1049.
Sadrzadeh M, Razmi A, Mohammadi T. Separation of different ions from wastewater at various operating conditions using electrodialysis. Sep Purif Technol, 2007, 54(2): 147-156.
Sako T, Matsumoto K, Tanaka R. Recent progress on research and applications of non-digestible galacto-oligosaccharides. Int Dairy J, 1999, 9: 69-80.
Saltzman JR, Russell RM. The aging gut. Nutritional issues. Gastroenterol Clin North Am 1998, 27:309-24.
Sata T, Kawamura K, Higa M, et al. Electrodialytic transport properties of cation exchange membranes in the presence of cyclodextrins. J Membr Sci, 2001, 183: 201-212.
Sayed Razavi SK, Harris JL, Sherkat F. Fouling and cleaning of membranes in the ultrafilation of the aqueous extract of soy flour. J Membr Sci, 1996, 114: 93-104.
Sayed Razavi SK, Harris JL. Shear controlled model of the ultrafilation of soy suspensions. J Membr Sci, 1996,118:279-288.
Sanchez-Mata MC, Camara Hurtado MM, Diez-Marques C. Effect of domestic processes and water hardness on soluble sugars content of chickpeas (Cicer arietinum L.). Food Chem, 1999, 65: 331 -338.
Scalabrini P, Rossi M, Spettoli P, et al. Characterization of Bifidobacterium strains for use in soymilk fermentation. Int J Food Microbiol, 1998, 39: 213-219.
Schiffrin EJ, Brassart D, Servin AL, et al. Immune modulation of blood leukocytes in humans by lactic acid bacteria: criteria for strain selection. Am J Clin Nutr, 1997, 66: 515S-S20.
Schiffrin EJ, Rochat F, Link-Amster H, et al. Immuno-modulation of human blood cells following theingestion of lactic acid bacteria. J Dairy Sci, 1995, 78: 491-497.
Scordino M, Mauro AD, Passerini A. Highly purified sugar concentrate from a residue of citrus pigments recovery process. LWT, 2007, 40: 713-721.
Seo WG, Pae HO, Kim NY, et al. Synergistic cooperation between water soluble chitosan oligomers and interferon-g for induction of nitric oxide synthesis and tumoricidal activity in murine peritoneal macrophages. Cancer Lett, 2000, 159: 189-95.
Serpen A, Atac B, Gokmen V. Adsorption of Maillard reaction products from aqueous solutions and sugar syrups using adsorbent resin. J Food Eng, 2007, 82: 342-350.
Shallo HE, Rao A, Ericson AP, et al. Preparation of soy protein concentrate by ultrafiltration. J Food Sci, 2001,66:242-246.
Shu YY, Ko MY, Chang YS. Microwave-assisted extraction of ginsenosides from ginseng root. Microchem J, 2003,74: 131-139.
Sinniah UR, Ellis RH, John P. Irrigation and Seed Quality Development in Rapid-cycling Brassica: Soluble Carbohydrates and Heat-stable Proteins. Ann Botany, 1998, 82: 647-655.
Snir R, Koehler PE, Sims KA, et al. pH and cations influence permeability of marsh grapefruit pectinerase on polysulfone ultrafiltration membrane. J Agric Chem, 1995, 43: 1155-1162.
Stark AH, Madar Z. In vitro production of shortchain fatty acids by bacterial fermentation of dietary fiber compared with effects of those fibers on hepatic sterol synthesis in rats. J Nutr, 1993, 123: 2166-2173.
Strathmann H. Electrodialysis and its application in the chemical process industry,.Sep Purif Meth, 1985,14(1): 44-66.
Strathmann H. Ion-exchange Membrane Separation Processes, Elsevier, Amsterdam, 2004.
Strickling JA, Harmon DL, Dawson KA, et al. Evaluation of oligosaccharide addition to dog diets: influences on nutrient digestion and microbial populations. Animal Feed Sci Technol, 2000, 86: 205-219.
Silva HC, Braga GL. Effect of soaking and cooking on the oligosaccharide content of dry beans (Phaseolus vulgaris L.). J Food Sci, 1982, 47: 924-925.
Somiari RI, Balogh E. Effect of soaking, cooking and crude α-galactosidase treatment on the oligosaccharide content of cowpea flours. J Sci Food Agric, 1993, 61: 339-343.
Susanto H, Ulbricht M. Insights into polysaccharide fouling of ultrafiltration Membranes. Desalination, 2006,200:181-182.
Tang CH, Wu H, Chen Z, et al. Formation and properties of glycinin-rich and β-conglycinin-rich soy protein isolate gels induced by microbial transglutaminase. Food Res Int, 2006, 39: 87-97.
Tanka Y. Concentration polarization in ion-exchange membrane electrodialysis-the events arising in a flowing solution in a desalting cell. J Membr Sci, 2003, 216: 149-164.
Taper HS, Roberfroid M. Influence of inulin and oligofructose on breast cancer and tumor growth. J Nutr, 1999, 129:1488S-1491S.
Tomomatsu H. Health effects of oligosaccharides. Food Technol, 1994, 10: 61-65.
Tomomatsu H. Health effects of oligosaccharides. Food Technol, 1994, 48(10): 61- 5.
Torres MR, FR Marin, Ramos AJ. Study of operating conditions in concentration of chicken blood plasma proteins by ultrafiltration. J Food Eng, 2002, 54: 215-219.
Trugo LC, Farah A, Cabral L. Oligosaccharides distribution in Brazilian soya bean cultivars. Food Chem, 1995,52:385-387.
Trugo LC, Ramos LA, Trugo NMF,et al. Oligosaccharide composition and trypsin inhibitor activity of Phaseolus vulgaris and e.ect of germination on the α-galactoside composition and fermentation in human colon. Food Chem, 1990, 36: 53-61.
Uwaegbute AC, Iroegbu CU, Eke O. Chemical and sensory evaluation of germinated cowpeas (Vigna unguiculata) and their products. Food Chem, 2000, 68: 141-146.
Ushikubo FY, Watanabe AP, Viotto LA. Effects of operating conditions and enzyme treatment on fouling and polarized layer formation during umbu (Spondias tuberosa An. Cam.) juice microfiltration. Desalination, 2006, 200: 546-548.
Unlu N, Ersoz M. Removal of heavy metal ions by using dithiocarbamatedsporopollenin. Sep Purif Technol, 2007, 52: 461-469.
De Van Lisdonk CAC, Van Paassen JAM, Schippers JC, et al. Monitoring scaling in nanofiltration and reverse osmosis membrane systems. Desalination, 2000, 132: 101-108.
Valerdi-Perez R, Ibanez-Mengual JA. Current-voltage curves for an electrodialysis reversal pilot plant: determination of limiting currents. Desalination, 2001, 141: 23-37.
Vaccari G, Lodi G, Tamburini E, et al. Chromatographic Separations in Sugar Analysis and Processes Detection of oligosaccharides in sugar products using planar chromatography. Food Chem, 2001, 74: 99-110.
Vegas R, Moure A, Dominguez H, et al. Purification of oligosaccharides from rice husk autohydrolysis liquors by ultra- and nano-filtration. Desalination, 2006, 199: 541-543.
Velazquez M, Davies C, Marett R, et al. Effect of oligosaccharides and fibre substitutes on short-chain fatty acid production by human faecal microflora. Anaerobe, 2000, 6: 87-92.
Vera E, Dornier M, Ruales J, et al. Comparison between different ion exchange resins for the deacidification of passion fruit juice. J Food Eng, 2003, 57: 199-207.
Vera E, Ruales J, Dornier M, et al. Comparison of different methods for deacidification of clarified passion fruit juice. J Food Eng, 2003, 59: 361-367.
Vera E, Sandeaux J, Persin F, et al. Deacidification of clarified tropical fruit juices by electrodialysis. Part I. Influence of operating conditions on the process performances. J Food Eng, 2007, 78: 1427-1438.
Vera E, Sandeaux J, Persin F, et al. Deacidification of clarified tropical fruit juices by electrodialysis. Part II. Characteristics of the deacidified juices. J Food Eng, 2007, 78: 1439-1445.
Vera E, Ruales J, Dornier M, et al. Comparison of different methods for deacidification of clarified passion fruit juice. J Food Eng, 2003, 59: 361-367.
Vijayakumari K, Siddhuraju P, Janardhanan K. Effect of soaking, cooking and autoclaving on phytic acid and oligosaccharide contents of the tribal pulse, Mucuna monosperma DC. ex. Wight. Food Chem, 1996, 55: 173-177.
Voragen AGJ. Technological aspects of functional foodrelated carbohydrates. Trends in Food Sci & Tech 1998,9:328-335.
Vyas PV, Shah BG. Separation of inorganic and organic acids from glyoxal by electrodialysis. Desalination, 2001, 140(1): 47-54.
Wang N, Daun JK. Effects of variety and crude protein content on nutrients and anti-nutrients in lentils (Lens culinaris). Food Chem, 2006, 95: 493-502.
Wang N, Lewis MJ, Brennan JG, et al. Effect of processing methods on nutrients and anti-nurtitional factors in cowpea. Food Chem, 1997, 58: 59-68.
Wang X, Zhang C, Ouyang P. The possibility of separating saccharides from a NaCl solution by using nanofiltration in diafiltration mode. J Membr Sci, 2002, 204: 271-281.
Wisniewski J, Suder S. Water recovery from etching effluents for the purpose of rinsing stainless steel. Desalination, 1995, 101: 245-253.
Wisniewski J,Rozanska A.Donnan dialysis with anion-exchange membranes as a pretreatment step before electrodialytic desalination.Desalination,2006,191:210-218.
Xu L,Lamb K,Layton L,Kumar A.A membrane-based process for recovering isoflavones from a waste stream of soy processing.Food Res Int,2004,37:867-874.
Xu Y,Lebrun RE.Comparison of nanofiltration properties of two membranes using electrolyte and non-electrolyte solutes.Desalination,1999,122:95-106.
Xu T.Ion exchange membranes:State of their development and perspective.J Mere Sci,2005,263:1-29
Yazicigil Z,Oztekin Y.Boron removal by electrodialysis with anion-exchange membranes.Desalination,2006,190:71-78.
Zhang F,Chert B,Xiao S,et al.Optimization and comparison of different extraction techniques for sanguinarine and chelerythrine in fruits ofMacleaya cordata(Willd).R Br Sep PurifTechnol,2005,42:283-290.
Zydney AL.Protein separation using membrane filtration:New opportunities for whey fractionation.Int Dairy J,1998,243-250.
曹凤芹,王少庸,刘荣.利用大豆废水提取功能性因子工艺技术.大豆通报,2005,4:25-26.
车向荣,岳文斌,臧建军等.功能性低聚糖对断奶仔猪腹泻的防治及生产性能的影响.中国兽医学报,2003,23(3):292-294.
陈浚,电渗析法处理含铅废水的研究,浙江工业大学,硕士学位论文,2004,05.01
陈文仙.腐竹生产与检验.福建轻纺,2005,3:15-19.
程桂石,汪群慧,齐虹等.pH值对电渗析法回收厨房垃圾发酵液中乳酸的影响.化工学报,2005,56(111):2200-2203.
崔岸,朱峰,黄惠华等.超滤法生产大豆分离蛋白的研究.食品科学,1996,17(11):18-22.
崔洪斌等.大豆生物活性物质的开发与应用.北京:中国轻工业出版社,2001,3:48-113.
董红兵.大豆加工中副产品的开发与应用(一)-大豆低聚糖的开发与应用.武汉商业服务学院学报,2003,12(4):13-14.
董玉枝.大豆低聚糖对高脂质过氧化的影响.中国老年杂志,1996,16:242-243.
冯志彪.大豆低聚糖及其在食品工业中的应用.山西食品工业,1998,4:5-8.
冯振宁,钟振声,王文铂.用离子色谱法提纯低聚糖的研究.广东化工,2004,4:38-40.
江洁,王文侠,栾广忠.大豆深加工技术.北京:中国轻工业出版社,2004:263-427.
甘林火,翁连进.氨基酸溶液脱盐技术的进展.福建化工,2002,4:72-73.
高安全,吴景远,梁伟.膜分离技术在大豆乳清回收中的应用.过滤与分离,2001,11(3):26-27.
高文宏,石彦国,高大维等.超滤法提取大豆低聚糖前处理的研究.中围粮油学报,2000,15(5):49-52.
高文宏,石彦国,李国基等.超滤法提取大豆低聚糖的研究.食品与发酵工业,2000,26(6):6-11.
高文宏,石彦国,李国基等.大豆低聚糖提取中超滤膜的选择.食品科学,2000,21(5):15-20.
高伟星,柳森.用超滤法提取大豆低聚糖的研究.大连民族学院学报,2005,7(1):95.
高以恒,叶凌碧.膜分离技术基础.北京:科学出版社,1989,236.
高英,单安山.大豆寡糖在肉仔鸡日粮中的应用.饲料研究,2004,5:11-13.
郭本恒,孔保华.保健与功能食品.哈尔滨:黑龙江科技出版社,1996:155.
郭敏亮,姜涌明.考马斯亮蓝显色液组分对蛋白质测定的影响.生物化学与生物物理进展,1996,23(6):558-561.
郭尧君.蛋白质电泳实验技术第二版.北京:科学技术出版社,2005:92-112.
郭尽力.大豆低聚糖的提取工艺研究.烟台大学学报(自然科学与工程版),2004,17(4):298-302.
郝健,刘德华.1,3-丙二醇发酵液电渗析法脱盐.过程工程学报,2005,5(1):36-39.
郝岩平,姜金斗,杨秀茹.HPLC法测定食品中大豆低聚糖的含量.中国甜菜糖业,2003,1:8-11.
何小维,薛新顺,罗发兴等.功能性大豆低聚糖分离纯化研究概况.食品研究与开发,2005,26(4):184-188.
黄海,杨瑞金,王璋.低聚木糖液脱色树脂的选择.食品与机械,2001(5):31-32.
黄海,杨瑞金,王璋.低聚木糖的脱色工艺.无锡轻工大学学报,2002,21(2):125-130.
黄进,夏继涛,张声华.大豆异黄酮、皂甙和低聚糖提取工艺研究.粮食与饲料工业,2002,9:36-38.
黄祥斌,于淑娟,高大维.几种离子交换树脂用于糖浆脱色的比较研究.食品科学,2001,22(4):11-13.
金丰秋,金其荣.低聚糖在饲料中的应用.中国饲料,1999,5:16.
金其荣,徐勤.大豆低聚糖生产、生理功能及其应用.食品科学,1994,11:7-12.
金华丽.大豆低聚糖制取及纯化工艺的研究.郑州工程学院学报,2001(2):35-38.
赖凤英,陈焕章,林福兰.离子交换树脂对糖浆脱色效能的评价.中国甜菜糖业,2000,6:12-14.
赖凤英,陈焕章,林福兰.用吸附等温线评价离子交换树脂的脱色效能.广西蔗糖,2000,2:31-33.
赖凤英,林庆生,许喜林等.活性炭对糖浆脱色效能的研究.中国甜菜糖业,1999,10:2-5.
兰建丽.大豆低聚糖生产工艺技术.大豆通报,2001,4:20-21.
李刚,焦凌霞,严晓艳.脱脂豆粕中大豆低聚糖制备工艺的研究.安徽农业科学,2006,15:3798-3814.
李耕,吴大宇,戴智河.膜技术在浓缩天然大豆低聚糖中的应用.膜科学与技术,2002,22(1):29-31.
丽娟,姚军虎,张周.功能性低聚糖及其在断奶仔猪饲养中的应用.饲料博览,2004,11:38-39.
李诗龙.腐竹食品的现代加工技术.粮油加工与食品机械,2005,3:72-75.
李里特.大豆加工与利用.北京:化学工业出版社,2003.
李玲,许多,赵国良等.大豆中生物物质的分离与分析的研究(Ⅰ)—用ODS柱高效液相色谱法测定大豆中的低聚糖.食品与发酵工业,1995,3:44-47.
李晓炼,刘志同,叶光.膜分离技术提取大豆乳清中的低聚糖.食品科技,1999,4:19-21.
李应彪,童军茂,翟金兰.膜及膜分离技术在食品工业中的应用.粮油加工与食品机械,2000,3(2):30-31.
梁冰,熊德鑫.双歧杆菌QJ405、乳杆菌QJ405在试管内对肠道致病菌抑杀效果的初步报告.中国微生态杂志,2000,12(5):269-271.
刘昌胜,邬行彦.超滤过程中操作条件的优化.膜科学与技术,1995,15(4):12-15.
刘国信,刘录声.膜法分离技术及其应用.北京:中国环境科学出版社.1991:115-177.
刘莉.超滤膜法处理大豆乳清废水工艺的研究.哈尔滨工业大学工程硕士学位论.20030901.
刘军,栾居科,李文涛.大豆低聚糖、乳清蛋白的提取.中国油脂,2002,27(4):45-49.
刘俏,范圣第.超滤处理豆腐废水阻力的研究.环境污染治理技术与设备,2005,6(2):49-52.
刘贤杰,陈福明.电渗析技术在酱油脱盐中的应用.中国调味品,2004,4:17-21.
刘祥.大豆低聚糖对肠道菌群结构调节的研究.中国微生态学杂志,2003,12:10-13.
刘欣,冯杰.大豆低聚糖的生理功能及其应用.中国饲料,2005,6:15-16.
刘永宁,范云鸽,施荣富等.交联聚丙烯酰多胺树脂的合成及脱色性能的研究.化学试剂,1994,16(4):215-217.
刘峥.微波法提取大豆中低聚糖的研究.食品研究与开发,2002,23(2):24-26.
马莺.大豆低聚糖的提取及酶改性的研究(博士论文).东北农业大学,2000.
马莺,骆承痒.大豆低聚糖生产中大豆乳清的预处理和超滤技术(Ⅱ).中国商办工业.2001,4:48-49.
马莺,骆承痒,吴昊.高效液相色谱法测定大豆乳清中大豆低聚糖.分析化学,1999,27(3):367.
马莺,骆承庠,肖志刚.超滤法提取大豆低聚糖的研究.粮油食品科技,2000,8(5):17-19.
毛跟年,柯蕾,李彦军等.离子交换法分离纯化麦芽低聚糖.食品工业科技,2005,26(4):127-128.
潘见,陈强,谢慧明等.大孔树脂对葛根黄酮的吸附分离特性研究.农业工程学报,1999,15(1):236-240.
钱庭宝,刘维林,李金和.吸附树脂及其应用.北京:化学工业出版社.1990,587-595.
秦志荣,于淑娟,高大维.糖浆脱色阴离子交换树脂再生新方法的研究.中国甜菜糖业,1999,8:10-13.
邵刚.膜法水处理技术(第2版).北京:冶金工业出版社,2001.
史锋.生物化学实验.杭州:浙江大学出版社,2002:1-3.
史宣明,赖本丽.大豆低聚糖的精制.中国油脂.2005,30(5):39-40.
石彦国.大豆制品工艺学.北京:中国轻工业出版社,2005:30-90.
唐宇,龚燕,王晓琳等.1,3-丙二醇发酵液电渗析脱盐的中试研究.化工进展,2004,23(1):84-87.
唐宇,龚燕,王晓琳等.1,3-丙二醇发酵液电渗析脱盐工艺的优化.水处理技术,2005,31(4):41-45.
田心健,钟世荣,张伟.酸沉淀法制取大豆低聚糖的工艺研究.四川轻化工学院学报,2001,14(3):75-78.
田三德,孙鹏.大豆低聚糖的生产及应用.实用技术,2003,10:18-19.
汪莉,苏军,苏宁.低聚糖对蛋雏鸡生长性能、免疫器官发育及粪臭的影响.黑龙江畜牧兽医,2001,11:9-11.
汪莉,苏宁,苏军等.低聚糖对蛋雏鸡生长性能及粪臭的影响.家畜生态,2002,23(1):30-32.
汪莉,罗淑琴,苏宁等.低聚糖对蛋雏鸡生长性能及粪臭的影响.畜牧与兽医,2002,34(6):6-8.
王炳南.用膜集成技术分离大豆低聚糖.水处理技术,2005,31(1):72-74.
王全军.低聚糖在动物饲养中的应用.中国饲料,2000,16:15-17.
王树勖,王立蓉.反渗透技术研究现状.甘肃科技,2005,21(12):187-188.
王水兴,夏慧玲,吴凌伟,晏有生.树脂法分离低聚木糖的研究.中国食品添加剂,2004,11:36-38.
王素敏.大豆低聚糖对大鼠血脂和抗氧化作用的影响.营养学报,1997,19(4):10-13.
王平,李立新,曹培刚等.浅谈反渗透脱盐的预处理.河北电力技术,2004,23(2):36-39.
王文侠,翟丽萍,张文超等.大豆低聚糖的制备工艺研究.中国乳品工业,1999,127(12):10-12.
王晓,张孝范.保健功能因子大豆低聚糖及其开发.西部粮油科技.1999,24(1):31-33.
王晓琳,张澄洪,欧阳平凯.应用纳滤膜分离糖和盐的实验研究.膜科学与技术,2001,21(1):44-48.
王晓忠,刘跃泉,任宏志.利用膜分离技术对大豆乳清废水综合利用.粮食与油脂,2004,4:45.
王学松.膜分离技术及其应用.北京:科学技术出版社,1994,7-10.
王元凤,金征宇.D315树脂分离茶多糖工艺的研究.农业工程学报,2005,21(10):147-150.
王湛.膜分离技术基础.北京:化学工业出版社,2000:1-6.
翁利荣,罗发兴,黄强等.低聚木糖脱色技术研究概括.食品科技,2004,7:51-54.
伍军,艾启俊,于同泉等.大豆黄浆水处理过程中超滤膜的选择.北京农学院学报,2003,18(3):223-225.
伍军,艾启俊,于同泉.应用纳滤膜分离大豆黄浆水的研究.粮油加工与食品机械,2004,3:56-60.
伍军,艾启俊,于同泉等.大豆黄浆水处理过程中超滤膜的选择.北京农学院学报,2003,18(3):17-19.
向东,王国政,赖凤英等.活性炭对南瓜粗多糖液的脱色研究.河南科学,2004,22(6):780-782.
辛嘉英.从豆腐黄浆水中提取大豆低聚糖.今日科技,1995,2:14.
熊泽,唐明,邵伟.大豆低聚糖的提取及其对乳酸菌生长影响的研究.现代食品科技,2005,4:25-27.
徐晓云,潘思轶,谢笔钧等.树脂法精制沙棘籽原花色素的研究.农业工程学报,2005,21(1):152-154.
徐勇,余世袁,勇强等.活性炭对低聚木糖的脱色.南京林业大学学报(自然科学版),2003,27(2):7-10.
徐忠,张洪微,韩玉洁.离子交换树脂对高麦芽糖浆的分离纯化研究.化学与黏合,2005,27(5):286-288.
徐忠,张亚丽.活性炭脱色对大豆低聚糖质量的影响.化学与粘合,2001,6:270-271.
徐超斗,梁爱君,祝业等.大豆低聚糖对免疫功能的促进作用.解放军药学学报,2005,21(1):37-39.
徐秀容,龚月生.低聚糖对早期断奶仔猪消化道微生物区系的调节作用.饲料工业,1999,20(6):31-32.
薛连海.气相色谱法测定大豆中低聚糖含量.分析化学,2003,31(3):382.
薛文通,王浩.功能性低聚糖-大豆低聚糖.食品研究与开发,2003,24(3):3-5.
姚文华,尹卓容.大枣多糖脱色的工业化试验.食品工业,2006,5:41-43.
杨汝德,张玲华,林晓珊等.大豆低聚糖的制取及其促生作用的研究.食品工业,1996,3:5-8.
杨云,刘福勤,冯卫生,孟江,田润涛.碱法提取大枣渣多糖及活性炭脱色的工艺研究.食品与发酵工业,2004,30(7):30-33.
叶桂安,杨希山.双歧杆菌及肠致病性大肠杆菌粘附的细胞膜通透性研究.中国微生态杂志,2000,12(3):132-133.
袁其朋,张恭孝,姜焱.树脂及活性碳吸附技术回收大豆乳清中的异黄酮和低聚糖.大豆科学,2003,22(1):6-10.
袁其朋,马润宇.膜分离技术处理大豆乳清废水.水处理技术,2001,27(3):161-163.
岳振峰,陈小霞,彭志英等.功能性低聚糖分离纯化方法概述.郑州工程学院学报,2001,22(1):89-92.
尤新.功能性低聚糖生产与应用.北京:中国轻工业出版社.2004:1-182.
张保平.饲用抗生素的替代品—低聚糖.河南畜牧兽医 2000,21(4):11-12.
张延坤,刘国忠.大豆低聚糖及其在食品工业的应用.食品工业,1999,3:5-8.
张延坤,房玉水,邓峰.用高效液相色谱法测定棉籽蛋白中的棉籽糖.食品工业,1996,3:58-59.
张延坤,张东祥,刘国忠等.高效液相色谱法测定大豆低聚糖.食品工业,2000,2:45-46.
张振红,黄仁录.大豆低聚糖的研究及其在饲料中的应用.兽药与饲料添加剂,2005,10(4):14-16.
赵冬梅,刘凌,张京健.豆制品生产中高浓度废水的检测与分析.食品与发酵工业,2006,32(1):
赵贵兴,陈霞,刘忠云等.大豆低聚糖制备工艺的研究.黑龙江农业科学,2002(2):13-15.68-71.
赵婧,冯骉.氨基酸溶液电渗析脱盐过程中的研究.2005,26(8):57-60.
赵丽颖,符群.膜分离技术在大豆乳清废水回收中应用.粮食与油脂,2002,9:48-49.
钟振声,冯焱,孙立杰等.柱色谱法对大豆低聚糖浆脱色效果的研究.精细化工,2006,23(6):565-568.
钟振声,冯三马,孙立杰等.柱色谱法对大豆低聚糖浆脱色效果的研究.精细化工,2006,23(6):565-567.
钟振声,王文铂.用离子交换树脂祛除低聚糖中的葡萄糖.化学与生物工程.2004,4:36-37.
周尽花,周春山.大孔吸附树脂法柚皮果胶脱色工艺研究.离子交换与吸附,2005,21(6):542-550.
周中凯.新型饲料添加剂—功能性低聚糖.广东饲料,1999,1:29-32.
周中凯,夏英.饲料用低聚糖的研究与认识.饲料研究,1999,3:3-6.
© 2004-2018 中国地质图书馆版权所有 京ICP备05064691号 京公网安备11010802017129号 地址：北京市海淀区学院路29号 邮编：100083 电话：办公室：(+86 10)66554848；文献借阅、咨询服务、科技查新：66554700 |