Application of fractionized sampling and stacking for construction of an interface for online heart-cutting two-dimensional liquid chromatography
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- 作者：Baocheng Ji ; Bing Xia ; xiabing@cib.ac.cn" class="auth_mail" title="E-mail the corresponding author ; Jie Liu ; Yuanji Gao ; Lisheng Ding ; Yan Zhou ; zhouyan@cib.ac.cn" class="auth_mail" title="E-mail the corresponding author
- 关键词：Fractionized sampling and stacking strategy ; Heart-cutting ; 2D LC ; Interface
- 刊名：Journal of Chromatography A
- 出版年：2016
- 出版时间：30 September 2016
- 年：2016
- 卷：1466
- 期：Complete
- 页码：199-204
- 全文大小：1464 K
文摘
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A fractionized sampling and stacking interface was developed for 2D LC system.
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The interface was successfully applied in developing an online heart-cutting 2D LC.
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Large volume injection in 2D was achieved using the interface.
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Excellent peak compression efficiency was achieved in 2D.
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A complex TCM sample was successfully analyzed using the developed method.