3D imaging by serial block face scanning electron microscopy for materials science using ultramicrotomy
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- 作者：Teruo Hashimoto ; t.hashimoto@manchester.ac.uk" class="auth_mail" title="E-mail the corresponding author ; George E. Thompson ; Xiaorong Zhou ; Philip J. Withers
- 关键词：SBFSEM ; Ultramicrotomy ; Material science
- 刊名：Ultramicroscopy
- 出版年：2016
- 出版时间：April 2016
- 年：2016
- 卷：163
- 期：Complete
- 页码：6-18
- 全文大小：9592 K
文摘
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The roughness of the ultramicrotomed block face of AA2024 in Al area was 1.2 nm.
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Surface texture associated with chattering was evident in grains with 45° diamond knife.
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A 76° rake angle minimises the stress on the block face.
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Using the oscillating knife with a cutting speed of 0.04 mms−1 minimised the surface texture.
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A variety of material applications were presented.