Validation of analytical conditions for determination of polycyclic aromatic hydrocarbons in roasted coffee by gas chromatography-mass spectrometry
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- 作者：Guadalupe Marí ; a Guatemala-Moralesa ; Elisa Alejandra Beltrá ; n-Medinaa ; b ; Mario Alfonso Murillo-Tovarc ; d ; Priscilla Ruiz-Palominoa ; Rosa Isela Corona-Gonzá ; lezb ; Enrique Arriola-Guevarab ; arriole@hotmail.com" class="auth_mail" title="E-mail the corresponding author
- 关键词：Benzo[a]pyrene (PubChem CID ; 2336) ; Benzo[a]anthracene (PubChem CID ; 5954) ; Benzo[b]fluoranthene (PubChem CID ; 9153) ; Benzo[k]fluoranthene (PubChem CID ; 9158) ; Benzo[ghi]perylene (PubChem CID ; 9117) ; Chrysene (PubChem CID ; 9171) ; Dibenzo[ah]anthracene (PubChem CID ; 5889) ; Indeno[1 ; 2 ; 3-cd]pyrene (PubChem CID ; 13757897)
- 刊名：Food Chemistry
- 出版年：2016
- 出版时间：15 April 2016
- 年：2016
- 卷：197
- 期：part_PA
- 页码：747-753
- 全文大小：556 K
文摘
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Sample preparation comprised of ultrasonic extraction, saponification and purification.
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Validation of the analytical conditions allowed reproducibility of the analytical method.
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Low polarity solvents favored the ultrasound extraction of PAHs.
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Recoveries of carcinogenic PAHs was independent from concentration.
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Saponification and purification minimized interferences for PAHs identification.