Multiresidue analysis of endocrine-disrupting compounds and perfluorinated sulfates and carboxylic acids in sediments by ultra-high-performance liquid chromatography-tandem mass spectrometry
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- 作者：Chiara Cavaliere ; Anna Laura Capriotti ; annalaura.capriotti@uniroma1.it" class="auth_mail" title="E-mail the corresponding author ; Francesca Ferraris ; Patrizia Foglia ; Roberto Samperi ; Salvatore Ventura ; Aldo Laganà
- 关键词：Endocrine-disrupting compounds ; Sediments ; Graphitized carbon black ; Solid phase extraction (SPE) ; Liquid chromatography&ndash ; mass spectrometry (LC&ndash ; MS) ; Experimental design
- 刊名：Journal of Chromatography A
- 出版年：2016
- 出版时间：18 March 2016
- 年：2016
- 卷：1438
- 期：Complete
- 页码：133-142
- 全文大小：1385 K
文摘
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Method developed and validated for determining 32 endocrine disruptors in sediments.
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Perfluorinated compounds determined with estrogenic compounds for the first time.
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Clean up with carbon black cartridge reduced matrix effect keeping good recovery.
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A robust matrix matched calibration ensured good trueness and precision.