Optimization of ultrasound-assisted dispersive liquid-liquid microextraction based on solidification of floating organic droplets by experimental design methodologies for determination of three anti-anxiety drugs in human serum and urine samples by high performance liquid chromatography
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- 作者：Sahar Farsimadan ; Nasser Goudarzi ; goudarzi@shahroodut.ac.ir" class="auth_mail" title="E-mail the corresponding author ; goudarzi10@gmail.com" class="auth_mail" title="E-mail the corresponding author ; Mansour Arab Chamjangali ; Ghadamali Bagherian
- 关键词：UA-DLLME-SFOD ; Anti-anxiety drugs ; Human serum samples ; Human urine samples ; Multiple response
- 刊名：Microchemical Journal
- 出版年：2016
- 出版时间：September 2016
- 年：2016
- 卷：128
- 期：Complete
- 页码：47-54
- 全文大小：701 K
文摘
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A UA-DLLME-SFOD method was developed for the pretreatment of three anti-anxiety drugs in human urine and serum samples.
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The proposed method is simple, reliable, inexpensive and environmentally friendly.
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Good analytical performance with low detection limits and acceptable recoveries of the target species was achieved.
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No significant matrix effects could be observed allowing a high analytical throughput.