X-ray tomography with 3D-EM are combined for imaging and quantification.
The features imaged are over a range of three orders of magnitude (7.7 μm–6.7 nm).
Quantification from images has a good agreement with nitrogen sorption, TOC and XRD.
The peaks of pore sizes distribution are correlative to pore types.
Organic matter and clay mineral connectivity is quantified for gas transport studies.