High-sensitivity detection of biogenic amines with multiple reaction monitoring in fish based on benzoyl chloride derivatization
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- 作者：Yanqing Fua ; b ; Zhihui Zhoua ; b ; Yanli Lia ; b ; Xin Lua ; b ; Chunxia Zhaoa ; b ; zhaocx@dicp.ac.cn" class="auth_mail" title="E-mail the corresponding author ; Guowang Xua ; b ; xugw@dicp.ac.cn" class="auth_mail" title="E-mail the corresponding author
- 关键词：Liquid chromatography&ndash ; mass spectrometry ; Multiple reaction monitoring ; Biogenic amines ; Benzoyl chloride ; Derivatization
- 刊名：Journal of Chromatography A
- 出版年：2016
- 出版时间：23 September 2016
- 年：2016
- 卷：1465
- 期：Complete
- 页码：30-37
- 全文大小：1396 K
文摘
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An efficient and sensitive method was developed for biogenic amines detection.
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Bead-beating disruption and extraction using 5-sulfosalicylic acid improves extraction efficiency.
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Benzoyl chloride derivatization shortens the reaction time greatly.
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MRM detection provides higher sensitivity, better reproducibility and linearity.
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The established method was successfully applied to detect biogenic amines in different fishes.