Laccase initiated CC couplings: Various techniques for reaction monitoring
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- 作者：Claudia Engelmanna ; Sabine Illnerb ; Udo Kragla ; udo.kragl@uni-rostock.de" class="auth_mail" title="E-mail the corresponding author
- 关键词：2 ; 6-DMOP ; 2 ; 6-dimethoxyphenol ; 2 ; 6-DMOP-DQ ; 2 ; 6-dimethoxyphenol-diquinone ; 2 ; 6-DMP ; 2 ; 6-dimethylphenol ; 2 ; 6-DIPP ; 2 ; 6-diisopropylphenol ; 2 ; 6-DIPP-DQ ; 2 ; 6-diisopropylphenol-diquinone ; HQ ; hydroquinone ; 3-MC ; 3-methylcatechol ; 4-MC ; 4-methylcatechol ; 4-tert-BC ; 4-tert-butylcatechol ; 2 ; 4-DHBaldehyde ; 2 ; 4-dihydroxybenzaldehyde ; 2 ; 5-DHBacid ; 2 ; 5-dihydroxybenzoeic acid ; 2 ; 6-tert-BP ; 2 ; 6-tert-butylphenol ; ABTS ; 2 ; 2&prime ; -azino-bis(3-ethylbenzothiazoline-6-sulphonic acid)
- 刊名：Process Biochemistry
- 出版年：2015
- 出版时间：October 2015
- 年：2015
- 卷：50
- 期：10
- 页码：1591-1599
- 全文大小：2171 K
文摘
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A pathway to identify selective laccase (Novozym® 51003) mediated coupling reactions is investigated.
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In situ FT-IR analysis facilitates new insights in laccase initiated oxidative couplings.
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Different analytical methods gained detailed insights resulting in a synthesis of 7 g of pure diquinone.