ChemInform Abstract: Rietveld Refinement of the Crystal Structures of Rb2XSi5O12 (X: Ni, Mn).
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The title compounds are prepared by melting and quenching of stoichiometric amounts of Rb2CO3, SiO2, and NiO or MnO (1573 K, 1.5 h for the Ni compound; 1673 K, 2 h for the Mn compound) followed by crystallization at 1193 K (12 h).

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