Interplay between sample size and grain size: Single crystalline vs. ultrafine-grained chromium micropillars

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• 作者：R. Fritz^a ; V. Maier-Kiener^b ; D. Lutz^a ; D. Kiener^a ; ^{daniel.kiener@unileoben.ac.at" class="auth_mail" title="E-mail the corresponding author}
• 关键词：Micromechanics ; Crystal plasticity ; Size effect ; Bcc ; Ultrafine-grained ; In-situ SEM
• 刊名：Materials Science & Engineering A
• 出版年：2016
• 出版时间：30 September 2016
• 年：2016
• 卷：674
• 期：Complete
• 页码：626-633
• 全文大小：1975 K

文摘

To gain insights into the influence of the microstructure on the strengthening behaviour in confined volumes, single crystalline (sxx) and ultrafine-grained (ufg) Cr micropillars were investigated using in-situ scanning electron microscope microcompression tests. Post-compression images of the sxx pillars indicate crystallographic slip, while the ufg pillars reveal a bulk-like deformation behaviour and an emergence of grains from the sample surface. Stress-strain curves of sxx samples show intermittent flow and a scaling behaviour agreeing well with other bcc metals investigated previously. Also for ufg samples a size-dependent strength with a reduced but non-negligible scaling exponent is determined. This latter ufg size effect contributes to an increasing influence of near-surface grains controlling plastic flow with decreasing pillar diameter. While for micron-sized pillars the strength differs between the two microstructures, the two scaling trends converge for sub-micron pillars with diameters close to the grain size, indicative of a transition from boundary-mediated to single crystal plasticity.