ChemInform Abstract: Application of the Dimensional Reduction Formalism to Pb12 [Li2(P2O7)2 (P4O13)2](P4O13): A Phosphate Containing Three Types of Isolated P—O Groups.
Polycrystalline Pb12 [Li2(P2O7)2 (P4O13)2](P4O13) is prepared via calcination of stoichiometric amounts of Li2CO3, PbO, and NH4H2PO4 (Al2O3 crucible, 630 °C, 3 d).