Zirconium and aluminum oxyhydroxides 25–44 nm particles were obtained during sol–gel synthesis.
Growth rate of primary particles in mixed Zr–Al solution is twice higher than in pure.
Reduction of carbamide concentration from M:carbamide = 1:3 to 1:1.75 leads to increasing of particles growth rate by 1.7 times.
Nanoparticles form highly porous structures due to aggregation of 50–60 nm particles in 1–10 渭m clusters.