A validated, rapid, simple and economical high-performance liquid-chromatography method to quantify palm tocopherol and tocotrienols
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- 作者：Yin Leng Kuaa ; Suyin Gana ; suyin.gan@nottingham.edu.my" class="auth_mail" title="E-mail the corresponding author ; Andrew Morrisb ; Hoon Kiat Ngc
- 关键词：AOAC ; Association of Official Agricultural Chemists ; AOCS ; American Oil Chemists&rsquo ; Society ; C30 ; triacontyl ; CDER ; Center for Drug Evaluation and Research ; CPO ; crude palm oil ; GC ; gas chromatography ; HPLC ; high ; performance liquid chromatography ; ICH ; The International Conference on Harmonization ; LOD ; limit of detection ; LOQ ; limit of quantification ; OH ; hydroxyl ; PFP ; pentafluorophenyl ; PTFE ; polytetrafluoroethylene ; R2 ; coefficient of determination ; RPO ; refined palm oil ; RSD ; relative
- 刊名：Journal of Food Composition and Analysis
- 出版年：2016
- 出版时间：October 2016
- 年：2016
- 卷：53
- 期：Complete
- 页码：22-29
- 全文大小：801 K
文摘
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The HPLC method to quantify tocols was rapid (last eluted peak ended at 8.8 min).
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The method had low solvent consumption (0.8 L/min).
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The method was simple with direct sample injection following dilution in n-hexane.
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The method was validated to assure its precision, accuracy and reliability.