Congener specific determination of polychlorinated naphthalenes in sediment and biota by gas chromatography high resolution mass spectrometry

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• 作者：R. Lega^a ; D. Megson^b ; ^c ; ^{dpmegson@hotmail.co.uk} ; C. Hartley^a ; P. Crozier^a ; K. MacPherson^a ; T. Kolic^a ; P.A. Helm^a ; A. Myers^a ; S.P. Bhavsar^a ; E.J. Reiner^a ; ^b
• 关键词：Polychlorinated naphthalenes ; PCN ; Sediment ; Biota ; Gas chromatography ; High resolution mass spectrometry
• 刊名：Journal of Chromatography A
• 出版年：2017
• 出版时间：6 January 2017
• 年：2017
• 卷：1479
• 期：Complete
• 页码：169-176
• 全文大小：1054 K
• 卷排序：1479

文摘

Congener specific analysis of 24 most toxic and abundant PCNs in sediment and biota. Femtogram IDLs and low to sub pg/g MDLs in sediment and biota. Average accuracy of 100% (precision of 12% RSD) for 34 spiked fish samples. Average accuracy of 104% (precision of 12% RSD) for 28 spiked sediment samples.