Free electron lasers (FEL) are new generation accelerator-based short wa
velength light sources pro
viding high pulse intensity and femtosecond pulse duration, which enable in
vestigation of interaction of elementary excitations in solids under extreme conditions. Using the FLASH facility of HASYLAB at DESY (Hamburg, Germany), we in
vestigated the response of different materials with scintillating properties based on intrinsic emissions to the 25.6 and 13.8 nm FEL radiation by means of time-resol
ved luminescence spectroscopy. FLASH deli
vered single pulses of 25 fs duration ha
ving energy per pulse up to 30 μJ resulting in power densities of
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12 W/cm
2 on crystals. As a function of excitation density we obser
ved the shortening of lifetime and non-exponential beha
viour of emission decays in CaWO
4, while the emission spectra recorded are comparable to those obtained at con
ventional excitation sources.