水中砷形态分析研究进展
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摘要
砷是一种自然界中广泛存在的元素,砷的毒性与其存在形态密切相关.总结了近年来砷形态分析的研究进展,对水样中砷形态的分析方法和应用进行了综述.总结了水中不同形态砷的分离方法、光谱分析方法、液相色谱-光谱在线联用方法,以及对于不同形态痕量砷的样品预处理技术.
Arsenic is an element widely found in nature.The toxicity of arsenic is closely related to its form in existence.This paper summarizes the research progress of arsenic speciation analysis in recent years,and reviews the analytical methods and applications of arsenic speciation in water samples.In this paper,we also summarize the separation methods and spectral analysis methods of different speciation of arsenic in water.For trace arsenic speciation analysis,liquid chromatography coupled with spectroscopy on-line and the sample pretreatment techniques are also summarized.
Arsenic is an element widely found in nature.The toxicity of arsenic is closely related to its form in existence.This paper summarizes the research progress of arsenic speciation analysis in recent years,and reviews the analytical methods and applications of arsenic speciation in water samples.In this paper,we also summarize the separation methods and spectral analysis methods of different speciation of arsenic in water.For trace arsenic speciation analysis,liquid chromatography coupled with spectroscopy on-line and the sample pretreatment techniques are also summarized.
引文
[1]WEN S P,ZHU X S.Speciation of inorganic arsenic(Ⅲ)and arsenic(V)by a facile dual-cloud point extraction coupled with inductively plasma-optical emission spectrometry[J].Talanta,2018,181:265-270.
[2]BASHDAR S,FOULKES M E,HILL S J.Coupled techniques for arsenic speciation in food and drinking water:A review[J].J Anal At Spectrom,2015,30:102-118.
[3]LEAL P M,ALONSO E V,LóPEZ Guerrero M M,et al.Speciation analysis of inorganic arsenic by magnetic solid phase extraction on-line with inductively coupled mass spectrometry determination[J].Talanta,2018,184:251-259.
[4]KOMOROWICZ I,BARA?KIEWICZ D.Arsenic and its speciation in water samples by high performance liquid chromatography inductively coupled plasma mass spectrometry:Last decade review[J].Talanta,2011,84:247-261.
[5]ANAWARA H M.Arsenic speciation in environmental samples by hydride generation and electrothermal atomic abso rption spectrometry[J].Talanta,2012,88:30-42.
[6]MA J P,XIAO R H,LI J H,et al.Determination of 16polycyclic aromatic hydrocarbons in environmental water samples by solidphase extraction using multi-walled carbon nanotubes as adsorbent coupled with gas chromatography-mass spectrometry[J].J Chromatogr:A,2010,1217:5462-5469.
[7]马继平,李茉,赵秀华,等.固相萃取-反相高效液相色谱法测定水中的邻苯二甲酸酯[J].分析实验室,2009,28(3):6-9.MA Ji-ping,LI Mo,ZHAO Xiu-hua,et al.Determination of phthalate esters in water by SPE-RPHPLC[J].Chinese Journal of Analysis Laboratory,2009,28(3):6-9.(in Chinese)
[8]CHEN S Z,ZHAN X L,LU D B,et al.Speciation analysis of inorganic arsenic in natural water by carbon nanofibers separation and inductively coupled plasma mass spectrometry determination[J].Anal Chim Acta,2009,634(2):192-196.
[9]CHEN D H,HUANG C Z,HE M,et al.Separation and preconcentration of inorganic arsenic species in natural water samples with 3-(2-aminoethylamino)propyltrimethoxysilane modified ordered mesoporous silica micro-column and their determination by inductively coupled plasma optical emission spectrometry[J].J Hazard Mater,2009,164(2/3):1144-1151.
[10]LI P,ZHANG X Q,CHEN Y J,et al.One-pot synthesis of thiol-and aminebifunctionalized mesoporous silica and applications in uptake and speciation of arsenic[J].RSC Adv,2014,4:49421-49428.
[11]PENG H Y,ZHANG N,HE M,et al.Simultaneous speciation analysis of inorganic arsenic,chromium and selenium in environmental waters by 3-(2-aminoethylamino)propyltrimethoxysilane modified multi-wall carbon nanotubes packed microcolumn solid phase extraction and ICP-MS[J].Talanta,2015,131:266-272.
[12]ALI J,TUZEN M,TASNEEN G K,et al.Inorganic arsenic speciation in water samples by miniaturized solid phase microextraction using a new polystyrene polydimethyl siloxane polymer in micropipettetip of syringe system[J].Talanta,2016,161:450-458.
[13]MA J P,YAO Z D,HOU L W,et al.Metal organic frameworks(MOFs)for magnetic solid-phase extraction of pyrazole/pyrrole pesticides in environmental water samples followed by HPLC-DAD determination[J].Talanta,2016,161:686-692.
[14]MA J P,JIANG L H,WU G G,et al.Determination of six sulfonylurea herbicides in environmental watersamples by magnetic solidphase extraction using multi-walledcarbon nanotubes as adsorbents coupled with high-performanceliquid chromatography[J].J Chromatogr:A,2016,1466:12-20.
[15]侯丽玮,马继平,姜莲华.基于离子液体的磁性富集技术及其在分析化学中的应用进展[J].分析测试学报,2015,34(6):715-723.HOU Li-wei,MA Ji-ping,JIANG Lian-hua.Progresses in magnetic enrichment techniques based on ionic liquids and their applications in analytical chemistry[J].Journal of Instrumental Analysis,2015,34(6):715-723.(in Chinese)
[16]HUANG C Z,XIE W,LI X.Speciation of inorganic arsenic in environmental waters using magnetic solid phase extraction and preconcentration followed by ICP-MS[J].Microchim Acta,2011,173(1/2):165-172.
[17]MA J P,LU W H,CHEN L X.Recent advances in dispersive liquid-liquid microextraction for organic compounds analysis in environmental water:A review[J].Curr Anal Chem,2012,8(1):78-90.
[18]RICARDO E R,LPEZ-GARCA I,HERNNDEZ-CRDOBA M.Speciation of very low amounts of arsenic and antimony in waters using dispersive liquid-liquid microextraction and electrothermal atomic absorption spectrometry[J].Spectrochim Acta:Part B,2009,64(4):329-333.
[19]ZOUNR R A,TUZEN M,KHUHAWAR M Y.Ultrasound assisted deep eutectic solvent based on dispersive liquid liquid microextraction of arsenic speciation in water and environmental samples by electrothermal atomic absorption spectrometry[J].J MolLiq,2017,242:441-446.
[20]LI S,WANG M,ZHONG Y Z,et al.Cloud point extraction for trace inorganic arsenic speciation analysis in water samples by hydride generation atomic fluorescence spectrometry[J].Spectrochim Acta:Part B,2015,111:74-79.
[21]边静,徐芳,李玲辉,等.氢化物发生-原子荧光光谱法测定海水中As(III)和As(V)[J].光谱学与光谱分析,2010,30(10):2834-2837.BIAN Jing,XU Fang,LI Ling-hui,et al.Determination of As(III)and As(V)in sea water by hydride generation atomic fluorescence spectrometry[J].Spectroscopy and Spectral Analysis,2010,30(10):2834-2837.(in Chinese)
[22]LóPEZ-GARCíA I,MARíN-HERNáNDEZ J J,HERNáNDEZ-CóRDOBA M.Magnetic ferrite particles combined with electrothermal atomic absorption spectrometry for the speciation of low concentrations of arsenic[J].Talanta,2018,181:6-12.
[23]ULUSOY H I,AKCAY M,ULUSOY S,et al.Determination of ultra trace arsenic species in water samples by hydride generation atomic absorption spectrometry after cloud point extraction[J].Anal Chim Acta,2011,703(2):137-144.
[24]RAHMAN I M M,BEGUM Z A,NAKANO M,et al.Selective separation of arsenic species from aqueous solutions with immobilized macrocyclic material containing solid phase extraction columns[J].Chemosphere,2011,82(4):549-556.
[25]刘崴,胡俊栋,杨红霞,等.高效液相色谱-电感耦合等离子体质谱法快速测定天然水中无机砷的形态[J].分析实验室,2014,33(4):462-465.LIU Wei,HU Jun-dong,YANG Hong-xia,et al.Rapid determination of inorganic arsenic in natural water by high performance liquid chromatographyinductively coupled plasma mass spectrometry[J].Chinese Journal of Analysis Laboratory,2014,33(4):462-465.(in Chinese)
[26]干宁,李榕生,李天华,等.高效液相色谱-氢化物发生-动态反应池-电感耦合等离子体质谱法检测废水中4种砷形态[J].冶金分析,2009,29(4):14-19.GAN Ning,LI Rong-sheng,LI Tian-hua,et al.Determination of four arsenic species in waste waters by high performance liquid chromatography-hydride generation-dynamic reaction cell-inductively coupled plasma mass spectrometry[J].Metallurgical Analysis,2009,29(4):14-19.(in Chinese)
[27]CASTILLO A,ROIG-NAVARRO A F,POZO O J.Capabilities of microbore columns coupled to inductively coupled plasma mass spectrometry in speciation of arsenic and selenium[J].J Chromatogr:A,2008,1202(2):132-137.
[28]韩梅,赵国兴,李淑珍,等.毛细管电泳-电感耦合等离子体质谱法测定地下水中不同形态的砷[J].分析化学,2013,41(11):1780-1781.HAN Mei,ZHAO Guo-xing,LI Shu-zhen,et al.Speciation analysis of arsenic in groundwater by capillary electrophoresis-inductively coupled plasma mass spectrometry[J].Chinese Journal of Analytical Chemistry,2013,41(11):1780-1781.(in Chinese)
[29]要志丹,马继平,胡钢强,等.离子色谱-氢化物发生原子荧光法测定海水中4种不同形态的砷[J].青岛理工大学学报,2014,35(5):58-63.YAO Zhi-dan,MA Ji-ping,HU Gang-qiang,et al.Determination of 4arsenic spceciations in seawater by ion chromatography-hydride generation-atomoc fluorescence spectrometry[J].Journal of Qingdao Technological University,2014,35(5):58-63.(in Chinese)
[30]PENA-PEREIRA F,ISELA L,BENDICHO C.Miniaturized preconcent-ration methods based on liquid-liquid extraction and their application in inorganic ultratrace analysis and speciation:A review[J].Spectrochim Acta:Part B,2009,64(1):1-15.
[31]JIA X Y,GONG D R,WANG J N,et al.Arsenic speciation in environmental waters by a new specific phosphine modified polymer microspherepre concentration and HPLC-ICP-MS determination[J].Talanta,2016,160:437-443.
[2]BASHDAR S,FOULKES M E,HILL S J.Coupled techniques for arsenic speciation in food and drinking water:A review[J].J Anal At Spectrom,2015,30:102-118.
[3]LEAL P M,ALONSO E V,LóPEZ Guerrero M M,et al.Speciation analysis of inorganic arsenic by magnetic solid phase extraction on-line with inductively coupled mass spectrometry determination[J].Talanta,2018,184:251-259.
[4]KOMOROWICZ I,BARA?KIEWICZ D.Arsenic and its speciation in water samples by high performance liquid chromatography inductively coupled plasma mass spectrometry:Last decade review[J].Talanta,2011,84:247-261.
[5]ANAWARA H M.Arsenic speciation in environmental samples by hydride generation and electrothermal atomic abso rption spectrometry[J].Talanta,2012,88:30-42.
[6]MA J P,XIAO R H,LI J H,et al.Determination of 16polycyclic aromatic hydrocarbons in environmental water samples by solidphase extraction using multi-walled carbon nanotubes as adsorbent coupled with gas chromatography-mass spectrometry[J].J Chromatogr:A,2010,1217:5462-5469.
[7]马继平,李茉,赵秀华,等.固相萃取-反相高效液相色谱法测定水中的邻苯二甲酸酯[J].分析实验室,2009,28(3):6-9.MA Ji-ping,LI Mo,ZHAO Xiu-hua,et al.Determination of phthalate esters in water by SPE-RPHPLC[J].Chinese Journal of Analysis Laboratory,2009,28(3):6-9.(in Chinese)
[8]CHEN S Z,ZHAN X L,LU D B,et al.Speciation analysis of inorganic arsenic in natural water by carbon nanofibers separation and inductively coupled plasma mass spectrometry determination[J].Anal Chim Acta,2009,634(2):192-196.
[9]CHEN D H,HUANG C Z,HE M,et al.Separation and preconcentration of inorganic arsenic species in natural water samples with 3-(2-aminoethylamino)propyltrimethoxysilane modified ordered mesoporous silica micro-column and their determination by inductively coupled plasma optical emission spectrometry[J].J Hazard Mater,2009,164(2/3):1144-1151.
[10]LI P,ZHANG X Q,CHEN Y J,et al.One-pot synthesis of thiol-and aminebifunctionalized mesoporous silica and applications in uptake and speciation of arsenic[J].RSC Adv,2014,4:49421-49428.
[11]PENG H Y,ZHANG N,HE M,et al.Simultaneous speciation analysis of inorganic arsenic,chromium and selenium in environmental waters by 3-(2-aminoethylamino)propyltrimethoxysilane modified multi-wall carbon nanotubes packed microcolumn solid phase extraction and ICP-MS[J].Talanta,2015,131:266-272.
[12]ALI J,TUZEN M,TASNEEN G K,et al.Inorganic arsenic speciation in water samples by miniaturized solid phase microextraction using a new polystyrene polydimethyl siloxane polymer in micropipettetip of syringe system[J].Talanta,2016,161:450-458.
[13]MA J P,YAO Z D,HOU L W,et al.Metal organic frameworks(MOFs)for magnetic solid-phase extraction of pyrazole/pyrrole pesticides in environmental water samples followed by HPLC-DAD determination[J].Talanta,2016,161:686-692.
[14]MA J P,JIANG L H,WU G G,et al.Determination of six sulfonylurea herbicides in environmental watersamples by magnetic solidphase extraction using multi-walledcarbon nanotubes as adsorbents coupled with high-performanceliquid chromatography[J].J Chromatogr:A,2016,1466:12-20.
[15]侯丽玮,马继平,姜莲华.基于离子液体的磁性富集技术及其在分析化学中的应用进展[J].分析测试学报,2015,34(6):715-723.HOU Li-wei,MA Ji-ping,JIANG Lian-hua.Progresses in magnetic enrichment techniques based on ionic liquids and their applications in analytical chemistry[J].Journal of Instrumental Analysis,2015,34(6):715-723.(in Chinese)
[16]HUANG C Z,XIE W,LI X.Speciation of inorganic arsenic in environmental waters using magnetic solid phase extraction and preconcentration followed by ICP-MS[J].Microchim Acta,2011,173(1/2):165-172.
[17]MA J P,LU W H,CHEN L X.Recent advances in dispersive liquid-liquid microextraction for organic compounds analysis in environmental water:A review[J].Curr Anal Chem,2012,8(1):78-90.
[18]RICARDO E R,LPEZ-GARCA I,HERNNDEZ-CRDOBA M.Speciation of very low amounts of arsenic and antimony in waters using dispersive liquid-liquid microextraction and electrothermal atomic absorption spectrometry[J].Spectrochim Acta:Part B,2009,64(4):329-333.
[19]ZOUNR R A,TUZEN M,KHUHAWAR M Y.Ultrasound assisted deep eutectic solvent based on dispersive liquid liquid microextraction of arsenic speciation in water and environmental samples by electrothermal atomic absorption spectrometry[J].J MolLiq,2017,242:441-446.
[20]LI S,WANG M,ZHONG Y Z,et al.Cloud point extraction for trace inorganic arsenic speciation analysis in water samples by hydride generation atomic fluorescence spectrometry[J].Spectrochim Acta:Part B,2015,111:74-79.
[21]边静,徐芳,李玲辉,等.氢化物发生-原子荧光光谱法测定海水中As(III)和As(V)[J].光谱学与光谱分析,2010,30(10):2834-2837.BIAN Jing,XU Fang,LI Ling-hui,et al.Determination of As(III)and As(V)in sea water by hydride generation atomic fluorescence spectrometry[J].Spectroscopy and Spectral Analysis,2010,30(10):2834-2837.(in Chinese)
[22]LóPEZ-GARCíA I,MARíN-HERNáNDEZ J J,HERNáNDEZ-CóRDOBA M.Magnetic ferrite particles combined with electrothermal atomic absorption spectrometry for the speciation of low concentrations of arsenic[J].Talanta,2018,181:6-12.
[23]ULUSOY H I,AKCAY M,ULUSOY S,et al.Determination of ultra trace arsenic species in water samples by hydride generation atomic absorption spectrometry after cloud point extraction[J].Anal Chim Acta,2011,703(2):137-144.
[24]RAHMAN I M M,BEGUM Z A,NAKANO M,et al.Selective separation of arsenic species from aqueous solutions with immobilized macrocyclic material containing solid phase extraction columns[J].Chemosphere,2011,82(4):549-556.
[25]刘崴,胡俊栋,杨红霞,等.高效液相色谱-电感耦合等离子体质谱法快速测定天然水中无机砷的形态[J].分析实验室,2014,33(4):462-465.LIU Wei,HU Jun-dong,YANG Hong-xia,et al.Rapid determination of inorganic arsenic in natural water by high performance liquid chromatographyinductively coupled plasma mass spectrometry[J].Chinese Journal of Analysis Laboratory,2014,33(4):462-465.(in Chinese)
[26]干宁,李榕生,李天华,等.高效液相色谱-氢化物发生-动态反应池-电感耦合等离子体质谱法检测废水中4种砷形态[J].冶金分析,2009,29(4):14-19.GAN Ning,LI Rong-sheng,LI Tian-hua,et al.Determination of four arsenic species in waste waters by high performance liquid chromatography-hydride generation-dynamic reaction cell-inductively coupled plasma mass spectrometry[J].Metallurgical Analysis,2009,29(4):14-19.(in Chinese)
[27]CASTILLO A,ROIG-NAVARRO A F,POZO O J.Capabilities of microbore columns coupled to inductively coupled plasma mass spectrometry in speciation of arsenic and selenium[J].J Chromatogr:A,2008,1202(2):132-137.
[28]韩梅,赵国兴,李淑珍,等.毛细管电泳-电感耦合等离子体质谱法测定地下水中不同形态的砷[J].分析化学,2013,41(11):1780-1781.HAN Mei,ZHAO Guo-xing,LI Shu-zhen,et al.Speciation analysis of arsenic in groundwater by capillary electrophoresis-inductively coupled plasma mass spectrometry[J].Chinese Journal of Analytical Chemistry,2013,41(11):1780-1781.(in Chinese)
[29]要志丹,马继平,胡钢强,等.离子色谱-氢化物发生原子荧光法测定海水中4种不同形态的砷[J].青岛理工大学学报,2014,35(5):58-63.YAO Zhi-dan,MA Ji-ping,HU Gang-qiang,et al.Determination of 4arsenic spceciations in seawater by ion chromatography-hydride generation-atomoc fluorescence spectrometry[J].Journal of Qingdao Technological University,2014,35(5):58-63.(in Chinese)
[30]PENA-PEREIRA F,ISELA L,BENDICHO C.Miniaturized preconcent-ration methods based on liquid-liquid extraction and their application in inorganic ultratrace analysis and speciation:A review[J].Spectrochim Acta:Part B,2009,64(1):1-15.
[31]JIA X Y,GONG D R,WANG J N,et al.Arsenic speciation in environmental waters by a new specific phosphine modified polymer microspherepre concentration and HPLC-ICP-MS determination[J].Talanta,2016,160:437-443.
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