Silica sol assisted chromatographic NMR spectroscopy for resolution of trans- and cis-isomers
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- 作者：Ying Yanga ; Rui Wub ; Shaohua Huanga ; huangsh@qibebt.ac.cn" class="auth_mail" title="E-mail the corresponding author ; Zhengwu Baib
- 关键词：Chromatographic NMR spectroscopy ; DOSY ; Silica sol ; Resolution ; Isomer
- 刊名：Journal of Magnetic Resonance
- 出版年：2016
- 出版时间：April 2016
- 年：2016
- 卷：265
- 期：Complete
- 页码：210-214
- 全文大小：624 K
文摘
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Chromatographic NMR spectroscopy provides high resolution spectra using silica sol as a matrix.
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Silica sol assisted DOSY greatly enhances the resolution of trans/cis-isomers.
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Mixed solvents improve the resolution of chromatographic NMR spectroscopy.