Development of a new extraction method based on counter current salting-out homogenous liquid-liquid extraction followed by dispersive liquid-liquid microextraction: Application for the extraction and preconcentration of widely used pesticides from fruit juices
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- 作者：Mir Ali Farajzadeh ; mafarajzadeh@yahoo.com" class="auth_mail" title="E-mail the corresponding author ; mafarajzadeh@tabrizu.ac.ir" class="auth_mail" title="E-mail the corresponding author ; Behruz Feriduni ; Mohammad Reza Afshar Mogaddam
- 关键词：CCSHLLE ; Counter current salting-out homogenous liquid&ndash ; liquid extraction ; DAD ; Diode array detector ; DLLME ; Dispersive liquid&ndash ; liquid microextraction ; EF ; Enrichment factor ; ER ; Extraction recovery ; FID ; Flame ionization detector ; FPD ; Flame photometric detector ; HPLC ; High-performance liquid chromatography ; GC ; Gas chromatography ; LLE ; Liquid&ndash ; liquid extraction ; LOD ; Limit of detection ; LOQ ; Limit of quantification ; MS ; Mass spectrometry ; NPD ; Nitrogen phosphorous detector ; RSD
- 刊名：Talanta
- 出版年：2016
- 出版时间：1 January 2016
- 年：2016
- 卷：146
- 期：Complete
- 页码：772-779
- 全文大小：1310 K
文摘
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For the first time, a new version of SHLLE has been developed.
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The method is applied for the analysis of pesticide residues in fruit juices.
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LODs are achievable at ng g−1 using GC–FID.
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EFs and ERs between 544–600 and 87–96% are obtained, respectively.