UPC~2法测定不同滤嘴卷烟主流烟气中8种羰基化合物

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• 英文论文题名：Determination of Carbonyls in the mainstream smoke of different filter cigarette by UPC~2
• 论文作者：何君 ; 张亮 ; 王颖 ; 谢涛
• 英文论文作者：HE Jun ; ZHANG Liang ; WANG Ying ; XIE Tao ; Shenzhen Tobacco Industry co. ; ITD
• 年：2016
• 作者机构：深圳烟草工业有限责任公司技术中心;
• 论文关键词：超高效合相色谱 ; 卷烟烟气 ; 滤嘴 ; 羰基化合物
• 英文论文关键词：UPC~2 ; Cigarette smoke ; filter ; carbonyl compounds
• 会议召开时间：2016-12-01
• 会议录名称：中国烟草学会2016年度优秀论文汇编——卷烟材料主题
• 语种：中文
• 分类号：TS411
• 学会代码：ZGYG
• 学会名称：中国烟草学会
• 页数：6
• 文件大小：808k
• 原文格式：D

摘要

为了研究不同滤嘴在卷烟降焦减害中的作用,文章建立了超高效合相色谱(UPC~2)等度洗脱测定对卷烟主流烟气中8种羰基化合物的方法。结果表明,(1)UPC~2相对于传统的反相色谱,具有良好的正交选择性,8种羰基化合物具有良好的线性关系(R~2>0.999),加标回收率在79%~93%,检出限0.06~0.15μg/支。(2)加入了活性炭的滤嘴卷烟对8种羰基化合物的综合过滤效果最好。(3)滤嘴材料的选择是降低目标有害成分的关键。
In order to study the different filters in the effect of depressing the tar and reducing the harm. We developed an ultra performance convergence chromatography(UPC~2) for analyzing eight carbonyl compounds in cigarette smoke. The results showed that:(1)Comparing to conventional reverse-phase chromatography, this method has a good orthogonal selectivity. The eight carbonyl compounds displayed good linearity(R~2>0.999). The standard addition recoveries ranged from 79% to 93%. The limits of detection of ranged from 0.08 to 0.05 μg/cig.(2)The cigarette adding active carbon in filter tip have the best comprehensive filtering effect of eight carbonyl compounds.(3)Selecting the appropriate filter material is the key to reduce the target harmful components.

引文

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