Gold nanocubes - Direct comparison of synthesis approaches reveals the need for a microfluidic synthesis setup for a high reproducibility
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- 作者：Matthias Thielea ; matthias.thiele@ipht-jena.de" class="auth_mail" title="E-mail the corresponding author ; Joanne Zi En Sohb ; Andrea Knauerc ; Daniell Malscha ; Ondrej Stranika ; Robert Mü ; llera ; Andrea Csá ; kia ; Thomas Henkela ; J. Michael Kö ; hlerc ; Wolfgang Fritzschea
- 关键词：meNP ; metal nanoparticle ; SPR ; surface plasmon resonance ; LSPR ; localized surface plasmon resonance ; GS 1 ; growth solution 1 ; GS 2 ; growth solution 2 ; DCS ; differential centrifugal sedimentation ; SF ; segmented flow ; FOM ; Figure Of Merit ; RI ; refractive index ; RIU ; refractive index unit ; FWHM ; full wide at half maximum
- 刊名：Chemical Engineering Journal
- 出版年：2016
- 出版时间：15 March 2016
- 年：2016
- 卷：288
- 期：Complete
- 页码：432-440
- 全文大小：2294 K
文摘
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Pointing out the need of four steps-synthesis (different incubation times) of Au-cubes.
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Investigates kinetic study and highlights the variations for different growth steps.
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We create a FOM (TEM, UV–VIS) for easy quantifications of the critical parameters.
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Discusses the need of reactor types (batch, microfluidics) for different parameters.
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Show automation ways, raise in yield/shape & reduced material usage by microfluidics.