One-pot synthesis of canola oil based biolubricants catalyzed by MoO3/Al2O3 and process optimization study
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- 作者：Asish K.R. Somidi ; Umashankar Das ; Ajay K. Dalai ; ajay.dalai@usask.ca" class="auth_mail" title="E-mail the corresponding author
- 关键词：Heterogeneous catalysis ; Epoxidation ; Vicinal di-O-acetylation ; Central composite design ; Canola oil ; Canola biodiesel
- 刊名：Chemical Engineering Journal
- 出版年：2016
- 出版时间：1 June 2016
- 年：2016
- 卷：293
- 期：Complete
- 页码：259-272
- 全文大小：1673 K
文摘
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Synthesis of biolubricants from canola oil and canola biodiesel as feed stocks.
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Preparation and physico-chemical characterization of MoO3/Al2O3.
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MoO3/Al2O3 is active catalyst for vicinal diacylation of unsaturated fatty acids.
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Development of one-pot synthesis procedure for two step reaction.
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Spectroscopic characterization and confirmation of vicinal di-O-acetylated products.