Optimisation of recovery protocols for double-base smokeless powder residues analysed by total vaporisation (TV) SPME/GC-MS
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文摘

Forensic investigation of explosions requires appropriate protocols to recover residues.

Central composite design used to optimise recovery parameters for explosive residues on metal surfaces.

Optimised parameters applied to the recovery of post-blast residues after a pipe bomb detonation.

Successful detection of all target components across the majority of samples.

Methodology will assist in establishing ‘best practice’ procedures for explosive investigations.

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