Pseudosandwich-type POV K2H5[NiIIIV14O40]·19H2O (rong class="boldFont">1rong>) was synthesized, characterized.
Magnetic studies indicate that antiferromagnetic interaction exists in compound rong class="boldFont">1rong>.
Compound rong class="boldFont">1rong> is the first example of NiIII-containing POV and the second 3d transition metal embedded tetradecavanadate.
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