Comparative evaluation of the chiral recognition potential of single-isomer sulfated beta-cyclodextrin synthesis intermediates in non-aqueous capillary electrophoresis
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- 作者：Ida Fejősa ; Erzsé ; bet Vargab ; Gá ; bor Benkovicsb ; c ; Andrá ; s Darcsia ; Milo Malangab ; É ; va Fenyvesib ; Tamá ; s Sohajdab ; Lajos Szenteb ; Szabolcs Bé ; nia ; beni.szabolcs@pharma.semmelweis-univ.hu" class="auth_mail" title="E-mail the corresponding author
- 关键词：Non-aqueous chiral capillary electrophoresis ; Enantioseparation ; Host-guest interaction ; 1H NMR ; ROESY NMR ; Single-isomer cyclodextrin
- 刊名：Journal of Chromatography A
- 出版年：2016
- 出版时间：7 October 2016
- 年：2016
- 卷：1467
- 期：Complete
- 页码：454-462
- 全文大小：2056 K
文摘
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Enantiorecognition of single-isomer β-cyclodextrins was investigated.
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The enantioselectivity was monitored by non-aqueous capillary electrophoresis.
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The enantioselective properties were further studied by NMR spectroscopy.
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The 2-O-methylated-3-O-acetylated CD showed remarkable enantioselectivity.