Optimization of a rapid QuEChERS sample treatment method for HILIC-MS2 analysis of paralytic shellfish poisoning (PSP) toxins in mussels
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- 作者：Monica Mattarozzia ; monica.mattarozzi@unipr.it" class="auth_mail" title="E-mail the corresponding author ; Marco Miliolia ; Federica Bianchia ; Antonella Cavazzaa ; Silvia Pigozzib ; Anna Milandrib ; Maria Careria
- 关键词：Paralytic shellfish poisoning (PSP) toxins ; Hydrophilic interaction liquid chromatography-tandem mass spectrometry (HILIC-MS2) ; Mussels ; QuEChERS ; Experimental design optimization
- 刊名：Food Control
- 出版年：2016
- 出版时间：February 2016
- 年：2016
- 卷：60
- 期：Complete
- 页码：138-145
- 全文大小：1130 K
文摘
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Development of a rapid sample pretreatment for saxitoxins determination in mussels.
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QuEChERS protocol optimisation by multivariate approach.
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Analytical method by HILIC-ESI-MS2 successfully validated.
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Suitability of the method for analysis of samples from different areas.