Validation of a novel and rapid method for the simultaneous determination of some phenolic organohalogens in human serum by GC-MS
详细信息 查看全文
- 作者：Patrice Dufoura ; b ; pdufour@ulg.ac.be" class="auth_mail" title="E-mail the corresponding author ; Catherine Pirarda ; b ; Corinne Charliera ; b
- 关键词：Phenolic organohalogens ; Serum ; GC-ENCI-MS ; Trimethylsilyldiazomethane
- 刊名：Journal of Chromatography B, Analytical Technologies in the Biomedical and Life Sciences
- 出版年：2016
- 出版时间：15 November 2016
- 年：2016
- 卷：1036-1037
- 期：Complete
- 页码：66-75
- 全文大小：1043 K
文摘
- •
A rapid method was developed for the determination of POH in human serum.
- •
The use of anionic exchange SPE reduces the number of extraction steps.
- •
The method was validated according the total error approach.
- •
Method successfully used to measure the POH concentration in real serum samples.