Analysis of the effective thermoelastic properties and stress fields in silicon nitride based on EBSD data

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• 作者：Yamen Othmani^a ; ^{yamen.othmani@partner.kit.edu" class="auth_mail" title="E-mail the corresponding author} ; Thomas Bö ; hlke^a ; ^{thomas.boehlke@kit.edu" class="auth_mail" title="E-mail the corresponding author} ; Tanja Lube^b ; ^{tanja.lube@unileoben.ac.at" class="auth_mail" title="E-mail the corresponding author} ; Andreas Fellmeth^c ; ^{andreas.fellmeth@kit.edu" class="auth_mail" title="E-mail the corresponding author} ; Zdenek Chlup^d ; ^{chlup@ipm.cz" class="auth_mail" title="E-mail the corresponding author} ; Francesco Colonna^e ; ^f ; ^{francesco.colonna@iwm.fraunhofer.de" class="auth_mail" title="E-mail the corresponding author} ; Adham Hashibon^e ; ^{adham.hashibon@iwm.fraunhofer.de" class="auth_mail" title="E-mail the corresponding author}
• 关键词：Silicon nitride ; EBSD data ; Hashin&ndash ; Shtrikman bounds ; Finite element analysis ; Thermomechanical behavior
• 刊名：Journal of the European Ceramic Society
• 出版年：2016
• 出版时间：April 2016
• 年：2016
• 卷：36
• 期：5
• 页码：1109-1125
• 全文大小：4581 K

文摘

The present work focuses on the determination of the effective thermoelastic properties and the statistical characterization of stress fluctuations in silicon nitride's local phases. For that purpose, full field finite element solutions have been considered, based on 3D electron backscatter diffraction (EBSD) data of silicon nitride. A second-order mean field homogenization scheme, consisting in Hashin–Shtrikman bounds, has been also considered. Ab-initio simulations have been performed in order to determine the temperature-dependent elastic properties of the local phases. The isotropic material microstructure has been checked based on both experimental results and full field solutions. The effective thermoelastic properties have been assessed with the newly obtained experimental results. The stress fluctuations within silicon nitride's local phases have been examined under mechanical and thermal loadings. It has been shown that the amorphous phase is the most vulnerable to fracture and to micro-cracks initiation.