Comparison of single-drop microextraction with microvolume pipette extraction directly coupled with capillary electrophoresis for extraction and separation of tricyclic antidepressant drugs
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- 作者：Hui-Fen Wua ; b ; c ; d ; hwu@faculty.nsysu.edu.tw" class="auth_mail ; Suresh Kumar Kailasaa ; b ; e ; Ja-Yi Yanf ; Chen-Che Chinf ; Hsin-Yi Kua
- 关键词：SDME ; single-drop microextraction ; MVPE ; micro-volume pipette extraction ; CE ; capillary electrophoresis ; GC ; gas chromatography ; LC ; liquid chromatography ; HPLC ; high-performance liquid chromatography.
- 刊名：Journal of Industrial and Engineering Chemistry
- 出版年：25 July 2014
- 年：2014
- 卷：20
- 期：4
- 页码：2071-2076
- 全文大小：788 K
文摘
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We described the use of SDME- and MVPE-CE for drug analysis.
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The best extraction was achieved within 10 min and separated within 15 min.
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This method shows good reproducibility, with RSD values 4.3–8.7%.
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The LODs values were found to be 0.4–1.0 渭g mL−1 for SDME- and MVPE- CE.