构建红外光谱显微系统实验平台——原位模拟物质反应动力学过程
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摘要
本项目通过对商用布鲁克Vertex 70v真空型红外光谱仪进行拓展,来构建一套水平红外光路的系统,并与红宝石测压系统、外加温温控系统联用,适用于高压、高/低温测量的傅立叶变换红外显微系统,从而真正实现在原位条件下观察与研究地球内部物质的性质和结构特征的实验平台。在此平台上,模拟并观察在俯冲带中不同深度(温压)环境下的绿帘石红外光谱特征,同时结合拉曼光谱特征,了解晶体结构和晶体化学的稳定性、水溶解度、高压化学和高压物理学现象,从而窥视洋壳/陆壳俯冲全过程中矿物物理化学性质及其水循环的动力学演化。
This project is to develop a custom in-situ infrared( IR) microscope for high-pressure and high/low temperature FT-IR studies on Bruker Vertex 70 v vacuum FT-IR spectrometer. This microscope system is specially designed with horizontal IR beam together with a ruby pressure calibration system and a temperature control system of external heater,an ideal platform for in-situ highpressure and high/low temperature IR spectroscopic research on the properties and structures of the materials in the deep interiors of planets. High pressure and temperature IR spectra of epidote were obtained with this experimental platform to simulate and investigate its structure and water solubility under condition of the different temperature and pressure during subduction,together with mineral chemical characteristics and Raman data,to look insight into the dynamic evolution of mineral's physicochemical property and water cycle in the whole process of subduction. The data of epidote on IR spectroscopic and Raman spectroscopic research in-situ under highpressure and high temperature show that the structure of the epidote remained stable,while temperature increasing from room temperature to 873 K,pressure from 0. 1 GPa to 11. 87 GPa. In particular,the M-O bond with weak compressibility of the epidote is related to the substitution of Fe-Al on the octahedron. OH vibration spectrums in infrared spectrum are sudden increase and disappearance,which maybe related to redox of Fe. Our results demonstrate that epidotite can be stable at least within the range of P =11. 87 ～ 12. 73 GPa and T = 773 ～ 873 K. Therefore,epidotite,as hydrous mineral,could have carried water into the mantle.
This project is to develop a custom in-situ infrared( IR) microscope for high-pressure and high/low temperature FT-IR studies on Bruker Vertex 70 v vacuum FT-IR spectrometer. This microscope system is specially designed with horizontal IR beam together with a ruby pressure calibration system and a temperature control system of external heater,an ideal platform for in-situ highpressure and high/low temperature IR spectroscopic research on the properties and structures of the materials in the deep interiors of planets. High pressure and temperature IR spectra of epidote were obtained with this experimental platform to simulate and investigate its structure and water solubility under condition of the different temperature and pressure during subduction,together with mineral chemical characteristics and Raman data,to look insight into the dynamic evolution of mineral's physicochemical property and water cycle in the whole process of subduction. The data of epidote on IR spectroscopic and Raman spectroscopic research in-situ under highpressure and high temperature show that the structure of the epidote remained stable,while temperature increasing from room temperature to 873 K,pressure from 0. 1 GPa to 11. 87 GPa. In particular,the M-O bond with weak compressibility of the epidote is related to the substitution of Fe-Al on the octahedron. OH vibration spectrums in infrared spectrum are sudden increase and disappearance,which maybe related to redox of Fe. Our results demonstrate that epidotite can be stable at least within the range of P =11. 87 ～ 12. 73 GPa and T = 773 ～ 873 K. Therefore,epidotite,as hydrous mineral,could have carried water into the mantle.
引文
Anderson OL,Isaak DG and Yamamoto S.1989.Anharmonicity and the equation of state for gold.Journal of Applied Physics,65(4):1534-1543
Aske N,Kallevik H and Sjoblom J.2002.Water-in-crude oil emulsion stability studied by critical electric field measurements:Correlation to physico-chemical parameters and near-infrared spectroscopy.Journal of Petroleum Science and Engineering,36(1-2):1-17
Belov NV and Rumanova JM.1954.The crystal structure of epidote.Trudy Inst.Kryst.Akad.Nauk.SSSR,9:103-164
Beran A.2002.Infrared spectroscopy of micas.In:Mottana A,Sassi EP,Thompson JB Jr and Guggenheim S(eds.).Reviews in Mineralogy and Geochemistry.Volume 46:Micas:Crystal Chemistry&Metamorphic Petrology.Washington:Mineralogical Society of America,17-28
Birch F.1947.Finite elastic strain of cubic crystals.Physics Review,71(11):809-824
Bonazzi P and Menchetti S.1995.Monoclinic members of the epidote group:Effects of the AI幑幐Fe幑幐3+Fe2+substitution and of the entry of REE3+.Mineralogy and Petrology,53(1-3):133-153
Bradbury SE and Williams Q.2003.Contrasting bonding behavior of two hydroxyl-bearing metamorphic minerals under pressure:Clinozoisite and topaz.American Mineralogist,88(10):1460-1470
Braithwaite JS,Wright K and Catlow CRA.2003.A theoretical study of the energetics and IR frequencies of hydroxyl defects in forsterite.Journal of Geophysical Research:Solid Earth,108(B6):2284
Burns RG and Strens RGJ.1967.Structural interpretation of polarized absorption spectra of the Al-Fe-Mn-Cr epidotes.Mineralogical Magazine,36(278):204-226
Busigny V,Cartigny P,Philippot P and Javoy M.2003.Ammonium quantification in muscovite by infrared spectroscopy.Chemical Geology,198(1-2):21-31
Carbonin S and Molin G.1980.Crystal-chemical considerations on eight metamorphic epidotes.Neues Jahrbuch fur MineralogieAbhandlungen,139:205-215
Decker DL.1971.High-pressure equation of state for Na Cl,KCl,and CsCl.Journal of Applied Physics,42(8):3239-3244
Della Ventura G,Mottana A,Parodi GC and Griffin WL.1996.FTIRspectroscopy in the OH-stretching region of monoclinic epidotes from Praborna(St.Marcel,Aosta Valley,Italy).European Journal of Mineralogy,8(4):655-665
Diaz M,Farmer VC and Prost R.2000.Characterization and assignment of far infrared absorption bands of K+in muscovite.Clays and Clay Minerals,48(4):433-438
Du JG,He DW,Gao XC,Gong ZZ,Wu XY,Zhou WG,Wang DJ,Zhai SM,Ji GF and Wei DQ.2011.Experimental and Theoretical Studies of Mineral and Rock at High Pressure and Temperature.Beijing:Seismological Press(in Chinese)
Enami M,Liou JG and Mattinson CG.2004.Epidote minerals in high P/T metamorphic terranes:Subduction zone and high-to ultrahighpressure metamorphism.Reviews in Mineralogy and Geochemistry,56(1):347-398
Fei YW,Ricolleau A,Frank M,Mibe K,Shen GY and Prakapenka V.2007.Toward an internally consistent pressure scale.Proceedings of the National Academy of Sciences of the United States of America,104(22):9182-9186
Forman RA,Piermarini GJ,Barnett JD and Block S.1972.Pressure measurement made by the utilization of ruby sharp-line luminescence.Science,176(4032):284-285
Funamori N and Jeanloz R.1997.High-pressure transformation of Al2O3.Science,278(5340):1109-1111
Giuli G,Bonazzi P and Menchetti S.1999.Al-Fe disorder in synthetic epidotes;A single-crystal X-ray diffraction study.American Mineralogist,84(5-6):933-936
Grasset O.2001.Calibration of the R ruby Fluorescence lines in the pressure range(0~1GPa)and the temperature range(250~300K).High Pressure Research,21(3-4):139-157
Han L,Zhou YS and He CR.2013.Water-enhanced plastic deformation in felsic rocks.Science China(Earth Sciences),56(2):203-216
Hermann J.2002.Allanite:Thorium and light rare earth element carrier in subducted crust.Chemical Geology,192(3-4):289-306
Heuss-Aβbichler S.2000.Ein neues Ordnungsmodell für die Mischkristallreihe Klinozoisit-Epidot und das Granat-EpidotGeothermometer.Munich:Habilitationthesis,105
Hirose K,Sata N,Komabayashi T and Ohishi Y.2008.Simultaneous volume measurements of Au and Mg O to 140GPa and thermal equation of state of Au based on the Mg O pressure scale.Physics of the Earth and Planetary Interiors,167(3-4):149-154
Holmes NC,Moriarty JA,Gathers GR and Nellis WJ.1989.The equation of state of platinum to 660GPa(6.6Mbar).Journal of Applied Physics,66(7):2962-2967
Langer K and Raith M.1974.Infrared spectra of Al-Fe(Ⅲ)-epidotes and zoisites,Ca2(Al1-pFe3+p)Al2O(OH)[Si2O7][SiO4].American Mineralogist,59(11-12):1249-1258
Langer K,Abu-Eid RM and Anastasiou P.1976.Absorptionsspektren synthetischer Piemontite in den Bereichen 43000~11000cm-1(232,6~909,1nm)und 4000~250cm-1(2,5~40μm).Zeitshrift fur Kristallographie,144:434-436
Liebscher A and Gottschalk M.2004.The T-X dependence of the isosymmetric displacive phase transition in synthetic Fe3+-Al zoisite:A temperature-dependent infrared spectroscopy study.American Mineralogist,89(1):31-38
Mao HK.1978.High-pressure physics:Sustained static generation of 1.36 to 1.72 megabars.Science,200(4346):1145-1147
Mao HK,Xu J and Bell PM.1986.Calibration of the ruby pressure gauge to 800kbar under quasi-hydrostatic conditions.Journal of Geophysical Research:Solid Earth,91(B5):4673-4676
Matsui M,Parker SC and Leslie M.2000.The MD simulation of the equation of state of Mg O:Application as a pressure calibration standard at high temperature and high pressure.American Mineralogist,85(2):312-316
Nagasaki A and Enami M.1998.Sr-bearing zoisite and epidote in ultrahigh pressure(UHP)metamorphic rocks from the Su-Lu province,eastern China:An important Sr reservoir under UHP conditions.American Mineralogist,83(3-4):240-247
Nazzareni S,Skogby H and Zanazzi PF.2011.Hydrogen content in clinopyroxene phenocrysts from Salina mafic lavas(Aeolian arc,Italy).Contributions to Mineralogy and Petrology,162(2):275-288
Parkin KM and Burns RG.1980.High temperature crystal field spectra of transition metal-bearing minerals:Relevance to remote-sensed spectra of planetary surfaces.In:Proceedings of the 11thLunar and Planetary Science Conference.Houston:NASA,731-755
Poirier JP.2000.Introduction to the Physics of the Earth’s Interior.Cambridge:Cambridge University Press,63-109
Poli S and Schmidt MW.2004.Experimental subsolidus studies on epidote minerals.Reviews in Mineralogy and Geochemistry,56(1):171-195
Qin F,Wu X,Wang Y,Fan DW,Qin S,Yang K,Townsend JP and Jacobsen SD.2016.High-pressure behavior of natural single-crystal epidote and clinozoisite up to 40GPa.Physics and Chemistry of Minerals,43(9):649-659
Qin S,Wu X,Liu J,Liu J,Wu ZY,Li XD and Lu AH.2003.Compressibility of epidote up to 20GPa at 298K.Chinese Physics Letters,20(7):1172-1174
Rekhi S,Dubrovinsky L and Saxena S.1999.Temperature-induced ruby fluorescence shifts up to a pressure of 15GPa in an externally heated diamond anvil cell.High Temperature-High Pressure,31(3):299-305
Rosén P,Vogel H,Cunningham L,Reuss N,Conley DJ and Persson P.2010.Fourier transform infrared spectroscopy,a new method for rapid determination of total organic and inorganic carbon and biogenic silica concentration in lake sediments.Journal of Paleolimnology,43(2):247-259
Rossman GR.2006.Analytical methods for measuring water in nominally anhydrous minerals.In:Keppler H and Smyth JR(eds.).Water in Nominally Anhydrous Minerals.Reviews in Mineralogy and Geochemistry.Chantilly:Mineralogical Society of America,62:1-28
Shim SH,Duffy TS and Kenichi T.2002.Equation of state of gold and its application to the phase boundaries near 660km depth in Earth’s mantle.Earth and Planetary Science Letters,203(2):729-739
Shuai K and Yang XZ.2017.Quantitative analysis of H-species in anisotropic minerals by polarized infrared spectroscopy along three orthogonal directions.Contributions to Mineralogy and Petrology,172(2-3):14,doi:10.1007/s00410-017-1336-2
Speziale S,Zha CS,Duffy TS,Hemley RJ and Mao HK.2001.Quasihydrostatic compression of magnesium oxide to 52GPa:Implications for the pressure-volume-temperature equation of state.Journal of Geophysical Research:Solid Earth,106(B1):515-528
Su W,Ji ZP,Ye K,You ZD,Liu JB,Yu J and Cong BL.2004.Distribution of hydrous components in jadeite of the Dabie Mountains.Earth and Planetary Science Letters,222(1):85-100
Su W,Zhang M,Redfern SAT and Bromiley GD.2008.Dehydroxylation of omphacite of eclogite from the Dabie-Sulu.Lithos,105(1-2):181-190
Su W,Zhang M,Redfern SAT,Gao J and Klemd R.2009.OH in zoned amphiboles of eclogite from the western Tianshan,NW-China.International Journal of Earth Sciences,98(6):1299-1309
Su W,Zhou Q and Liu X.2013.Characteristic of pargasitic amphibole at high pressure by in situμ-Raman,μ-FTIR spectroscopy and synchrotron X-ray diffraction.In:American Geophysical Union,Fall Meeting 2013.Washington:AGU
Taran MN and Langer K.2000.Electronic absorption spectra of Fe3+in andradite and epidote at different temperatures and pressures.European Journal of Mineralogy,12(1):7-15
Tateyama H,Shimda S and Sudo T.1977.Estimation of K-O distance and tetrahedral rotation angle of K-micas from far-infrared absorption spectral data.American Mineralogist,62(5-6):534-539
Tokiwai K and Nakashima S.2010.Dehydration kinetics of muscovite by in situ infrared microspectroscopy.Physics and Chemistry of Minerals,37(2):91-101
Vennari CE,O’Bannon EF and Williams Q.2017.The ammonium ion in a silicate under compression:Infrared spectroscopy and powder X-ray diffraction of NH4Al Si3O8-buddingtonite to 30GPa.Physics and Chemistry of Minerals,44(2):149-161
Wei QG,Dubrovinskaia N and Dubrovinsky L.2011.Ruby and Sm:YAG fluorescence pressure gauges up to 120GPa and 700K.Journal of Applied Physics,110(4):043513,doi:10.1063/1.3624618
Xu JA,Mao HK and Bell PM.1986.High-pressure ruby and diamond fluorescence:Observations at 0.21 to 0.55 terapascal.Science,232(4756):1404-1406
Yang XZ and Keppler H.2011.In-situ infrared spectra of OH in olivine to 1100℃.American Mineralogist,96(2-3):451-454
Yao YP,Ye K,Liu JB,Cong BL and Wang QC.2000.A transitional eclogite-to high pressure granulite-facies overprint on coesite-eclogite at Taohang in the Sulu ultrahigh-pressure terrane,Eastern China.Lithos,52(1-4):109-120
Zhang M,Redfern SAT,Salje EKH,Carpenter MA and Hayward CL.2010a.Thermal behavior of vibrational phonons and hydroxyls of muscovite in dehydroxylation:In situ high-temperature infrared spectroscopic investigations.American Mineralogist,95(10):1444-1457
Zhang M,Redfern SAT,Salje EKH,Carpenter MA and Wang L.2010b.H2O and the dehydroxylation of phyllosilicates:An infrared spectroscopic study.American Mineralogist,95(11):1686-1693
杜建国,贺端威,高春晓,龚自正,伍向阳,周文戈,王多君,翟双猛,姬广富,魏冬青.2011.矿物岩石高温高压实验与理论研究.北京:地震出版社
Aske N,Kallevik H and Sjoblom J.2002.Water-in-crude oil emulsion stability studied by critical electric field measurements:Correlation to physico-chemical parameters and near-infrared spectroscopy.Journal of Petroleum Science and Engineering,36(1-2):1-17
Belov NV and Rumanova JM.1954.The crystal structure of epidote.Trudy Inst.Kryst.Akad.Nauk.SSSR,9:103-164
Beran A.2002.Infrared spectroscopy of micas.In:Mottana A,Sassi EP,Thompson JB Jr and Guggenheim S(eds.).Reviews in Mineralogy and Geochemistry.Volume 46:Micas:Crystal Chemistry&Metamorphic Petrology.Washington:Mineralogical Society of America,17-28
Birch F.1947.Finite elastic strain of cubic crystals.Physics Review,71(11):809-824
Bonazzi P and Menchetti S.1995.Monoclinic members of the epidote group:Effects of the AI幑幐Fe幑幐3+Fe2+substitution and of the entry of REE3+.Mineralogy and Petrology,53(1-3):133-153
Bradbury SE and Williams Q.2003.Contrasting bonding behavior of two hydroxyl-bearing metamorphic minerals under pressure:Clinozoisite and topaz.American Mineralogist,88(10):1460-1470
Braithwaite JS,Wright K and Catlow CRA.2003.A theoretical study of the energetics and IR frequencies of hydroxyl defects in forsterite.Journal of Geophysical Research:Solid Earth,108(B6):2284
Burns RG and Strens RGJ.1967.Structural interpretation of polarized absorption spectra of the Al-Fe-Mn-Cr epidotes.Mineralogical Magazine,36(278):204-226
Busigny V,Cartigny P,Philippot P and Javoy M.2003.Ammonium quantification in muscovite by infrared spectroscopy.Chemical Geology,198(1-2):21-31
Carbonin S and Molin G.1980.Crystal-chemical considerations on eight metamorphic epidotes.Neues Jahrbuch fur MineralogieAbhandlungen,139:205-215
Decker DL.1971.High-pressure equation of state for Na Cl,KCl,and CsCl.Journal of Applied Physics,42(8):3239-3244
Della Ventura G,Mottana A,Parodi GC and Griffin WL.1996.FTIRspectroscopy in the OH-stretching region of monoclinic epidotes from Praborna(St.Marcel,Aosta Valley,Italy).European Journal of Mineralogy,8(4):655-665
Diaz M,Farmer VC and Prost R.2000.Characterization and assignment of far infrared absorption bands of K+in muscovite.Clays and Clay Minerals,48(4):433-438
Du JG,He DW,Gao XC,Gong ZZ,Wu XY,Zhou WG,Wang DJ,Zhai SM,Ji GF and Wei DQ.2011.Experimental and Theoretical Studies of Mineral and Rock at High Pressure and Temperature.Beijing:Seismological Press(in Chinese)
Enami M,Liou JG and Mattinson CG.2004.Epidote minerals in high P/T metamorphic terranes:Subduction zone and high-to ultrahighpressure metamorphism.Reviews in Mineralogy and Geochemistry,56(1):347-398
Fei YW,Ricolleau A,Frank M,Mibe K,Shen GY and Prakapenka V.2007.Toward an internally consistent pressure scale.Proceedings of the National Academy of Sciences of the United States of America,104(22):9182-9186
Forman RA,Piermarini GJ,Barnett JD and Block S.1972.Pressure measurement made by the utilization of ruby sharp-line luminescence.Science,176(4032):284-285
Funamori N and Jeanloz R.1997.High-pressure transformation of Al2O3.Science,278(5340):1109-1111
Giuli G,Bonazzi P and Menchetti S.1999.Al-Fe disorder in synthetic epidotes;A single-crystal X-ray diffraction study.American Mineralogist,84(5-6):933-936
Grasset O.2001.Calibration of the R ruby Fluorescence lines in the pressure range(0~1GPa)and the temperature range(250~300K).High Pressure Research,21(3-4):139-157
Han L,Zhou YS and He CR.2013.Water-enhanced plastic deformation in felsic rocks.Science China(Earth Sciences),56(2):203-216
Hermann J.2002.Allanite:Thorium and light rare earth element carrier in subducted crust.Chemical Geology,192(3-4):289-306
Heuss-Aβbichler S.2000.Ein neues Ordnungsmodell für die Mischkristallreihe Klinozoisit-Epidot und das Granat-EpidotGeothermometer.Munich:Habilitationthesis,105
Hirose K,Sata N,Komabayashi T and Ohishi Y.2008.Simultaneous volume measurements of Au and Mg O to 140GPa and thermal equation of state of Au based on the Mg O pressure scale.Physics of the Earth and Planetary Interiors,167(3-4):149-154
Holmes NC,Moriarty JA,Gathers GR and Nellis WJ.1989.The equation of state of platinum to 660GPa(6.6Mbar).Journal of Applied Physics,66(7):2962-2967
Langer K and Raith M.1974.Infrared spectra of Al-Fe(Ⅲ)-epidotes and zoisites,Ca2(Al1-pFe3+p)Al2O(OH)[Si2O7][SiO4].American Mineralogist,59(11-12):1249-1258
Langer K,Abu-Eid RM and Anastasiou P.1976.Absorptionsspektren synthetischer Piemontite in den Bereichen 43000~11000cm-1(232,6~909,1nm)und 4000~250cm-1(2,5~40μm).Zeitshrift fur Kristallographie,144:434-436
Liebscher A and Gottschalk M.2004.The T-X dependence of the isosymmetric displacive phase transition in synthetic Fe3+-Al zoisite:A temperature-dependent infrared spectroscopy study.American Mineralogist,89(1):31-38
Mao HK.1978.High-pressure physics:Sustained static generation of 1.36 to 1.72 megabars.Science,200(4346):1145-1147
Mao HK,Xu J and Bell PM.1986.Calibration of the ruby pressure gauge to 800kbar under quasi-hydrostatic conditions.Journal of Geophysical Research:Solid Earth,91(B5):4673-4676
Matsui M,Parker SC and Leslie M.2000.The MD simulation of the equation of state of Mg O:Application as a pressure calibration standard at high temperature and high pressure.American Mineralogist,85(2):312-316
Nagasaki A and Enami M.1998.Sr-bearing zoisite and epidote in ultrahigh pressure(UHP)metamorphic rocks from the Su-Lu province,eastern China:An important Sr reservoir under UHP conditions.American Mineralogist,83(3-4):240-247
Nazzareni S,Skogby H and Zanazzi PF.2011.Hydrogen content in clinopyroxene phenocrysts from Salina mafic lavas(Aeolian arc,Italy).Contributions to Mineralogy and Petrology,162(2):275-288
Parkin KM and Burns RG.1980.High temperature crystal field spectra of transition metal-bearing minerals:Relevance to remote-sensed spectra of planetary surfaces.In:Proceedings of the 11thLunar and Planetary Science Conference.Houston:NASA,731-755
Poirier JP.2000.Introduction to the Physics of the Earth’s Interior.Cambridge:Cambridge University Press,63-109
Poli S and Schmidt MW.2004.Experimental subsolidus studies on epidote minerals.Reviews in Mineralogy and Geochemistry,56(1):171-195
Qin F,Wu X,Wang Y,Fan DW,Qin S,Yang K,Townsend JP and Jacobsen SD.2016.High-pressure behavior of natural single-crystal epidote and clinozoisite up to 40GPa.Physics and Chemistry of Minerals,43(9):649-659
Qin S,Wu X,Liu J,Liu J,Wu ZY,Li XD and Lu AH.2003.Compressibility of epidote up to 20GPa at 298K.Chinese Physics Letters,20(7):1172-1174
Rekhi S,Dubrovinsky L and Saxena S.1999.Temperature-induced ruby fluorescence shifts up to a pressure of 15GPa in an externally heated diamond anvil cell.High Temperature-High Pressure,31(3):299-305
Rosén P,Vogel H,Cunningham L,Reuss N,Conley DJ and Persson P.2010.Fourier transform infrared spectroscopy,a new method for rapid determination of total organic and inorganic carbon and biogenic silica concentration in lake sediments.Journal of Paleolimnology,43(2):247-259
Rossman GR.2006.Analytical methods for measuring water in nominally anhydrous minerals.In:Keppler H and Smyth JR(eds.).Water in Nominally Anhydrous Minerals.Reviews in Mineralogy and Geochemistry.Chantilly:Mineralogical Society of America,62:1-28
Shim SH,Duffy TS and Kenichi T.2002.Equation of state of gold and its application to the phase boundaries near 660km depth in Earth’s mantle.Earth and Planetary Science Letters,203(2):729-739
Shuai K and Yang XZ.2017.Quantitative analysis of H-species in anisotropic minerals by polarized infrared spectroscopy along three orthogonal directions.Contributions to Mineralogy and Petrology,172(2-3):14,doi:10.1007/s00410-017-1336-2
Speziale S,Zha CS,Duffy TS,Hemley RJ and Mao HK.2001.Quasihydrostatic compression of magnesium oxide to 52GPa:Implications for the pressure-volume-temperature equation of state.Journal of Geophysical Research:Solid Earth,106(B1):515-528
Su W,Ji ZP,Ye K,You ZD,Liu JB,Yu J and Cong BL.2004.Distribution of hydrous components in jadeite of the Dabie Mountains.Earth and Planetary Science Letters,222(1):85-100
Su W,Zhang M,Redfern SAT and Bromiley GD.2008.Dehydroxylation of omphacite of eclogite from the Dabie-Sulu.Lithos,105(1-2):181-190
Su W,Zhang M,Redfern SAT,Gao J and Klemd R.2009.OH in zoned amphiboles of eclogite from the western Tianshan,NW-China.International Journal of Earth Sciences,98(6):1299-1309
Su W,Zhou Q and Liu X.2013.Characteristic of pargasitic amphibole at high pressure by in situμ-Raman,μ-FTIR spectroscopy and synchrotron X-ray diffraction.In:American Geophysical Union,Fall Meeting 2013.Washington:AGU
Taran MN and Langer K.2000.Electronic absorption spectra of Fe3+in andradite and epidote at different temperatures and pressures.European Journal of Mineralogy,12(1):7-15
Tateyama H,Shimda S and Sudo T.1977.Estimation of K-O distance and tetrahedral rotation angle of K-micas from far-infrared absorption spectral data.American Mineralogist,62(5-6):534-539
Tokiwai K and Nakashima S.2010.Dehydration kinetics of muscovite by in situ infrared microspectroscopy.Physics and Chemistry of Minerals,37(2):91-101
Vennari CE,O’Bannon EF and Williams Q.2017.The ammonium ion in a silicate under compression:Infrared spectroscopy and powder X-ray diffraction of NH4Al Si3O8-buddingtonite to 30GPa.Physics and Chemistry of Minerals,44(2):149-161
Wei QG,Dubrovinskaia N and Dubrovinsky L.2011.Ruby and Sm:YAG fluorescence pressure gauges up to 120GPa and 700K.Journal of Applied Physics,110(4):043513,doi:10.1063/1.3624618
Xu JA,Mao HK and Bell PM.1986.High-pressure ruby and diamond fluorescence:Observations at 0.21 to 0.55 terapascal.Science,232(4756):1404-1406
Yang XZ and Keppler H.2011.In-situ infrared spectra of OH in olivine to 1100℃.American Mineralogist,96(2-3):451-454
Yao YP,Ye K,Liu JB,Cong BL and Wang QC.2000.A transitional eclogite-to high pressure granulite-facies overprint on coesite-eclogite at Taohang in the Sulu ultrahigh-pressure terrane,Eastern China.Lithos,52(1-4):109-120
Zhang M,Redfern SAT,Salje EKH,Carpenter MA and Hayward CL.2010a.Thermal behavior of vibrational phonons and hydroxyls of muscovite in dehydroxylation:In situ high-temperature infrared spectroscopic investigations.American Mineralogist,95(10):1444-1457
Zhang M,Redfern SAT,Salje EKH,Carpenter MA and Wang L.2010b.H2O and the dehydroxylation of phyllosilicates:An infrared spectroscopic study.American Mineralogist,95(11):1686-1693
杜建国,贺端威,高春晓,龚自正,伍向阳,周文戈,王多君,翟双猛,姬广富,魏冬青.2011.矿物岩石高温高压实验与理论研究.北京:地震出版社
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