茜草植物染料染色莫代尔纤维的超声波处理
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摘要
为改善茜草植物染料染色莫代尔纤维的可纺性,采用超声波处理方法去除染色后纤维表面附着颗粒物,通过试验探讨超声波功率密度、温度、时间对颗粒物去除的影响。在此基础上选取试验因素和水平,用BoxBehnken试验设计方法,研究各变量及其交互作用对茜草植物染料染色纤维表面颗粒附着物去除的影响。结果表明:超声波处理温度对纤维表面颗粒物的去除影响最大,功率密度影响最小;利用Design Expert软件得到回归方程的预测模型对工业化处理有预测作用;超声波去除纤维表面颗粒物的最佳条件为超声波功率密度0. 67 W/cm2,超声波处理温度43℃,超声波处理时间22 min。
In order to improve the spinnability of the Modal fiber dyed with madder,ultrasonic treatment was employed to remove the attached particulate matters on the surface of the dyed fibers. The influence of ultrasonic power density,temperature and time on the removal of particulate matters was discussed by single factor test. The experimental factors and levels were selected on the basis of the single factor experiment. The effects of the variates and their interactions on the removal of attached particulate matters on the dyed fiber surface were then studied by the Box-Behnken experiment. The results show that ultrasonic temperature has the greatest effect on the removal of particulate matters on the surface of the fiber,and the influence of power density is the least. The prediction model of regression equation obtained by using Design Expert software has a predictive effect on industrialization. The optimum conditions for the ultrasonic particle removal are as follows: ultrasonic power density of 0. 67 W/cm~2,ultrasonic temperature of 43 ℃ and ultrasonic time of 22 min.
In order to improve the spinnability of the Modal fiber dyed with madder,ultrasonic treatment was employed to remove the attached particulate matters on the surface of the dyed fibers. The influence of ultrasonic power density,temperature and time on the removal of particulate matters was discussed by single factor test. The experimental factors and levels were selected on the basis of the single factor experiment. The effects of the variates and their interactions on the removal of attached particulate matters on the dyed fiber surface were then studied by the Box-Behnken experiment. The results show that ultrasonic temperature has the greatest effect on the removal of particulate matters on the surface of the fiber,and the influence of power density is the least. The prediction model of regression equation obtained by using Design Expert software has a predictive effect on industrialization. The optimum conditions for the ultrasonic particle removal are as follows: ultrasonic power density of 0. 67 W/cm~2,ultrasonic temperature of 43 ℃ and ultrasonic time of 22 min.
引文
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[14]王丽丽,高忠涛,杜冰,等.基于响应面法优化生物酶洗毛工艺[J].毛纺科技,2010,38(7):9-14.WANG Lili,GAO Zhongtao,DU Bing,et al. Enzymatic wool scouring optimization by response surface methodology[J]. Wool Textile Joumal,2010,38(7):9-14.
[15]刘齐,杜萍,王飞生,等.超声波法提取板栗壳多糖的工艺条件优化[J].食品工业科技,2014,35(3):221-224.LIU Qi,DU Ping,WANG Feisheng,et al. Study on ultrasonic extraction of polysaccharides in chestnut shell by response surface methodology[J]. Science and Technology of Food Industry,2014,35(3):221-224.
[16]赵玉萍,张娟,郭雅琳,等.基于响应面分析法的超声波洗涤羽毛纤维工艺条件优化[J].纺织学报,2012,33(7):24-30.ZHAO Yuping, ZHANG Juan, GUO Yalin, et al.Process optimization of ultrasonic washing of feather fibers based on response surface method[J]. Journal of Textile Research,2012,33(7):24-30.
[17]胡敏,刘凡清,张玉先.纤维滤料的超声波清洗技术研究[J].给水排水,2008,34(11):34-37.HU Min,LIU Fanqing,ZHANG Yuxian. Research of ultrasonic cleaning technology for fiber filter media[J].Water&Wastewater Engineering,2008,34(11):34-37.
[18] MOHANA S,SHRIVASTAVA S,DIVECHA J,et al.Response surface methodology for optimization of medium for decolorization of textile dye Direct Black 22by a novel bacterial consortium[J]. Bioresource Technology,2008,99(3):562-569.
[2]榕嘉.茜草的性能和染色试验[J].丝绸,2002(2):28-29.RONG Jia. The properties and dyeing experiments of madder[J]. Journal of Silk,2002(2):28-29.
[3]万震,周红丽.莫代尔散纤维染色技术[J].染整技术,2007,29(4):21-23.WAN Zhen,ZHOU Hongli. Dyeing of modal loose stock fibres[J]. Textile Dyeing and Finishing Journal,2007,29(4):21-23.
[4]刘祥霞,杜文琴,吴翠.植物染料分子状态与其上染关系[J].纺织学报,2013,34(9):84-88.LIU Xiangxia,DU Wenqin,WU Cui. Vegetable dyes:molecular status vs dyeing ability[J]. Journal of Textile Research,2013,34(9):84-88.
[5]肖敏,杨峰,王旭荣,等.分光光度法测定金黄色葡萄球菌菌液浓度方法的建立[J].动物医学进展,2014(11):40-43.XIAO Min, YANG Feng, WANG Xurong, et al.Establishment of concentration determination of Staphylococcus aureus by spectrophotometry[J].Progress in Veterinary Medicine,2014(11):40-43.
[6]毕延根,杨少峰.用紫外-可见分光光度计测定油样中沥青质含量[J].分析测试学报,2000,19(1):41-44.BI Yangen,YANG Shaofeng. Determination of asphaltene in petroleum by UV/VIS spectrophotometry[J]. Journal of Instrumental Analysis,2000,19(1):41-44.
[7] SHEIKH J,JAGTAP P S,TELI M D. Ultrasound assisted extraction of natural dyes and natural mordants vis a vis dyeing[J]. Fibers&Polymers,2016,17(5):738-743.
[8] VEDAR A N,SANDHYA K V,CHARUKESH N R B,et al. Ultrasonic extraction of natural dye from Rubia Cordifolia, optimisation using response surface methodology(RSM)&comparison with artificial neural network(ANN)model and its dyeing properties on different substrates[J]. Chemical Engineering&Processing Process Intensification,2017,114:46-54.
[9] KUSUMA H S,SUDRAJAT R G M,SUSANTO D F,et al. Response surface methodology(RSM)modeling of microwave-assisted extraction of natural dye from Swietenia mahagony:a comparation between BoxBehnken and central composite design method[J]. AIP Conference Proceedings,2015,1699(1):212-216.
[10]陆洋,彭飞,黄丽霞,等.响应面法优化超声辅助提取贯众多酚工艺[J].天然产物研究与开发,2015(1):103-108.LU Yang,PENG Fei,HUANG Lixia,et al. Optimization of ultrasonic-assisted extraction conditions of polyphenol from cyrtomium fortunei by response surface methodology[J]. Nat Prod Res Develop,2015(1):103-108.
[11]崔方玲,纪威.超声空化气泡动力学仿真及其影响因素分析[J].农业工程学报,2013,29(17):24-29.CUI Fangling,JI Wei. Dynamic simulation of ultrasonic cavitation bubble and analysis of its influencing factors[J]. Transactions of the Chinese Society of Agricultural Engineering,2013,29(17):24-29.
[12]高永慧,耿小丕.超声波清洗液温度变化规律的研究[J].承德石油高等专科学校学报,2005,7(3):39-41.GAO Yonghui,GENG Xiaopei. Temperature change of ultrasonic wave cleaning fluid[J]. Journal of Chengde Petroleum College,2005,7(3):39-41.
[13]尤丽霞,张羡,李丹,等.超声波处理对棉织物污渍去除的影响[J].纺织学报,2011,32(4):91-94.YOU Lixia,ZHANG Xian,LI Dan, et al. Effect of ultrasonic treatment on stain removal of cotton fabric[J].Journal of Textile Research,2011,32(4):91-94.
[14]王丽丽,高忠涛,杜冰,等.基于响应面法优化生物酶洗毛工艺[J].毛纺科技,2010,38(7):9-14.WANG Lili,GAO Zhongtao,DU Bing,et al. Enzymatic wool scouring optimization by response surface methodology[J]. Wool Textile Joumal,2010,38(7):9-14.
[15]刘齐,杜萍,王飞生,等.超声波法提取板栗壳多糖的工艺条件优化[J].食品工业科技,2014,35(3):221-224.LIU Qi,DU Ping,WANG Feisheng,et al. Study on ultrasonic extraction of polysaccharides in chestnut shell by response surface methodology[J]. Science and Technology of Food Industry,2014,35(3):221-224.
[16]赵玉萍,张娟,郭雅琳,等.基于响应面分析法的超声波洗涤羽毛纤维工艺条件优化[J].纺织学报,2012,33(7):24-30.ZHAO Yuping, ZHANG Juan, GUO Yalin, et al.Process optimization of ultrasonic washing of feather fibers based on response surface method[J]. Journal of Textile Research,2012,33(7):24-30.
[17]胡敏,刘凡清,张玉先.纤维滤料的超声波清洗技术研究[J].给水排水,2008,34(11):34-37.HU Min,LIU Fanqing,ZHANG Yuxian. Research of ultrasonic cleaning technology for fiber filter media[J].Water&Wastewater Engineering,2008,34(11):34-37.
[18] MOHANA S,SHRIVASTAVA S,DIVECHA J,et al.Response surface methodology for optimization of medium for decolorization of textile dye Direct Black 22by a novel bacterial consortium[J]. Bioresource Technology,2008,99(3):562-569.
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